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1.发明授权
公开(公告)号：US4655961A
公开(公告)日：1987-04-07
申请号：US688227
申请日：1985-01-02
IPC分类号： C08K3/00 , B01D19/04 , C08K3/34 , C08K5/00 , C08K5/01 , C08K5/05 , C08K13/02 , C08L7/00 , C08L21/00 , C08L33/00 , C08L33/02 , C08L67/00 , C08L101/00 , C09D5/02 , C09D7/00 , C09D7/12 , B01D17/00
CPC分类号： B01D19/04 , B01D19/0404
摘要： The formation of troublesome microfoams in aqueous lacquer and synthetic resin dispersions, particularly in gloss lacquers, is prevented by the addition of from 0.01 to 1.5% by weight of a silicone-free foam inhibitor mixture. These foam inhibitor mixtures contain (a) from 70 to 98% by weight of a liquid, branched C.sub.16 -C.sub.30 alcohol, (b) from 0.5 to 20% by weight of hard paraffin, and (c) from 0.05 to 5% by weight of hydrophobized finely divided silica, and, optionally, small quantities of other ingredients.
摘要翻译： 在水性漆和合成树脂分散体，特别是光泽漆中形成麻烦的微泡，通过加入0.01至1.5重量％的无硅氧烷泡沫抑制剂混合物来防止。 这些泡沫抑制剂混合物包含（a）70至98重量％的液体，支链C16-C30醇，（b）0.5至20重量％的硬石蜡，和（c）0.05至5重量％ 疏水化的细分二氧化硅，以及任选的少量其它成分。
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公开(公告)号：US4655960A
公开(公告)日：1987-04-07
申请号：US688225
申请日：1985-01-02
IPC分类号： C08K3/00 , B01D19/04 , C08K3/34 , C08K5/00 , C08K5/01 , C08K5/05 , C08K13/02 , C08L7/00 , C08L21/00 , C08L33/00 , C08L33/02 , C08L67/00 , C08L101/00 , C09D5/02 , C09D7/00 , C09D7/12 , B01D17/00
CPC分类号： C09D7/00 , B01D19/04 , B01D19/0404
摘要： The formation of troublesome microfoams in aqueous lacquer and synthetic resin dispersions, particularly in gloss lacquers, is prevented by the addition of from about 0.01 to about 1.5% by weight of a silicone-free foam inhibitor mixture. This mixture consists of (a) from about 70 to about 98% by weight of a mineral oil liquid at room temperature or a mixture of such mineral oil with a C.sub.16 -C.sub.30 branched alcohol of the following formulaR.sup.1 --CH.sub.2 --CH.sub.2 --CHR.sup.2 --CH.sub.2 --CH.sub.2 --CH.sub.2 OH (I)in which R.sup.1 and R.sup.2 are C.sub.4 -C.sub.16 alkyl radicals, (b) from about 0.2 to about 5% by weight of a microcrystalline wax, (c) from about 0.5 to about 20% by weight of hard paraffin, (d) from 0.05 to 5% by weight of hydrophobized finely divided silica, and (e) from 0 to about 10% by weight of a soft paraffin (M.p. 32.degree.-42.degree. C.). Component (a) preferably consists of a mixture of mineral oil and branched alcohol (I) in a ratio of from 50:1 to 1:1.
摘要翻译： 通过加入约0.01至约1.5重量％的无硅氧烷泡沫抑制剂混合物可以防止水性漆和合成树脂分散体中特别是光泽漆中的麻烦的微泡的形成。 该混合物由（a）在室温下约70-约98重量％的矿物油液体或这种矿物油与具有下列通式的C16-C30支链醇的混合物R1-CH2-CH2-CHR2- （I）其中R 1和R 2是C 4 -C 16烷基，（b）约0.2至约5重量％的微晶蜡，（c）约0.5至约20重量％ 硬石蜡，（d）0.05-5重量％的疏水化细碎二氧化硅，和（e）0至约10重量％的软石蜡（Mp 32℃-42℃）。 组分（a）优选由矿物油和支链醇（I）的混合物组成，比例为50:1至1:1。
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公开(公告)号：US4418217A
公开(公告)日：1983-11-29
申请号：US257632
申请日：1981-04-27
IPC分类号： C07C43/164 , B01F17/42 , B01J27/00 , B01J27/02 , B01J27/16 , B01J29/00 , B01J29/04 , B01J31/00 , B01J31/02 , B01J31/08 , C07C41/00 , C07C41/48 , C07C43/11 , C07C43/30 , C07C43/315 , C07C67/00 , C08G4/00 , C08G65/00 , C08G65/32 , C08G65/331 , C08G65/34 , C11D1/72 , C07C41/14
CPC分类号： C08G65/331 , C07C43/30 , C08G4/00 , C08G65/34 , C11D1/721 , Y10S516/01
摘要： A process for the production of a mixed formal of polyglycol ethers having formulae selected from the group consisting of ##STR1## wherein R.sup.1 is a straight or branched chain alkyl having from 1 to 18 carbon atoms, and R.sup.2 is selected from the group consisting of hydrogen and straight or branched chain alkyl having from 1 to 17 carbon atoms, where the sum of the carbon atoms in R.sup.1 plus R.sup.2 is from 6 to 18, R.sup.3 is a member selected from the group consisting of monoalkylphenyl having from 14 to 26 carbon atoms, dialkylphenyl having from 14 to 26 carbon atoms, trialkylphenyl having from 14 to 26 carbon atoms, a straight or branched chain alkyl having from 8 to 22 carbon atoms, a straight or branched chain alkenyl having from 8 to 22 carbon atoms, and a radical having the formula ##STR2## wherein R.sup.1 and R.sup.2 have the above assigned values, and R.sup.5 is selected from the group consisting of a straight or branched chain alkyl having from 1 to 5 carbon atoms, phenyl and alkylphenyl having from 7 to 9 carbon atoms, R.sup.4 is a straight or branched chain alkyl having from 1 to 5 carbon atoms, A and B are selected from the group consisting of ethylene and isopropylene, m and n are integers from 0 to 50, p is an integer from 2 to 50, and q is an integer from 0 to 3, where the sum of m plus n is from 2 to 50, consisting essentially of the steps of(1) reacting a polyglycol ether having the formulae selected from the group consisting of ##STR3## wherein R.sup.1, R.sup.2, R.sup.3, A, m, n and p have the above-assigned meanings, with a diformal having the formulaR.sup.4 --O--(B--O).sub.q --CH.sub.2 --(O--B).sub.q --O--R.sup.4wherein R.sup.4, B and q have the above-assigned meanings, at a temperature of from 60.degree. to 150.degree. C. in the presence of a strong acid, while employing from 2 to 10 mols of said diformal per mol of hydroxyl groups in said polyglycol ether.(2) distilling off the alcohol formed having the formulaR.sup.4 --O--(B--O).sub.q --H(3) neutralizing,(4) distilling of unreacted diformal, and(5) recovering said mixed formal of polyglycol ethers; as well as novel mixed formals of polyglycol ethers produced by the process.
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4.发明授权Stable, aqueous or aqueous-alcoholic solutions of fat-soluble perfume oils containing hydroxyalkyl ether-ethoxylates 失效含有羟烷基醚 - 乙氧基化物的脂溶性香料油的稳定的含水或含水溶液
公开(公告)号：US4184985A
公开(公告)日：1980-01-22
申请号：US923575
申请日：1978-07-11
摘要： Stable, aqueous or aqueous-alcoholic solutions of fat-soluble perfume oils, containing hydroxyalkyl ether-ethoxylates of the formula ##STR1## wherein R.sub.1 and/or R.sub.2 are an alkyl group having 1 to 24 carbon atoms or hydrogen, and R.sub.3 and/or R.sub.4 are an alkyl group having 2 to 22 carbon atoms or hydrogen, and x and y independently are integers of from 1 to 16, with the proviso that the total of the carbon atoms of R.sub.1 +R.sub.2 or R.sub.3 +R.sub.4 is from 2 to 26 and the total of the integers x+y is a value of from 2 to 18.
摘要翻译： 含有下式的羟烷基醚 - 乙氧基化物的脂溶性香料油的稳定的含水或含水醇溶液，其中R 1和/或R 2是具有1至24个碳原子的烷基或氢，R 3 和/或R 4为具有2至22个碳原子的烷基或氢，x和y独立地为1至16的整数，条件是R1 + R2或R3 + R4的碳原子总数来自 2〜26，整数x + y的总和为2〜18。
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公开(公告)号：US4765875A
公开(公告)日：1988-08-23
申请号：US527316
申请日：1983-08-29
IPC分类号： C09G1/00 , C07C309/17 , C07C309/62 , C07C309/80 , C09G1/18 , C14C9/02 , C07C143/90
CPC分类号： C14C9/02 , C07C309/00
摘要： This invention relates to sulfonated lubricating agents for leather and furs. More specifically, this invention relates to a process for the production of sulfonated lubricating agent for leather and tanned furs consisting of the steps of:(a) sulfochlorinating higher fatty acids or esters of higher fatty acids having chain lengths of from 8 to 24 carbon atoms with chlorine and SO.sub.2 at a temperature of from about 20.degree. to 90.degree. C. under UV-radiation for a time sufficient to obtain a compound having a chlorine content of from about 5 to 30 percent by weight and a content of --SO.sub.2 Cl groups of from about 1 to 20 percent by weight, the ratio of chlorine atoms to --SO.sub.2 Cl groups being from about 0.7:1 to 70:1; and(b) forming a water-emulsifiable alkali metal, ammonium, or lower alkyl-ammonium salt of the compound produced in step (a).
摘要翻译： 本发明涉及用于皮革和毛皮的磺化润滑剂。 更具体地说，本发明涉及生产用于皮革和鞣皮的磺化润滑剂的方法，该方法包括以下步骤：（a）将链长为8至24个碳原子的高级脂肪酸或高级脂肪酸酯磺基氯化 在大约20-90℃的温度下用氯和SO2在UV辐射下反应足以获得氯含量为约5-30％重量的化合物和-SO2Cl基团的含量 约1至20重量％，氯原子与-SO 2 Cl基团的比例为约0.7:1至70:1; 和（b）形成步骤（a）中制备的化合物的水可乳化的碱金属，铵或低级烷基 - 铵盐。
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公开(公告)号：US4654042A
公开(公告)日：1987-03-31
申请号：US869486
申请日：1986-06-02
IPC分类号： C09G1/00 , C07C309/17 , C07C309/62 , C07C309/80 , C09G1/18 , C14C9/02 , C07C143/90
CPC分类号： C14C9/02 , C07C309/00
摘要： This invention relates to sulfonated lubricating agents for leather and furs. More specifically, this invention relates to a process for the production of sulfonated lubricating agent for leather and tanned furs consisting of the steps of:(a) sulfochlorinating higher fatty acids or esters of higher fatty acids having chain lengths of from 8 to 24 carbon atoms with chlorine and SO.sub.2 at a temperature of from about 20.degree. to 90.degree. C. under UV-radiation for a time sufficient to obtain a compound having a chlorine content of from about 5 to 30 percent by weight and a content of --SO.sub.2 Cl groups of from about 1 to 20 percent by weight, the ratio of chlorine atoms to --SO.sub.2 Cl groups being from about 0.7:1 to 70:1; and(b) forming a water-emulsifiable alkaimetal, ammonium, or lower-alkyl-ammonium salt of the compound produced in step (a).
摘要翻译： 本发明涉及用于皮革和毛皮的磺化润滑剂。 更具体地说，本发明涉及生产用于皮革和鞣皮的磺化润滑剂的方法，该方法包括以下步骤：（a）将链长为8至24个碳原子的高级脂肪酸或高级脂肪酸酯磺基氯化 在大约20-90℃的温度下用氯和SO2在UV辐射下反应足以获得氯含量为约5-30％重量的化合物和-SO2Cl基团的含量 约1至20重量％，氯原子与-SO 2 Cl基团之比为约0.7:1至70:1; 和（b）形成步骤（a）中制备的化合物的水可乳化的烷基铵，铵或低级烷基 - 铵盐。
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7.发明授权Quaternary ammonium compounds, their preparation, and their use as softening agents 失效季铵化合物，它们的制备及其用作软化剂
公开(公告)号：US4281196A
公开(公告)日：1981-07-28
申请号：US83850
申请日：1979-10-11
申请人： Horst Rutzen , Jochen Heidrich , Martin Bischoff , Udo Kloubert , Peter Waltenberger , Ingo Wegener
发明人： Horst Rutzen , Jochen Heidrich , Martin Bischoff , Udo Kloubert , Peter Waltenberger , Ingo Wegener
IPC分类号： C11D1/62 , C11D3/00 , D06M13/372 , D06M13/463 , C07C91/26
CPC分类号： D06M13/372 , C11D1/62 , C11D3/001 , D06M13/463 , D06M2200/00 , D06M2200/20 , D06M2200/25 , D06M2200/50
摘要： This invention is directed to quaternary compounds of the formula ##STR1## wherein R.sup.1 represents an aliphatic hydrocarbon radical of from about 1 to 21 carbon atoms; R.sup.2 represents hydrogen or has the same meaning as R.sup.1, the total number of carbon atoms in R.sup.1 and R.sup.2 being from 6 to 22, and, when R.sup.2 is hydrogen, R.sup.1 has from 6 to 21 carbon atoms; R.sup.3 represents an alkyl or hydroxyalkyl group having from 1 to 4 carbon atoms or a radical of formula ##STR2## wherein R and R are devined above, X and Y are each either hydrogen or a methyl group, with the proviso that X and Y cannot both be a methyl group, and p is an integer of from 1 to 20; R.sup.4 represents an alkyl radical of from 1 to 4 carbon atoms; m and n are integers of from about 1 to 20; and A.crclbar. is an anion. The quaternary compounds are useful as fabric softeners.
摘要翻译： 本发明涉及式（I）的季铵化合物，其中R 1表示约1至21个碳原子的脂族烃基; R2表示氢或具有与R1相同的含义，R 1和R 2中的碳原子总数为6至22，并且当R 2为氢时，R 1具有6至21个碳原子; R3表示具有1至4个碳原子的烷基或羟烷基或式（Ia）的基团，其中R和R分别位于上，X和Y各自为氢或甲基，条件是X Y不能同时为甲基，p为1〜20的整数。 R4表示1〜4个碳原子的烷基; m和n为约1至20的整数; 而A（ - ）是阴离子。 四元化合物可用作织物柔软剂。
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公开(公告)号：US4226637A
公开(公告)日：1980-10-07
申请号：US962371
申请日：1978-11-20
IPC分类号： C08K9/00 , C08K9/04 , C08L67/00 , C09B67/08 , C09B67/20 , C09C1/24 , C09C1/36 , C09C3/00 , C09C3/08 , C09D3/00
CPC分类号： C09C3/006 , C09B67/0008 , C09B67/006 , C09C1/24 , C09C1/3623 , C01P2004/84
摘要： Dispersion adjuvants are described comprising .beta.-hydroxyalkyl esters of the formula ##STR1## wherein the R.sub.1 and R.sub.2 represent hydrogen or alkyl with 1 to 21 carbon atoms, in which at least one of R.sub.1 and R.sub.2 is alkyl and the sum of the carbon atoms in R.sub.1 and R.sub.2 ranges from 6 to 22, and wherein R.sub.3 represents alkyl with 1 to 8 carbon atoms, optionally substituted with 1 to 2 hydroxyl groups and/or interrupted by 1 to 2 ether bridges, as well as the adducts of compounds of Formula I with alkylene oxides, preferably ethylene oxide and/or propylene oxide. The dispersion adjuvants are coated on pigment and filler materials for paints and lacquers. The coating is applied before or during the dispersion of the materials in the paint or lacquer media or vehicle.
摘要翻译： 描述了分散助剂，其包含式（I）的β-羟烷基酯，其中R 1和R 2表示氢或具有1至21个碳原子的烷基，其中R 1和R 2中的至少一个是烷基， R 1和R 2中的碳原子的范围为6至22，并且其中R 3表示具有1至8个碳原子的烷基，任选被1至2个羟基取代和/或被1至2个醚桥连，以及化合物的加合物 具有环氧烷，优选环氧乙烷和/或环氧丙烷。 将分散助剂涂覆在颜料和用于油漆和漆的填料上。 涂料在材料分散在涂料或漆介质或载体中之前或期间施加。
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