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公开(公告)号：US08048193B2
公开(公告)日：2011-11-01
申请号：US12298313
申请日：2007-05-29
IPC分类号： B22F9/24
CPC分类号： B01J13/0043 , B22F1/0022 , B22F9/24 , B82Y30/00 , Y10S977/896
摘要： It is an object of the present invention to provide a method for producing gold colloid having a targeted particle size, a sharp particle size distribution and a uniform and perfect spherical shape. The present invention relates to a method for producing gold colloid including a nucleation step of forming nuclear colloidal particles by adding a first reducing agent to a first gold salt solution; and a growth step of growing nuclear colloid by adding a second gold salt and a second reducing agent to the solution of the nuclear colloidal particles, characterized in that the growth step is performed at least once; a citrate is used as the first reducing agent and an ascorbate is used as the second reducing agent; and the addition of the ascorbate in the growth step is performed simultaneously with addition of the second gold salt. According to the method for producing gold colloid of the present invention, gold colloid having a sharp particle size distribution and a uniform and perfect spherical shape can be obtained.
摘要翻译： 本发明的目的是提供一种具有目标粒度，尖锐的粒度分布和均匀且完美的球形形状的金胶体的制造方法。 本发明涉及一种生产金胶体的方法，包括通过向第一金盐溶液中加入第一还原剂形成核胶体颗粒的成核步骤; 以及通过向核胶体粒子的溶液中添加第二金盐和第二还原剂来生长核胶体的生长步骤，其特征在于，所述生长步骤至少进行一次; 使用柠檬酸盐作为第一还原剂，使用抗坏血酸作为第二还原剂; 并且在添加第二金盐的同时进行生长步骤中的抗坏血酸盐的添加。 根据本发明的金胶体的制造方法，可以获得具有尖锐的粒度分布和均匀且完美的球形的金胶体。
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公开(公告)号：US20100159471A1
公开(公告)日：2010-06-24
申请号：US12298313
申请日：2007-05-29
IPC分类号： G01N33/553
CPC分类号： B01J13/0043 , B22F1/0022 , B22F9/24 , B82Y30/00 , Y10S977/896
摘要： It is an object of the present invention to provide a method for producing gold colloid having a targeted particle size, a sharp particle size distribution and a uniform and perfect spherical shape. The present invention relates to a method for producing gold colloid including a nucleation step of forming nuclear colloidal particles by adding a first reducing agent to a first gold salt solution; and a growth step of growing nuclear colloid by adding a second gold salt and a second reducing agent to the solution of the nuclear colloidal particles, characterized in that the growth step is performed at least once; a citrate is used as the first reducing agent and an ascorbate is used as the second reducing agent; and the addition of the ascorbate in the growth step is performed simultaneously with addition of the second gold salt. According to the method for producing gold colloid of the present invention, gold colloid having a sharp particle size distribution and a uniform and perfect spherical shape can be obtained.
摘要翻译： 本发明的目的是提供一种具有目标粒度，尖锐的粒度分布和均匀且完美的球形形状的金胶体的制造方法。 本发明涉及一种生产金胶体的方法，包括通过向第一金盐溶液中加入第一还原剂形成核胶体颗粒的成核步骤; 以及通过向核胶体粒子的溶液中添加第二金盐和第二还原剂来生长核胶体的生长步骤，其特征在于，所述生长步骤至少进行一次; 使用柠檬酸盐作为第一还原剂，使用抗坏血酸作为第二还原剂; 并且在添加第二金盐的同时进行生长步骤中的抗坏血酸盐的添加。 根据本发明的金胶体的制造方法，可以获得具有尖锐的粒度分布和均匀且完美的球形的金胶体。
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3.发明授权CVD material compound and method for manufacturing the same and CVD method of ruthenium or ruthenium compound thin film 失效CVD材料化合物及其制造方法以及钌或钌化合物薄膜的CVD法公开(公告)号：US06555701B2
公开(公告)日：2003-04-29
申请号：US10175873
申请日：2002-06-21
申请人： Masayuki Saito , Junichi Taniuchi , Koji Okamoto , Hiroaki Suzuki
发明人： Masayuki Saito , Junichi Taniuchi , Koji Okamoto , Hiroaki Suzuki
IPC分类号： C07F1500
摘要： The present invention provides a CVD material compound based on an organic ruthenium compound, the organic ruthenium compound consisting of one of cis and trans isomers of tris (2,4-octa-dionato) ruthenium (III). The organic ruthenium compound which consists of cis or trans isomer can be isolated by the steps of preparing tris (2,4-octa-dionato) ruthenium (III) in any method, making the tris (2,4-octa-dionato) ruthenium (III) adsorbed on an adsorbent including alumina, bringing the adsorbent into contact with a first solvent to elute the trans isomer and then bringing the adsorbent into contact with a second solvent having a polarity higher than that of the first solvent to elute the cis isomer.
摘要翻译： 本发明提供一种基于有机钌化合物的CVD材料化合物，由三（2,4-octa-dionato）钌（III）的顺式和反式异构体之一组成的有机钌化合物。 由顺式或反式异构体组成的有机钌化合物可以通过以任何方法制备三（2,4-辛二醛）钌（III）的步骤来分离，制备三（2,4-辛二醛）钌 （III）吸附在包含氧化铝的吸附剂上，使吸附剂与第一溶剂接触以洗脱反式异构体，然后使吸附剂与极性高于第一溶剂的第二溶剂接触以洗脱顺式异构体 。
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4.发明授权Cis-oxalato(trans-1-1,2-cyclohexanediamine) Pt(II) complex having high optical purity and process of preparing same 失效具有高光学纯度的顺式（反式-1-1,2-环己二胺）Pt（II）络合物及其制备方法
公开(公告)号：US5420319A
公开(公告)日：1995-05-30
申请号：US117892
申请日：1993-09-07
IPC分类号： A61K31/555 , A61P35/00 , C07B53/00 , C07B57/00 , C07B63/00 , C07C209/88 , C07C211/36 , C07F15/00 , G07F15/00
CPC分类号： C07F15/0093 , C07C209/88 , C07C2101/14
摘要： Disclosed is cis-oxalato(trans-1-1,2-cyclohexanediamine) Pt(II) complex having high optical purity and no toxicity and exhibiting anticancer performance, as shown in the below Formula.Cis-oxalato(trans-1-1,2-cyclohexanediamine) Pt(II) complex of the invention possesses high optical purity or 99.94% or more e.e. and a melting point of 198.3.degree. to 199.7.degree. C. The complex is synthesized employing as starting material trans-1-1,2-cyclohexamediamine or a derivative of the trans-1-1,2-cyclohexanediamine optically resoluted by means of a high performance liquid chromatography. ##STR1##
摘要翻译： 公开了具有高光学纯度并且没有毒性并具有抗癌性能的顺式 - 草酸（反式 - 1-1,2-环己烷二胺）Pt（II）络合物，如下式所示。 本发明的顺式（反式 - 1-1,2-环己烷二胺）Pt（II）络合物具有高光学纯度或99.94％或更高e.e。 熔点为198.3℃〜199.7℃。使用反式-1-1,2-环己二胺作为起始原料合成络合物，或通过高分子光学测定反式-1-1,2-环己二胺的衍生物 高效液相色谱。
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5.发明授权Cis oxalato (trans 1-1,2-cyclohexanediamine) PT(II) having optically high purity 失效具有光学高纯度的草酸（反式1-1,2-环己烷二胺）PT（II）
公开(公告)号：US5338874A
公开(公告)日：1994-08-16
申请号：US43901
申请日：1993-04-07
申请人： Chihiro Nakanishi , Yuko Ohnishi , Junji Ohnishi , Junichi Taniuchi , Koji Okamoto , Takeshi Tozawa
发明人： Chihiro Nakanishi , Yuko Ohnishi , Junji Ohnishi , Junichi Taniuchi , Koji Okamoto , Takeshi Tozawa
IPC分类号： A61K31/28 , A61K31/282 , A61K33/24 , A61P35/00 , C07F15/00
CPC分类号： C07F15/0093
摘要： Disclosed herein is cis-oxalato (trans-1-1,2-cyclohexanediamine) Pt(II) optically high purity. Because of its complete optical purity, the compound is effective as raw material of such a medicine as a carcinostatic agent. The complete optical purity of the above compound may be proved by comparing the respective melting points of the cis-oxalato (trans-1-1,2-cyclohexanediamine).
摘要翻译： 本文公开了光学上高纯度的顺式 - 草酸（反式 - 1-1,2-环己烷二胺）Pt（II）。 由于其完全的光学纯度，该化合物作为制剂的药物的原料是有效的。 上述化合物的完全光学纯度可以通过比较顺式 - 草酸（反式 - 1-1,2-环己烷二胺）的相应熔点来证明。
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6.发明授权
公开(公告)号：US5298642A
公开(公告)日：1994-03-29
申请号：US43577
申请日：1993-04-07
申请人： Takeshi Tozawa , Yasunobu Komoda , Junji Ohnishi , Yukie Masuda , Junichi Taniuchi , Chihiro Nakanishi , Koji Okamoto
发明人： Takeshi Tozawa , Yasunobu Komoda , Junji Ohnishi , Yukie Masuda , Junichi Taniuchi , Chihiro Nakanishi , Koji Okamoto
IPC分类号： B01D15/08 , B01J20/281 , B01J20/291 , C01G55/00 , C07B57/00 , C07F15/00 , G01N30/88
CPC分类号： C07F15/0093
摘要： Disclosed herein is a process of optically resoluting optically active platinum complex compounds which comprises optically resoluting a d-isomer and an 1-isomer of a cis-Pt(II) complex of a 1,2-cyclohexanediamine isomer characterized in that the mixture of the d-isomer and the 1-isomer is optically resoluted by means of high performance liquid chromatography employing a column packed with a chiral filler.The chiral filler include, for example, a cellulose ester derivative, a cellulose carbamate derivative, an amylose carbamate derivative, a polymethacryl acid ester and .beta.- and .gamma.-cyclodextrin.According to the present invention, the optical resolution of a platinum complex compound essentially consisting of the mixture of two optical isomers which cannot be resoluted in accordance with a normal resolution method due to the small structural difference can be easily performed utilizing the characteristics of a chiral filler.
摘要翻译： 本文公开了一种光学拆分光学活性铂络合物的方法，其包括旋光拆分1,2-环己烷二胺异构体的顺式-PP（II）络合物的D-异构体和1-异构体，其特征在于， 通过使用填充有手性填料的柱的高效液相色谱法将1-异构体旋光。 手性填料包括例如纤维素酯衍生物，氨基甲酸纤维素衍生物，直链淀粉氨基甲酸酯衍生物，聚甲基丙烯酸酯和（β） - 和（γ） - 环糊精。 根据本发明，可以容易地利用手性的特征，轻易地进行基本上由两种光学异构体的混合物组成的铂配位化合物的光学拆分，所述两种光学异构体由于结构差异小而根据正常分辨率不能解决 填料。
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公开(公告)号：US08109497B2
公开(公告)日：2012-02-07
申请号：US12385836
申请日：2009-04-21
申请人： Koji Okamoto , Ken Obikane , Jun Kondo
发明人： Koji Okamoto , Ken Obikane , Jun Kondo
IPC分类号： B65H37/04
CPC分类号： B65H37/04 , B65H45/18 , B65H45/28 , B65H2801/27 , G03G15/6544 , G03G2215/00831
摘要： A sheet post-processing apparatus includes a cutting device for cutting a fore-edge portion of a center-folded bunch of sheets disposed in a position spaced from a sheet discharge outlet to eliminate the risk for inflicting a wound on the body of an operator, an end binding device for gathering sheets received from a carry-in entrance and performing binding processing in the end portion of a bunch of sheets, a saddle-stitching device for gathering sheets received from the carry-in entrance and performing binding processing in the center portion of a bunch of sheets, and a center-folding device for performing center-folding processing on the bunch of sheets subjected to the saddle-stitching processing. A cutting device is subjected to the center-folding processing. A second discharge outlet is disposed in the other side face of the apparatus frame to discharge the bunch of sheets subjected to the center-folding processing in the center-folding device.
摘要翻译： 片材后处理装置包括切割装置，用于切割布置在与片材排出口间隔开的位置的中心折叠的片材的前边缘部分，以消除在操作者的身体上造成伤口的风险， 用于收集从携带入口接收的纸张的端部装订装置，并且在一堆纸张的端部执行装订处理;鞍形装订装置，用于收集从进入入口接收的纸张并在中心执行装订处理 一束片材的一部分，以及用于对经过马鞍缝合处理的一束片材进行中心折叠处理的中心折叠装置。 切割装置经受中心折叠处理。 第二排出口设置在装置框架的另一侧面中，以将经过中心折叠处理的一束纸张排放到中心折叠装置中。
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公开(公告)号：US20110314344A1
公开(公告)日：2011-12-22
申请号：US12816987
申请日：2010-06-16
申请人： Koji Okamoto , Ben Maxson
发明人： Koji Okamoto , Ben Maxson
摘要： A test device is disclosed having a display and a graphical user interface (GUI) that provides guidance to a user by displaying first and second icons for representing first and second actions to be taken by the test device upon selecting the first and the second icons, respectively, by the user. To provide the guidance to the user, the second icon has graphical features indicative of the current status of the first action. For cases where the first action is a test that failed, the second action is highlighted thereby guiding the user to take the second action in response to the failed test. At least one of the graphical features of the second icon is indicative of whether the second icon is currently selectable by the user.
摘要翻译： 公开了一种具有显示器和图形用户界面（GUI）的测试装置，其通过在选择第一和第二图标时显示用于表示测试装置要采取的第一和第二动作的第一和第二图标来向用户提供指导， 分别由用户。 为了向用户提供指导，第二图标具有指示第一动作的当前状态的图形特征。 对于第一个操作是失败测试的情况，第二个操作被突出显示，从而指导用户采取第二个动作来响应失败的测试。 第二图标的至少一个图形特征指示用户当前是否可选择第二图标。
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公开(公告)号：US07980084B2
公开(公告)日：2011-07-19
申请号：US11975066
申请日：2007-10-17
申请人： Koji Okamoto , Masanobu Kimura
发明人： Koji Okamoto , Masanobu Kimura
IPC分类号： F25B21/02
CPC分类号： F25B21/02 , F25B2321/021 , G05D23/1919
摘要： A temperature control apparatus is provided which controls temperature of a control target disposed on the side of an A-side of a Peltier device. The apparatus includes a temperature regulator which performs regulating operation on temperature of a B-side of the Peltier device opposite to the A-side on the basis of a drive voltage for the Peltier device.
摘要翻译： 设置有控制设置在珀耳帖装置的A侧的控制对象的温度的温度控制装置。 该装置包括温度调节器，其基于珀尔帖装置的驱动电压对与珀耳帖装置相对的A侧的B侧的温度进行调节操作。
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公开(公告)号：US20090261521A1
公开(公告)日：2009-10-22
申请号：US12385836
申请日：2009-04-21
申请人： Koji Okamoto , Ken Obikane , Jun Kondo
发明人： Koji Okamoto , Ken Obikane , Jun Kondo
IPC分类号： B41L43/12
CPC分类号： B65H37/04 , B65H45/18 , B65H45/28 , B65H2801/27 , G03G15/6544 , G03G2215/00831
摘要： To provide a sheet post-processing apparatus where a cutting means for cutting a fore-edge portion of a center-folded bunch of sheets is disposed in a position spaced from a sheet discharge outlet in an apparatus frame to eliminate the risk for inflicting a wound on the body such as the finger, hand and the like of an operator, provided are an end binding means (31) for gathering sheets received from a carry-in entrance (23a) in a bunch form and performing binding processing in the end portion of a bunch of sheets, saddle-stitching means (40) for gathering sheets received from the carry-in entrance in a bunch form and performing binding processing in the center portion of a bunch of sheets, center-folding means for performing center-folding processing on the bunch of sheets subjected to the saddle-stitching processing, cutting means for cutting a fore edge of the bunch of sheets subjected to the center-folding processing, and a second discharge outlet (22x) disposed in the other side face of the apparatus frame to discharge the bunch of sheets subjected to the center-folding processing in the center-folding means, where the saddle-stitching means and the center-folding means are disposed below the carry-in entrance on the side of the one side face of the apparatus frame.
摘要翻译： 为了提供一种片材后处理装置，其中用于切割中心折叠的片状片材的前边缘部分的切割装置设置在与装置框架中的片材排出口间隔开的位置以消除造成伤口的风险 在操作者的手指，手等身体上设置有用于收集从堆放式入口（23a）接收的纸张的端部装订装置（31），并在端部进行装订处理 一束鞍形装订装置，用于收集从堆垛入口接收的纸张，并在一堆纸张的中心部分进行装订处理，中心折叠装置用于执行中心折叠 在经过鞍式拼接处理的纸张束上进行处理，切割经过中心折叠处理的纸张束的前端的切割装置和设置在另一侧的第二排出口（22x） 该装置框架用于将经过中心折叠处理的一束纸张排放在中心折叠装置中，其中鞍形装订装置和中心折叠装置设置在 设备框架的一个侧面。
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