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    Process of optically resoluting optically active platinum complex compound
    1.
    发明授权
    Process of optically resoluting optically active platinum complex compound 失效
    旋光光学活性铂络合物的光学拆分方法

    公开(公告)号：US5298642A

    公开(公告)日：1994-03-29

    申请号：US43577

    申请日：1993-04-07

    申请人： Takeshi Tozawa ,  Yasunobu Komoda ,  Junji Ohnishi ,  Yukie Masuda ,  Junichi Taniuchi ,  Chihiro Nakanishi ,  Koji Okamoto

    发明人： Takeshi Tozawa ,  Yasunobu Komoda ,  Junji Ohnishi ,  Yukie Masuda ,  Junichi Taniuchi ,  Chihiro Nakanishi ,  Koji Okamoto

    IPC分类号： B01D15/08 ,  B01J20/281 ,  B01J20/291 ,  C01G55/00 ,  C07B57/00 ,  C07F15/00 ,  G01N30/88

    CPC分类号： C07F15/0093

    摘要： Disclosed herein is a process of optically resoluting optically active platinum complex compounds which comprises optically resoluting a d-isomer and an 1-isomer of a cis-Pt(II) complex of a 1,2-cyclohexanediamine isomer characterized in that the mixture of the d-isomer and the 1-isomer is optically resoluted by means of high performance liquid chromatography employing a column packed with a chiral filler.The chiral filler include, for example, a cellulose ester derivative, a cellulose carbamate derivative, an amylose carbamate derivative, a polymethacryl acid ester and .beta.- and .gamma.-cyclodextrin.According to the present invention, the optical resolution of a platinum complex compound essentially consisting of the mixture of two optical isomers which cannot be resoluted in accordance with a normal resolution method due to the small structural difference can be easily performed utilizing the characteristics of a chiral filler.

    摘要翻译： 本文公开了一种光学拆分光学活性铂络合物的方法，其包括旋光拆分1,2-环己烷二胺异构体的顺式-PP（II）络合物的D-异构体和1-异构体，其特征在于， 通过使用填充有手性填料的柱的高效液相色谱法将1-异构体旋光。 手性填料包括例如纤维素酯衍生物，氨基甲酸纤维素衍生物，直链淀粉氨基甲酸酯衍生物，聚甲基丙烯酸酯和（β） - 和（γ） - 环糊精。 根据本发明，可以容易地利用手性的特征，轻易地进行基本上由两种光学异构体的混合物组成的铂配位化合物的光学拆分，所述两种光学异构体由于结构差异小而根据正常分辨率不能解决 填料。

    Method for producing gold colloid and gold colloid
    4.
    发明授权
    Method for producing gold colloid and gold colloid 有权
    金胶体和金胶体的生产方法

    公开(公告)号：US08048193B2

    公开(公告)日：2011-11-01

    申请号：US12298313

    申请日：2007-05-29

    申请人： Junichi Taniuchi ,  Hirofumi Nakagawa ,  Koji Okamoto

    发明人： Junichi Taniuchi ,  Hirofumi Nakagawa ,  Koji Okamoto

    IPC分类号： B22F9/24

    CPC分类号： B01J13/0043 ,  B22F1/0022 ,  B22F9/24 ,  B82Y30/00 ,  Y10S977/896

    摘要： It is an object of the present invention to provide a method for producing gold colloid having a targeted particle size, a sharp particle size distribution and a uniform and perfect spherical shape. The present invention relates to a method for producing gold colloid including a nucleation step of forming nuclear colloidal particles by adding a first reducing agent to a first gold salt solution; and a growth step of growing nuclear colloid by adding a second gold salt and a second reducing agent to the solution of the nuclear colloidal particles, characterized in that the growth step is performed at least once; a citrate is used as the first reducing agent and an ascorbate is used as the second reducing agent; and the addition of the ascorbate in the growth step is performed simultaneously with addition of the second gold salt. According to the method for producing gold colloid of the present invention, gold colloid having a sharp particle size distribution and a uniform and perfect spherical shape can be obtained.

    摘要翻译： 本发明的目的是提供一种具有目标粒度，尖锐的粒度分布和均匀且完美的球形形状的金胶体的制造方法。 本发明涉及一种生产金胶体的方法，包括通过向第一金盐溶液中加入第一还原剂形成核胶体颗粒的成核步骤; 以及通过向核胶体粒子的溶液中添加第二金盐和第二还原剂来生长核胶体的生长步骤，其特征在于，所述生长步骤至少进行一次; 使用柠檬酸盐作为第一还原剂，使用抗坏血酸作为第二还原剂; 并且在添加第二金盐的同时进行生长步骤中的抗坏血酸盐的添加。 根据本发明的金胶体的制造方法，可以获得具有尖锐的粒度分布和均匀且完美的球形的金胶体。

    PROCESS FOR PRODUCTION OF COLLOIDAL GOLD AND COLLOIDAL GOLD
    5.
    发明申请
    PROCESS FOR PRODUCTION OF COLLOIDAL GOLD AND COLLOIDAL GOLD 有权
    生产胶体金和胶体金的方法

    公开(公告)号：US20100159471A1

    公开(公告)日：2010-06-24

    申请号：US12298313

    申请日：2007-05-29

    申请人： Junichi Taniuchi ,  Hirofumi Nakagawa ,  Koji Okamoto

    发明人： Junichi Taniuchi ,  Hirofumi Nakagawa ,  Koji Okamoto

    IPC分类号： G01N33/553

    CPC分类号： B01J13/0043 ,  B22F1/0022 ,  B22F9/24 ,  B82Y30/00 ,  Y10S977/896

    摘要： It is an object of the present invention to provide a method for producing gold colloid having a targeted particle size, a sharp particle size distribution and a uniform and perfect spherical shape. The present invention relates to a method for producing gold colloid including a nucleation step of forming nuclear colloidal particles by adding a first reducing agent to a first gold salt solution; and a growth step of growing nuclear colloid by adding a second gold salt and a second reducing agent to the solution of the nuclear colloidal particles, characterized in that the growth step is performed at least once; a citrate is used as the first reducing agent and an ascorbate is used as the second reducing agent; and the addition of the ascorbate in the growth step is performed simultaneously with addition of the second gold salt. According to the method for producing gold colloid of the present invention, gold colloid having a sharp particle size distribution and a uniform and perfect spherical shape can be obtained.

    摘要翻译： 本发明的目的是提供一种具有目标粒度，尖锐的粒度分布和均匀且完美的球形形状的金胶体的制造方法。 本发明涉及一种生产金胶体的方法，包括通过向第一金盐溶液中加入第一还原剂形成核胶体颗粒的成核步骤; 以及通过向核胶体粒子的溶液中添加第二金盐和第二还原剂来生长核胶体的生长步骤，其特征在于，所述生长步骤至少进行一次; 使用柠檬酸盐作为第一还原剂，使用抗坏血酸作为第二还原剂; 并且在添加第二金盐的同时进行生长步骤中的抗坏血酸盐的添加。 根据本发明的金胶体的制造方法，可以获得具有尖锐的粒度分布和均匀且完美的球形的金胶体。

    CVD material compound and method for manufacturing the same and CVD method of ruthenium or ruthenium compound thin film
    6.
    发明授权
    CVD material compound and method for manufacturing the same and CVD method of ruthenium or ruthenium compound thin film 失效
    CVD材料化合物及其制造方法以及钌或钌化合物薄膜的CVD法

    公开(公告)号：US06555701B2

    公开(公告)日：2003-04-29

    申请号：US10175873

    申请日：2002-06-21

    申请人： Masayuki Saito ,  Junichi Taniuchi ,  Koji Okamoto ,  Hiroaki Suzuki

    发明人： Masayuki Saito ,  Junichi Taniuchi ,  Koji Okamoto ,  Hiroaki Suzuki

    IPC分类号： C07F1500

    CPC分类号： C07C49/92 ,  C23C16/18 ,  H01L28/65

    摘要： The present invention provides a CVD material compound based on an organic ruthenium compound, the organic ruthenium compound consisting of one of cis and trans isomers of tris (2,4-octa-dionato) ruthenium (III). The organic ruthenium compound which consists of cis or trans isomer can be isolated by the steps of preparing tris (2,4-octa-dionato) ruthenium (III) in any method, making the tris (2,4-octa-dionato) ruthenium (III) adsorbed on an adsorbent including alumina, bringing the adsorbent into contact with a first solvent to elute the trans isomer and then bringing the adsorbent into contact with a second solvent having a polarity higher than that of the first solvent to elute the cis isomer.

    摘要翻译： 本发明提供一种基于有机钌化合物的CVD材料化合物，由三（2,4-octa-dionato）钌（III）的顺式和反式异构体之一组成的有机钌化合物。 由顺式或反式异构体组成的有机钌化合物可以通过以任何方法制备三（2,4-辛二醛）钌（III）的步骤来分离，制备三（2,4-辛二醛）钌 （III）吸附在包含氧化铝的吸附剂上，使吸附剂与第一溶剂接触以洗脱反式异构体，然后使吸附剂与极性高于第一溶剂的第二溶剂接触以洗脱顺式异构体 。

    Organoruthenium compound for chemical vapor deposition raw material and production method for the organoruthenium compound
    7.
    发明授权
    Organoruthenium compound for chemical vapor deposition raw material and production method for the organoruthenium compound 有权
    用于化学气相沉积原料的有机钌化合物和有机钌化合物的制备方法

    公开(公告)号：US09290841B2

    公开(公告)日：2016-03-22

    申请号：US14007763

    申请日：2012-07-24

    申请人： Masayuki Saito ,  Junichi Taniuchi ,  Hirofumi Nakagawa

    发明人： Masayuki Saito ,  Junichi Taniuchi ,  Hirofumi Nakagawa

    IPC分类号： C07F15/00 ,  C23C16/00 ,  C23C16/16 ,  C23C16/30 ,  H01L21/285

    CPC分类号： C23C16/16 ,  C07F15/0046 ,  C23C16/30 ,  H01L21/28556

    摘要： The present invention is an organoruthenium compound for a chemical vapor deposition raw material, including dodecacarbonyl triruthenium represented by the following chemical formula, wherein the iron (Fe) concentration is 1 ppm or less. The DCR in the present invention can be produced by obtaining crude DCR by directly carbonylating ruthenium through allowing a ruthenium salt and carbon monoxide to react with each other and by purifying the crude DCR by a sublimation method. In the synthesis step, the concentration of Fe in the obtained crude DCR is preferably set at 10 ppm or less.

    摘要翻译： 本发明是用于化学气相沉积原料的有机钌化合物，其包括由以下化学式表示的十二羰基三钌，其中铁（Fe）浓度为1ppm以下。 本发明中的DCR可以通过使钌盐和一氧化碳相互反应并通过升华法纯化粗制DCR，通过直接羰基化钌来获得粗制DCR来制备。 在合成步骤中，所得到的粗制DCR中的Fe浓度优选为10ppm以下。

    Hydrogen Combustion Catalyst and Method for Producing Thereof, and Method For Combusting Hydrogen
    9.
    发明申请
    Hydrogen Combustion Catalyst and Method for Producing Thereof, and Method For Combusting Hydrogen 有权
    氢燃烧催化剂及其生产方法，以及用于燃烧氢的方法

    公开(公告)号：US20120263636A1

    公开(公告)日：2012-10-18

    申请号：US13518976

    申请日：2011-01-07

    申请人： Hirosi Noguchi ,  Junichi Taniuchi ,  Hitoshi Kubo ,  Yasunori Iwai ,  Katsumi Sato

    发明人： Hirosi Noguchi ,  Junichi Taniuchi ,  Hitoshi Kubo ,  Yasunori Iwai ,  Katsumi Sato

    IPC分类号： B01D53/46 ,  B01J31/02

    CPC分类号： G21B1/115 ,  B01J21/08 ,  B01J23/42 ,  B01J31/0274 ,  B01J33/00 ,  B01J37/0203 ,  B01J37/0207 ,  B01J37/0209 ,  C01B5/00 ,  Y02E60/324

    摘要： The present invention is a hydrogen combustion catalyst including a catalyst metal supported on a carrier composed of an inorganic oxide, wherein a functional group having at the end thereof at least an alkyl group having three or less carbon atoms is bonded by substitution to each of a certain fraction or the whole of the hydroxyl groups on the surface of the carrier. The functional group bonded to each of a certain fraction or the whole of the hydroxyl groups on the surface of the carrier is preferably an organic silane. The hydrogen combustion catalyst according to the present invention is capable of maintaining the activity thereof even when a hydrogen-containing gas, a treatment object, contains a water content equal to or less than the saturated water vapor content and the reaction temperature is set at or around room temperature, namely, at 0 to 40° C.

    摘要翻译： 本发明是一种氢燃烧催化剂，其包含负载在由无机氧化物构成的载体上的催化剂金属，其中末端至少具有3个以下碳原子的烷基的官能团通过取代键接至 载体表面上的某些部分或全部羟基。 与载体表面上的某一部分或全部羟基键合的官能团优选为有机硅烷。 本发明的氢燃烧催化剂即使在含氢气体，处理对象物含有等于或小于饱和水蒸汽含量的水含量并且反应温度设定在或等于或等于或等于 在室温附近，即在0至40℃

    ORGANORUTHENIUM COMPOUND FOR USE IN CHEMICAL VAPOR DEPOSITION AND CHEMICAL VAPOR DEPOSITION USING THE SAME
    10.
    发明申请
    ORGANORUTHENIUM COMPOUND FOR USE IN CHEMICAL VAPOR DEPOSITION AND CHEMICAL VAPOR DEPOSITION USING THE SAME 有权
    化学气相沉积中使用的有机金属化合物和使用该化合物的化学气相沉积

    公开(公告)号：US20110268878A1

    公开(公告)日：2011-11-03

    申请号：US13182720

    申请日：2011-07-14

    申请人： Junichi Taniuchi ,  Masayuki Saito ,  Minoru Ishida

    发明人： Junichi Taniuchi ,  Masayuki Saito ,  Minoru Ishida

    IPC分类号： C23C16/18

    CPC分类号： C07F15/0046 ,  C07F17/02 ,  C23C16/18 ,  H01L21/28556

    摘要： The present invention is an organoruthenium compound for use in production of a ruthenium or ruthenium compound thin film by chemical vapor deposition, including ruthenium and an arene group and norbornadiene both coordinated to the ruthenium and represented by the following formula. The present invention is an organoruthenium compound for use in chemical vapor deposition which does not require the coexistence of oxygen during the thin film formation, and moreover, is liquid at ordinary temperature, thereby having good handleability and recyclability. wherein the substituents, R1 to R6, of the arene group are each hydrogen or an alkyl group, and the total number of carbons of R1 to R6 (R1+R2+R3+R4+R5+R6) is 6 or less.

    摘要翻译： 本发明是用于通过化学气相沉积制造钌或钌化合物薄膜的有机钌化合物，包括钌和芳族基团和降冰片二烯，二者均与钌配位并由下式表示。 本发明是用于化学气相沉积的有机钌化合物，其在薄膜形成期间不需要氧的共存，而且在常温下为液体，因此具有良好的可操作性和可回收性。 其中芳基的取代基R 1〜R 6各自为氢或烷基，R 1〜R 6（R 1 + R 2 + R 3 + R 4 + R 5 + R 6）的碳原子数为6以下。