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    Epoxy interpenetrating polymer networks having internetwork chemical bonds
    1.
    发明授权
    Epoxy interpenetrating polymer networks having internetwork chemical bonds 失效
    具有互联网络化学键的环氧互穿聚合物网络

    公开(公告)号：US5360877A

    公开(公告)日：1994-11-01

    申请号：US61395

    申请日：1993-05-13

    申请人： Jyi-Faa Hwang ,  John P. Dismukes

    发明人： Jyi-Faa Hwang ,  John P. Dismukes

    IPC分类号： C08G59/14 ,  C08G59/20 ,  C08G59/22 ,  C08G59/24 ,  C08G59/28 ,  C08G59/30 ,  C08G59/50 ,  C08L63/00 ,  G08G59/22

    CPC分类号： C08G59/28 ,  C08G59/22 ,  C08G59/30 ,  C08G59/50 ,  C08L63/00 ,  Y10S525/903

    摘要： Epoxy interpenetrating polymer networks having chemical bonds between the interpenetrating networks are prepared from a first and a second polymer network, at least one of which contains an EPRXE resin; a resin having two epoxide functionalities represented by E and a reactive pendant nonepoxide functionality X. The two resin networks are sequentially crosslinked followed by activation of the pendant functionality of the EPRXE resin to form internetwork chemical bonds between the two resin networks affording an epoxy resin with both increased strength and toughness. The invention is also directed to the process of making interpenetrating polymer networks.

    摘要翻译： 在互穿网络之间具有化学键的环氧互穿聚合物网络由第一和第二聚合物网络制备，其中至少一个含有EPRXE树脂; 具有由E表示的两个环氧官能度和反应性侧链非环氧官能度X的树脂。两个树脂网络依次交联，随后激活EPRXE树脂的侧链官能团，以在两个树脂网络之间形成互连网络化学键，从而提供环氧树脂与 增加强度和韧性。 本发明还涉及制备互穿聚合物网络的方法。

    Fullerene-polymer compositions
    2.
    发明授权
    Fullerene-polymer compositions 失效
    富勒烯聚合物组合物

    公开(公告)号：US5281653A

    公开(公告)日：1994-01-25

    申请号：US797525

    申请日：1991-11-25

    申请人： Hans Thomann ,  Patrick Brant ,  John P. Dismukes ,  David J. Lohse ,  Jyi-Faa Hwang ,  Edward N. Kresge

    发明人： Hans Thomann ,  Patrick Brant ,  John P. Dismukes ,  David J. Lohse ,  Jyi-Faa Hwang ,  Edward N. Kresge

    IPC分类号： C08K3/02 ,  C08K3/04 ,  C08L101/00 ,  C08K5/01

    CPC分类号： C08K3/04 ,  Y10S977/753

    摘要： The present invention relates to novel compositions of matter comprising fullerenes and polymers, wherein the fullerenes are combined with the polymer in an amount sufficient to result in a change or modification in the viscoelastic properties of the resulting composition from that of the unmodified polymer typically within the range of from about 0.01 wt. % to about 85 wt. %. Also included in the present invention is the process for making the novel fullerene-polymer compositions and the products produced by the process disclosed therein. The novel compositions show changes in the viscoelastic properties in comparison to the unmodified polymer, and hence, have utility in any application in which the unmodified polymer may be used, but wherein the application would benefit from the resulting change in the viscoelastic properties.

    摘要翻译： 本发明涉及包含富勒烯和聚合物的新型物质组合物，其中富勒烯与聚合物结合的量足以导致所得组合物的粘弹性性质与未改性聚合物的粘弹性性质的改变或改性， 范围为约0.01重量％ ％至约85重量％ ％。 本发明还包括制备新型富勒烯聚合物组合物和通过其中公开的方法制备的产品的方法。 与未改性的聚合物相比，该新型组合物显示出粘弹性性能的变化，因此在可以使用未改性聚合物的任何应用中具有实用性，但是其应用将受益于所得到的粘弹性质的变化。

    Synthesis of microporous ceramics
    3.
    发明授权
    Synthesis of microporous ceramics 失效
    微孔陶瓷的合成

    公开(公告)号：US5563212A

    公开(公告)日：1996-10-08

    申请号：US248291

    申请日：1994-05-24

    申请人： John P. Dismukes ,  Jack W. Johnson ,  Edward W. Corcoran, Jr. ,  Joseph Vallone

    发明人： John P. Dismukes ,  Jack W. Johnson ,  Edward W. Corcoran, Jr. ,  Joseph Vallone

    IPC分类号： C04B38/06 ,  C04B38/00 ,  C04B35/52

    CPC分类号： C04B38/0022

    摘要： The present invention provides for microporous ceramic materials having a surface area in excess of 50 m.sup.2 /gm and an open microporous cell structure wherein the micropores have a mean width of less than 20 Angstroms and wherein said microporous structure comprises a volume of greater than about 0.015 cm.sup.3 /gm of the ceramic. The invention also provides for a preceramic composite intermediate composition comprising a mixture of a ceramic precursor and finely divided particles comprising a non-silicon containing ceramic, carbon, or an inorganic compound having a decomposition temperature in excess of 400.degree. C., whose pyrolysis product in inert atmosphere or in an ammonia atmosphere at temperatures of up to less than about 1100.degree. C. gives rise to the microporous ceramics of the invention. Also provided is a process for the preparation of the microporous ceramics of the invention involving pyrolysis of the ceramic intermediate under controlled conditions of heating up to temperatures of less than 1100.degree. C. to form a microporous ceramic product.

    摘要翻译： 本发明提供了具有超过50m 2 / gm的表面积的微孔陶瓷材料和开孔的微孔孔结构，其中微孔具有小于20埃的平均宽度，并且其中所述微孔结构包括大于约0.015的体积 cm3 / gm的陶瓷。 本发明还提供一种预陶瓷复合中间体组合物，其包含陶瓷前体和包含非硅含量陶瓷，碳或分解温度超过400℃的无机化合物的细碎颗粒的混合物，其热分解产物 在惰性气氛中或在高达少于约1100℃的氨气氛中，产生本发明的微孔陶瓷。 还提供了制备本发明的微孔陶瓷的方法，其包括在加热至低于1100℃的温度的受控条件下陶瓷中间体的热解，以形成微孔陶瓷产品。

    Nanoporous ceramics with catalytic functionality
    4.
    发明授权
    Nanoporous ceramics with catalytic functionality 失效
    具有催化功能的纳米多孔陶瓷

    公开(公告)号：US5852088A

    公开(公告)日：1998-12-22

    申请号：US578084

    申请日：1995-12-27

    申请人： John P. Dismukes ,  Jack Wayne Johnson ,  John Stewart Bradley

    发明人： John P. Dismukes ,  Jack Wayne Johnson ,  John Stewart Bradley

    IPC分类号： B01J35/10 ,  C04B38/00 ,  C08K5/00

    CPC分类号： C04B38/0022 ,  B01J35/1014 ,  B01J35/1019 ,  B01J35/1038 ,  B01J35/1057 ,  C04B2111/00801 ,  C04B2111/0081

    摘要： The present invention provides for amorphous, nanoporous, catalytic metal-containing ceramic material having a surface area in excess of 70 m.sup.2 /gm and characterized by a high content of open microporous cell structure wherein the micropores have a mean width of less than 20 Angstroms and wherein said microporous structure comprises a volume of greater than about 0.03 cm.sup.3 /gm of the ceramic. The invention also provides for a preceramic composite intermediate composition comprising a mixture of a ceramic precursor and from about 0.5 up to about 65 wt % of an organometallic compound containing a metal of Group IB, II, III, IV, IV, V, VIB, VIIA or VIII of the Periodic Table, including rare earth metals, whose pyrolysis product in ammonia or an inert atmosphere at temperatures of up to less than about 1100.degree. C. gives rise to the nanoporous catalytic ceramics of the invention. Also provided is a process for the preparation of the nanoporous ceramics of the invention involving pyrolysis of the ceramic intermediate under controlled conditions of heating up to temperatures of less than about 1100.degree. C. to form a nanoporous ceramic product useful in catalytic and membrane separation processes.

    摘要翻译： 本发明提供了具有超过70m 2 / gm的表面积的无定形，纳米孔，催化含金属的陶瓷材料，其特征在于高含量的开孔微孔孔结构，其中微孔的平均宽度小于20埃， 其中所述微孔结构包括大于约0.03cm 3 / gm的陶瓷体积。 本发明还提供了一种预陶瓷复合中间体组合物，其包含陶瓷前体和约0.5至约65重量％的含有IB，II，III，IV，IV，V，VIB族金属的金属的有机金属化合物的混合物， 包括稀土金属的元素周期表VIIA或VIII，它们的热解产物在氨或惰性气氛中，温度高达约1100℃，产生本发明的纳米多孔催化陶瓷。 还提供了制备本发明的纳米多孔陶瓷的方法，其包括在加热到低于约1100℃的温度的受控条件下陶瓷中间体的热解，以形成可用于催化和膜分离过程的纳米多孔陶瓷产物 。

    Electrical steels and method for producing same
    6.
    发明授权
    Electrical steels and method for producing same 失效
    电工钢及其制造方法

    公开(公告)号：US5200145A

    公开(公告)日：1993-04-06

    申请号：US729246

    申请日：1991-07-12

    申请人： Richard C. Krutenat ,  Robert S. Barnard ,  John P. Dismukes ,  Bernard H. Kear ,  Horst Witzke

    发明人： Richard C. Krutenat ,  Robert S. Barnard ,  John P. Dismukes ,  Bernard H. Kear ,  Horst Witzke

    IPC分类号： C23C10/46

    CPC分类号： C23C10/46

    摘要： The present invention relates to a novel process for producing silicon and/or aluminum containing iron alloy product as well as the material produced from same in either sheet or bulk structure form for electromagnetic circuit application. The process entails modifying an iron feedstock containing less than about 2.5 wt % silicon, aluminum or a combination thereof. The process further consists of diffusion of silicon or silicon and aluminum or aluminum into an iron feedstock by a pack diffusion or a chemical vapor deposition method in which the iron feedstock is heated to a temperature at which diffusion occurs in the presence of a pack containing silicon and/or aluminum sources, a reducing agent, a catalyst, and a filler, or in the presence of a flowing gas stream containing a volatile silicon compound. The resulting iron alloy product, which has a silicon content in the range of 0.25%--7% silicon, and an aluminum content in the range of about 0%--4% aluminum, has favorable properties for motor and transformer applications.

    摘要翻译： 本发明涉及用于生产含硅和/或铝的铁合金产品的新方法以及用于电磁电路应用的以片或块结构形式制造的材料的材料。 该方法需要修饰含有小于约2.5重量％硅，铝或其组合的铁原料。 该方法还包括将硅或硅和铝或铝通过包装扩散或化学气相沉积方法扩散到铁原料中，其中将铁原料加热至在含硅包的存在下发生扩散的温度 和/或铝源，还原剂，催化剂和填料，或在含有挥发性硅化合物的流动气流的存在下。 所得到的铁含量在0.25％-7％硅中，铝含量在约0％-4％铝范围内的铁合金产品具有用于电动机和变压器应用的良好性能。

    Synthesis of preceramic polymer-stabilized metal colloids and their conversion to microporous ceramics
    7.
    发明授权
    Synthesis of preceramic polymer-stabilized metal colloids and their conversion to microporous ceramics 失效
    合成前陶瓷聚合物稳定金属胶体及其转化为微孔陶瓷

    公开(公告)号：US5952421A

    公开(公告)日：1999-09-14

    申请号：US579444

    申请日：1995-12-27

    申请人： John Stewart Bradley ,  Ernestine Williams Hill ,  John P. Dismukes ,  Paul James Tindall

    发明人： John Stewart Bradley ,  Ernestine Williams Hill ,  John P. Dismukes ,  Paul James Tindall

    IPC分类号： B01D71/02 ,  B01J37/08 ,  C04B38/00 ,  C08G77/06

    CPC分类号： B01D67/0072 ,  B01D67/0044 ,  B01D67/0067 ,  B01D71/02 ,  B01J37/082 ,  C04B38/0022 ,  B01D2323/08 ,  B01D2323/18 ,  B01D2325/02

    摘要： The present invention provides for microporous ceramic materials having a surface area in excess of 70 m.sup.2 /gm and an open microporous cell structure wherein the micropores have a mean width of less than 20 Angstroms and wherein said microporous structure comprises a volume of greater than about 0.03 cm.sup.3 /gm of the ceramic. The invention also provides for a preceramic composite intermediate composition comprising a mixture of a ceramic precursor and nanoscale size metallic particles, whose pyrolysis product in inert atmosphere or in an ammonia atmosphere at temperatures of up to less than about 1100.degree. C. gives rise to the microporous ceramics of the invention. Also provided is a process for the preparation of the microporous ceramics of the invention involving pyrolysis of the composite intermediate under controlled conditions of heating up to temperatures of less than about 1100.degree. C. to form a microporous ceramic product.

    摘要翻译： 本发明提供了具有超过70m 2 / gm的表面积的微孔陶瓷材料和一种开孔微孔孔结构，其中微孔具有小于20埃的平均宽度，其中所述微孔结构包括大于约0.03的体积 cm3 / gm的陶瓷。 本发明还提供了一种预陶瓷复合中间体组合物，其包含陶瓷前体和纳米尺寸金属颗粒的混合物，其在惰性气氛中或在氨气氛中的热解产物在高至少于约1100℃的温度下产生 本发明的微孔陶瓷。 还提供了一种制备本发明的微孔陶瓷的方法，包括在加热至少于约1100℃的温度的受控条件下复合中间体的热解，以形成微孔陶瓷产物。