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    Preparation of N-benzylamines
    5.
    发明授权
    Preparation of N-benzylamines 失效
    N-苄胺的制备

    公开(公告)号：US06476268B1

    公开(公告)日：2002-11-05

    申请号：US10106390

    申请日：2002-03-27

    申请人： Harald Winsel ,  Wolfgang Siegel ,  Michael Bartsch

    发明人： Harald Winsel ,  Wolfgang Siegel ,  Michael Bartsch

    IPC分类号： C07C20900

    CPC分类号： C07C213/02 ,  C07C209/52 ,  C07C249/02 ,  C07C211/27 ,  C07C217/58 ,  C07C251/24

    摘要： N-Benzylamines are prepared by a process in which (i) in a first step, a benzaldehyde is reacted with a primary amine to give the imine and (ii) in a second step, the imine is hydrogenated with hydrogen in the presence of a catalyst containing one or more metals of groups 8 to 10 of the Periodic Table of the Elements to give the N-benzylamine, wherein the iminization (i) is carried out in a water-miscible solvent and the resulting water of reaction is not removed, and the hydrogenation (ii) is carried out in the imine solution obtained in the iminization (i) and containing water of reaction.

    摘要翻译： N-苄胺通过以下方法制备，其中（i）在第一步中，苯甲醛与伯胺反应得到亚胺，和（ii）在第二步中，亚胺在氢气存在下用氢气氢化 含有元素周期表第8至10族的一种或多种金属的催化剂，得到N-苄胺，其中亚胺化（i）在水混溶性溶剂中进行，并且所得到的反应水不被除去， 并且氢化（ⅱ）在亚胺化（ⅰ）中得到的亚胺溶液中进行并含有反应水。

    PROCESS FOR PREPARING SOLUTIONS OF RADIATION-SENSITIVE, FREE-RADICALLY POLYMERIZABLE ORGANIC COMPOUNDS
    8.
    发明申请
    PROCESS FOR PREPARING SOLUTIONS OF RADIATION-SENSITIVE, FREE-RADICALLY POLYMERIZABLE ORGANIC COMPOUNDS 有权
    制备辐射敏感性，无机可聚合有机化合物溶液的方法

    公开(公告)号：US20120016079A1

    公开(公告)日：2012-01-19

    申请号：US13258899

    申请日：2010-03-30

    申请人： Verena Weiskopf ,  Franz Niklaus Windlin ,  Harald Winsel ,  Markus Ruckpaul ,  Dirk Wulff ,  Uwe Duesterwald ,  Ulrike Licht

    发明人： Verena Weiskopf ,  Franz Niklaus Windlin ,  Harald Winsel ,  Markus Ruckpaul ,  Dirk Wulff ,  Uwe Duesterwald ,  Ulrike Licht

    IPC分类号： C08F220/10 ,  C08K5/07 ,  C08F2/06

    CPC分类号： C08F220/06 ,  C07C68/02 ,  C08F212/08 ,  C08F212/12 ,  C08F2220/1825 ,  C09D133/08 ,  C09J133/08 ,  C09J2201/606 ,  C09J2201/61 ,  C07C69/96 ,  C08F2220/301

    摘要： A description is given of a process for preparing solutions of radiation-sensitive, free-radically polymerizable organic compounds, where a first starting compound, which has an acid halide group, and a second starting compound, which has an alcoholic hydroxyl group, are esterified with one another in a solvent or in a solvent mixture. The solvent comprises one or more ketones having a boiling point of below 150° C. under atmospheric pressure (1 bar), or the solvent mixture is composed to an extent of at least 50% by weight of said ketones. One of the two starting compounds has at least one radiation-sensitive group and the other of the two starting compounds has at least one ethylenically unsaturated, free-radically polymerizable group. A description is also given of corresponding solutions of radiation-sensitive, free-radically polymerizable organic compounds and of their use for preparing radiation-crosslinkable, free-radically copolymerized copolymers, more particularly for hotmelt pressure-sensitive adhesives or aqueous polymer dispersions.

    摘要翻译： 描述了制备具有卤化物基团的第一起始化合物和具有醇羟基的第二起始化合物的辐射敏感的可自由基聚合的有机化合物的溶液的方法，所述方法被酯化 彼此在溶剂或溶剂混合物中。 溶剂包含一种或多种在大气压（1巴）下沸点低于150℃的酮，或溶剂混合物的组成为所述酮的至少50重量％。 两种起始化合物中的一种具有至少一个辐射敏感性基团，并且两种起始化合物中的另一种具有至少一个烯键式不饱和的可自由基聚合的基团。 还给出了对辐射敏感的可自由基聚合的有机化合物的相应解决方案的描述，以及它们用于制备辐射可交联的自由基共聚共聚物的用途，更特别地用于热熔粘合剂或水性聚合物分散体。

    Process for preparing solutions of radiation-sensitive, free-radically polymerizable organic compounds
    9.
    发明授权
    Process for preparing solutions of radiation-sensitive, free-radically polymerizable organic compounds 有权
    制备辐射敏感的可自由基聚合的有机化合物的方法

    公开(公告)号：US08648212B2

    公开(公告)日：2014-02-11

    申请号：US13258899

    申请日：2010-03-30

    申请人： Verena Weiskopf ,  Franz Niklaus Windlin ,  Harald Winsel ,  Markus Ruckpaul ,  Dirk Wulff ,  Uwe Duesterwald ,  Ulrike Licht

    发明人： Verena Weiskopf ,  Franz Niklaus Windlin ,  Harald Winsel ,  Markus Ruckpaul ,  Dirk Wulff ,  Uwe Duesterwald ,  Ulrike Licht

    IPC分类号： C08F220/10 ,  C08K5/07 ,  C08F2/06

    CPC分类号： C08F220/06 ,  C07C68/02 ,  C08F212/08 ,  C08F212/12 ,  C08F2220/1825 ,  C09D133/08 ,  C09J133/08 ,  C09J2201/606 ,  C09J2201/61 ,  C07C69/96 ,  C08F2220/301

    摘要： A description is given of a process for preparing solutions of radiation-sensitive, free-radically polymerizable organic compounds, where a first starting compound, which has an acid halide group, and a second starting compound, which has an alcoholic hydroxyl group, are esterified with one another in a solvent or in a solvent mixture. The solvent comprises one or more ketones having a boiling point of below 150° C. under atmospheric pressure (1 bar), or the solvent mixture is composed to an extent of at least 50% by weight of said ketones. One of the two starting compounds has at least one radiation-sensitive group and the other of the two starting compounds has at least one ethylenically unsaturated, free-radically polymerizable group. A description is also given of corresponding solutions of radiation-sensitive, free-radically polymerizable organic compounds and of their use for preparing radiation-crosslinkable, free-radically copolymerized copolymers, more particularly for hotmelt pressure-sensitive adhesives or aqueous polymer dispersions.

    摘要翻译： 描述了制备具有卤化物基团的第一起始化合物和具有醇羟基的第二起始化合物的辐射敏感的可自由基聚合的有机化合物的溶液的方法，所述方法被酯化 彼此在溶剂或溶剂混合物中。 溶剂包含一种或多种在大气压（1巴）下沸点低于150℃的酮，或溶剂混合物的组成为所述酮的至少50重量％。 两种起始化合物中的一种具有至少一个辐射敏感性基团，并且两种起始化合物中的另一种具有至少一个烯键式不饱和的可自由基聚合的基团。 还给出了对辐射敏感的可自由基聚合的有机化合物的相应解决方案的描述，以及它们用于制备辐射可交联的自由基共聚共聚物的用途，更特别地用于热熔粘合剂或水性聚合物分散体。