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    Process and apparatus for reactive distillation with a particular distribution of liquid and vapour phases
    1.
    发明授权
    Process and apparatus for reactive distillation with a particular distribution of liquid and vapour phases 失效
    具有液相和汽相特定分布的反应蒸馏的方法和装置

    公开(公告)号：US5776320A

    公开(公告)日：1998-07-07

    申请号：US686101

    申请日：1996-07-24

    申请人： Marie-Claire Marion ,  Jean-Charles Viltard ,  Philippe Travers ,  Isabelle Harter ,  Alain Forestiere

    发明人： Marie-Claire Marion ,  Jean-Charles Viltard ,  Philippe Travers ,  Isabelle Harter ,  Alain Forestiere

    IPC分类号： B01D3/26 ,  B01D3/00 ,  B01J8/04 ,  B01J19/24 ,  C07C2/64 ,  C07C15/073 ,  C07C41/42 ,  C07C43/04 ,  C10G7/00 ,  B01D3/34

    CPC分类号： B01J8/0469 ,  B01D3/009 ,  B01J8/0492 ,  Y02P20/127

    摘要： The invention concerns a reactive distillation process carried out in a reactive distillation zone which includes at least one catalytic zone flanked by two distillation zones, the vapor from the distillation circulating from bottom to top so as to be in practically no contact with the catalyst, and the liquid circulating from the upper distillation zone (5) to a substantially central zone at the bottom of the catalytic zone without contacting the catalyst, then circulating radially below the catalytic zone via at least one means (20) so as to be introduced into a liquid distribution zone (23), then circulating through the catalytic bed (8) in the catalytic zone, following which the liquid is recovered via at least one liquid overflow means (19) in a lower distillation zone (14). The invention also concerns an apparatus for reactive distillation.

    摘要翻译： 本发明涉及在反应蒸馏区中进行的反应蒸馏方法，该反应蒸馏区包括至少一个侧面有两个蒸馏区的催化区，来自蒸馏的蒸气从底部到顶部循环，以便几乎不与催化剂接触，以及 所述液体从所述上部蒸馏区域（5）循环到所述催化区域的底部的基本中心区域，而不接触所述催化剂，然后经由至少一个装置（20）径向地在所述催化区域下方循环，以便被引入到 液体分配区（23），然后在催化区循环通过催化床（8），随后通过下蒸馏区（14）中的至少一个液体溢流装置（19）回收液体。 本发明还涉及用于反应蒸馏的装置。

    Process for producing a tertiary olefin by decomposing a tertiary alkyl ether
    2.
    发明授权
    Process for producing a tertiary olefin by decomposing a tertiary alkyl ether 失效
    通过分解叔烷基醚生产叔烯烃的方法

    公开(公告)号：US6100438A

    公开(公告)日：2000-08-08

    申请号：US26682

    申请日：1998-02-20

    申请人： Marie-Claire Marion ,  Vincent Coupard ,  Alain Forestiere ,  Philippe Travers ,  Jean-Charles Viltard

    发明人： Marie-Claire Marion ,  Vincent Coupard ,  Alain Forestiere ,  Philippe Travers ,  Jean-Charles Viltard

    IPC分类号： C07C1/20 ,  C07C11/02 ,  C07C1/00

    CPC分类号： C07C11/02 ,  C07C1/20 ,  C07C2531/025 ,  C07C2531/06

    摘要： A process for producing a tertiary olefin by decomposing a tertiary alkyl ether comprises a) decomposing at least one ether to a product containing an alcohol and a tertiary olefin, b) fractionating at least a portion of the product from a) in a fractionation zone (C1) to obtain the tertiary olefin and the alcohol, c) purifying at least a portion of the tertiary olefin obtained from step b) wherein said portion is sent to a water washing extraction zone (L1) from which a fraction (D) containing the tertiary olefin is recovered, and d) a step in which at least a portion of the fraction (D) from c) is sent to a separation zone (Co) from which a liquid aqueous fraction (Le) and a liquid hydrocarbon fraction (Lc) containing the major portion of the tertiary olefin are recovered.

    摘要翻译： 通过分解叔烷基醚来生产叔烯烃的方法包括：a）将至少一种醚分解成含有醇和叔烯烃的产物，b）在分馏区（a）中分馏至少一部分产物， C1）以获得叔烯烃和醇，c）纯化至少一部分由步骤b）获得的叔烯烃，其中所述部分被送至水洗提取区（L1），从其中含有 回收叔烯烃，d）将来自c）的馏分（D）的至少一部分送至分离区（Co）的步骤，液体含水馏分（Le）和液体烃馏分（Lc ）回收了主要部分的叔烯烃。

    Process for producing a tertiary olefin by decomposing a tertiary alkylether, comprising a first step of purification by washing with water
    3.
    发明授权
    Process for producing a tertiary olefin by decomposing a tertiary alkylether, comprising a first step of purification by washing with water 失效
    通过分解叔烷基醚生产叔烯烃的方法，包括通过用水洗涤来净化的第一步骤

    公开(公告)号：US6072095A

    公开(公告)日：2000-06-06

    申请号：US30916

    申请日：1998-02-26

    申请人： Marie-Claire Marion ,  Vincent Coupard ,  Alain Forestiere ,  Philippe Travers ,  Jean-Charles Viltard

    发明人： Marie-Claire Marion ,  Vincent Coupard ,  Alain Forestiere ,  Philippe Travers ,  Jean-Charles Viltard

    IPC分类号： C07C1/20 ,  C07C11/02 ,  C07C1/00

    CPC分类号： C07C11/02 ,  C07C1/20

    摘要： A process for producing a tertiary olefin by decomposing an ether comprises a) decomposing an ether to a product containing an alcohol and a tertiary olefin, b) purifying at least a portion of the product from a) in a water washing extraction zone (L1) to obtain an aqueous fraction (A1) containing the major portion of the alcohol and a fraction (B1) containing the major portion of the tertiary olefin, the fraction (B1) containing the tertiary olefin, water, possibly ether and light compounds and being substantially free of alcohol, and c) in which at least a portion of the fraction (B1) from b) is sent to a separation zone (Co1) from which a liquid aqueous fraction (La1) and a liquid fraction (Lb1) containing the major portion of the tertiary olefin, possibly ether and possibly light compounds, are recovered.

    摘要翻译： 通过分解醚制备叔烯烃的方法包括：a）将乙醚分解成含有醇和叔烯烃的产物，b）在水洗提取区（L1）中从a）中纯化至少一部分产物， 得到含有主要部分醇的含水馏分（A1）和含有主要部分的叔烯烃的馏分（B1），含有叔烯烃的馏分（B1），水，可能的醚和轻质化合物，并且基本上 不含醇，c）将来自b）的馏分（B1）的至少一部分送至分离区（Co1），分离区（Co1）从该分离区（Co1）中分出含有主要的液体含水馏分（La1）和液体馏分（Lb1） 回收了部分叔烯烃，可能是醚和可能的轻化合物。

    Process for producing an alpha olefin, a tertiary olefin and/or an ether from an unsaturated hydrocarbon cut
    4.
    发明授权
    Process for producing an alpha olefin, a tertiary olefin and/or an ether from an unsaturated hydrocarbon cut 失效
    从不饱和烃馏分制备α-烯烃，叔烯烃和/或醚的方法

    公开(公告)号：US5994594A

    公开(公告)日：1999-11-30

    申请号：US53061

    申请日：1998-04-01

    申请人： Marie-Claire Marion ,  Vincent Coupard ,  Alain Forestiere ,  Philippe Travers ,  Jean-Charles Viltard

    发明人： Marie-Claire Marion ,  Vincent Coupard ,  Alain Forestiere ,  Philippe Travers ,  Jean-Charles Viltard

    IPC分类号： C07C11/02 ,  C07C41/06 ,  C07C41/00 ,  C07C2/00 ,  C07C7/00 ,  C07C9/00

    CPC分类号： C07C11/02 ,  C07C41/06 ,  C07C41/42

    摘要： A process for producing an alpha olefin, a tertiary olefin or a tertiary alkyl ether from an unsaturated hydrocarbon cut containing at least one alpha olefin and at least one etherifiable tertiary olefin comprises synthesising at least one tertiary alkyl ether to obtain a product which is separated into a fraction (O1) which is depleted in ether and containing the alpha olefin and a fraction (E1) which is enriched in ether, followed by decomposition of at least a portion of the ether in fraction (E1) into a product (P1) containing at least one alcohol and at least one tertiary olefin, which is fractionated in a fractionation zone (C5) into a fraction (B1) containing the major portion of the tertiary olefin and a fraction (A1) containing the major portion of the alcohol.

    摘要翻译： 从含有至少一种α烯烃和至少一种可醚化叔烯烃的不饱和烃馏分中制备α-烯烃，叔烯烃或叔烷基醚的方法包括合成至少一种叔烷基醚以获得分离成 在乙醚中耗尽并含有α-烯烃的馏分（O1）和富含乙醚的馏分（E1），然后将部分（E1）中的至少一部分乙醚分解成含有 至少一种醇和至少一种叔烯烃，其在分馏区（C5）中分馏成含有主要部分的叔烯烃的级分（B1）和含有主要部分醇的级分（A1）。

    Reaction and distillation device
    7.
    发明授权
    Reaction and distillation device 失效
    反应和蒸馏装置

    公开(公告)号：US6159344A

    公开(公告)日：2000-12-12

    申请号：US900878

    申请日：1997-07-25

    申请人： Marie-Claire Marion ,  Alain Forestiere ,  Christophe Thille ,  Jean-Charles Viltard

    发明人： Marie-Claire Marion ,  Alain Forestiere ,  Christophe Thille ,  Jean-Charles Viltard

    IPC分类号： B01D3/00 ,  B01D3/14 ,  B01J8/02 ,  C07C41/06 ,  C07C41/42

    CPC分类号： B01J8/02 ,  B01D3/009 ,  B01D3/146 ,  C07C41/06 ,  C07C41/42 ,  B01J2208/00247 ,  Y02P20/127 ,  Y10S203/06 ,  Y10S203/20

    摘要： The invention relates to a distillation and reaction device having a reaction section and a distillation-reaction section. The distillation-reaction section has a distillation zone with at least one device for circulation of the effluent from the reaction section to the distillation zone. Effluent from the reaction section is circulated to the distillation zone. The distillation-reaction section also has at least one distillation-reaction zone having at least one catalyst bed. The distillation-reaction zone is distinct from the distillation zone and provides at least partly the reflux of the distillation zone. The distillation-reaction section can also have at least one complementary reaction zone containing at least one catalyst bed. The invention further relates to a process for preparing at least one aliphatic monoalcohol, generally in excess, and at least one olefin.

    摘要翻译： 本发明涉及具有反应段和蒸馏反应段的蒸馏和反应装置。 蒸馏反应段具有至少一个用于将流出物从反应段循环到蒸馏区的装置的蒸馏区。 来自反应段的流出物循环到蒸馏区。 蒸馏反应段还具有至少一个具有至少一个催化剂床的蒸馏反应区。 蒸馏反应区不同于蒸馏区，并且至少部分地提供蒸馏区的回流。 蒸馏反应部分还可以具有至少一个含有至少一个催化剂床的互补反应区。 本发明还涉及制备至少一种通常为过量的脂族一元醇和至少一种烯烃的方法。

    Reaction and distillation device and etherification process
    8.
    发明授权
    Reaction and distillation device and etherification process 有权
    反应和蒸馏装置和醚化过程

    公开(公告)号：US06472568B1

    公开(公告)日：2002-10-29

    申请号：US09657280

    申请日：2000-09-07

    申请人： Marie-Claire Marion ,  Alain Forestiere ,  Christophe Thille ,  Jean-Charles Viltard

    发明人： Marie-Claire Marion ,  Alain Forestiere ,  Christophe Thille ,  Jean-Charles Viltard

    IPC分类号： C07C4109

    CPC分类号： B01J8/02 ,  B01D3/009 ,  B01D3/146 ,  B01J2208/00247 ,  C07C41/06 ,  C07C41/42 ,  Y02P20/127 ,  Y10S203/06 ,  Y10S203/20 ,  C07C43/046

    摘要： The invention relates to a process for preparing at least one aliphatic monoalcohol, generally in excess, and at least one olefin. The process is performed in a distillation and reaction device having a reaction section and a distillation-reaction section. The distillation-reaction section has a distillation zone with at least one means for circulation of the effluent from the reaction section to the distillation zone. Effluent from the reaction section is circulated to the distillation zone. The distillation-reaction section also has at least one distillation-reaction zone having at least one catalyst bed. The distillation-reaction zone is distinct from the distillation zone and provides at least partly the reflux of the distillation zone. The distillation-reaction section can also have at least one complementary reaction zone containing at least one catalyst bed.

    摘要翻译： 本发明涉及制备至少一种通常为过量的脂族一元醇和至少一种烯烃的方法。 该方法在具有反应段和蒸馏反应段的蒸馏和反应装置中进行。 蒸馏反应段具有至少一种用于将流出物从反应段循环到蒸馏区的装置的蒸馏区。 来自反应段的流出物循环到蒸馏区。 蒸馏反应段还具有至少一个具有至少一个催化剂床的蒸馏反应区。 蒸馏反应区不同于蒸馏区，并且至少部分地提供蒸馏区的回流。 蒸馏反应部分还可以具有至少一个含有至少一个催化剂床的互补反应区。

    Process for the production of a diene in three successive stages from a tertiary alkyl ether
    10.
    发明授权
    Process for the production of a diene in three successive stages from a tertiary alkyl ether 有权
    从叔烷基醚三个阶段生产二烯的方法

    公开(公告)号：US06667423B2

    公开(公告)日：2003-12-23

    申请号：US09392571

    申请日：1999-09-09

    申请人： Claire Dumonteil ,  Alain Forestiere ,  Marie-Claire Marion

    发明人： Claire Dumonteil ,  Alain Forestiere ,  Marie-Claire Marion

    IPC分类号： C07C1207

    CPC分类号： C07C11/12 ,  C07C1/20 ,  C07C5/48 ,  C07C7/11 ,  C07C2523/04 ,  C07C2523/28 ,  C07C2523/30 ,  C07C2523/75 ,  C07C2523/755 ,  C07C2531/025 ,  C07C11/02

    摘要： For the production of a diene a process in three stages comprises a stage a) for decomposition of at least one tertiary alkyl ether in a mixture that contains at least one tertiary olefin, at least one alcohol and at least one residual ether, in the presence of a catalyst that comprises at least one mineral solid that is grafted by at least one organic group such as alkyl sulfonic acid, sulfonic aryl and/or sulfonic alkylaryl, a stage b) for purification of the olefin that is obtained in stage a), and a stage c) for oxidizing dehydrogenation of the tertiary olefin that is obtained in stage b) in the presence of a catalyst under conditions for obtaining a diene.

    摘要翻译： 对于二烯的生产，在三个阶段中的方法包括a）在含有至少一种叔烯烃，至少一种醇和至少一种残余醚的混合物中分解至少一种叔烷基醚，在存在 包含至少一种通过至少一种有机基团如烷基磺酸，磺酸芳基和/或磺酸烷基芳基接枝的矿物固体的催化剂，以及用于纯化在步骤a）中获得的烯烃的步骤b） 在阶段b）中在催化剂存在下，在获得二烯的条件下氧化脱氢的阶段c）。