Manufacture of target for use in magnetron sputtering of nickel and like magnetic metals for forming metallization films having consistent uniformity through life
    2.
    发明授权
    Manufacture of target for use in magnetron sputtering of nickel and like magnetic metals for forming metallization films having consistent uniformity through life 失效
    用于镍和类似磁性金属的磁控溅射的靶的制造,用于形成具有一致均匀性的金属化膜

    公开(公告)号:US06436207B1

    公开(公告)日:2002-08-20

    申请号:US09566657

    申请日:2000-05-08

    IPC分类号: C23C1435

    摘要: Improved targets for use in DC magnetron sputtering of nickel or like ferromagnetic face-centered cubic (FCC) metals are disclosed for forming metallization films having effective edge-to-edge deposition uniformity of 5% (3&sgr;) or better. Such targets may be characterized as having: (a) a homogeneous texture mix that is at least 20% of a texture content and less than 50% of a texture content, (b) an initial pass-through flux factor (%PTF) of about 30% or greater; and(c) a homogeneous grain size of about 200 &mgr;m or less.

    摘要翻译: 公开了用于形成具有5%(3σ)或更好的边缘到边缘沉积均匀性的金属化膜的镍或类似铁磁面心立方(FCC)金属的直流磁控溅射的改进目标。 这样的目标可以被表征为具有:(a)均匀纹理混合物,其具有至少20%的质感含量和小于50%的<111>质地含量,(b)初始直通通量 因子(%PTF)约30%以上; 和(c)约200μm或更小的均匀晶粒尺寸。

    Target for use in magnetron sputtering of nickel for forming metallization films having consistent uniformity through life
    3.
    发明授权
    Target for use in magnetron sputtering of nickel for forming metallization films having consistent uniformity through life 失效
    用于镍的磁控溅射的目标,用于形成具有一致均匀性的金属化膜

    公开(公告)号:US06521107B2

    公开(公告)日:2003-02-18

    申请号:US09823341

    申请日:2001-03-29

    IPC分类号: C23C1434

    摘要: Improved targets for use in DC magnetron sputtering of nickel or like ferromagnetic face-centered cubic (FCC) metals are disclosed for forming metallization films having effective edge-to-edge deposition uniformity of 5%(3&sgr;) or better. Such targets may be characterized as having: (a) a homogeneous texture mix that is at least 20% of a texture content and less than 50% of a texture content, (b) an initial pass-through flux factor (% PTF) of about 30% or greater; and(c) a homogeneous grain size of about 200 &mgr;m or less.

    摘要翻译: 公开了用于形成具有5%(3σ)或更好的边缘到边缘沉积均匀性的金属化膜的镍或类似铁磁面心立方(FCC)金属的直流磁控溅射的改进目标。 这样的目标可以被表征为具有:(a)均匀纹理混合物,其具有至少20%的质感含量和小于50%的<111>质地含量,(b)初始直通通量 因子(%PTF)约30%以上; 和(c)约200μm或更小的均匀晶粒尺寸。

    Target for use in magnetron sputtering of nickel for forming metallization films having consistent uniformity through life
    4.
    发明授权
    Target for use in magnetron sputtering of nickel for forming metallization films having consistent uniformity through life 有权
    用于镍的磁控溅射的目标,用于形成具有一致均匀性的金属化膜

    公开(公告)号:US06472867B1

    公开(公告)日:2002-10-29

    申请号:US09791967

    申请日:2001-02-21

    IPC分类号: G01N2772

    CPC分类号: C23C14/3414

    摘要: Improved targets for use in DC magnetron sputtering of nickel or like ferromagnetic face-centered cubic (FCC) metals are included for forming metallization films having effective edge-to-edge deposition uniformity of 5% (3&sgr;) or better. Such targets may be characterized as having: (a) a homogeneous texture mix that is at least 20% of a texture content and less than 50% of a texture content, (b) an initial pass-through flux factor (% PTF) of about 30% or greater; and(c) a homogeneous grain size of about 200 &mgr;m or less.

    摘要翻译: 包括用于镍或类似铁磁面心立方(FCC)金属的直流磁控溅射的改进目标,用于形成具有5%(3σ)或更好的边缘到边缘沉积均匀度的金属化膜。 这样的目标可以被表征为具有:(a)均匀纹理混合物,其具有至少20%的质感含量和小于50%的<111>质地含量,(b)初始直通通量 因子(%PTF)约30%以上; 和(c)约200μm或更小的均匀晶粒尺寸。

    Copper target for sputter deposition
    5.
    发明授权
    Copper target for sputter deposition 有权
    用于溅射沉积的铜靶

    公开(公告)号:US6139701A

    公开(公告)日:2000-10-31

    申请号:US272974

    申请日:1999-03-18

    CPC分类号: C23C14/3414

    摘要: A copper sputtering target is provided for producing copper films having reduced in-film defect densities. In addition to reducing dielectric inclusion content of the copper target material, the hardness of the copper target is maintained within a range greater than 45 Rockwell. Within this range defect generation from arc-induced mechanical failure is reduced. Preferably hardness is achieved by limiting grain size to less than 50 microns, and most preferably to less than 25 microns. The surface roughness preferably is limited to less than 20 micro inches, or more preferably, less than 5 micro inches to reduce defect generation from field-enhanced emission. This grain size range preferably is achieved by limiting the purity level of the copper target material to a level less than 99.9999%, preferably within a range between 99.995% to 99.9999%, while reducing particular impurity levels.

    摘要翻译: 提供一种铜溅射靶,用于制造薄膜缺陷密度降低的铜膜。 除了降低铜靶材料的电介质夹杂物含量外,铜靶的硬度保持在大于45的洛氏硬度范围内。 在此范围内,电弧引起的机械故障的缺陷产生减少。 优选地,通过将​​晶粒尺寸限制为小于50微米,最优选小于25微米来实现硬度。 表面粗糙度优选限于小于20微英寸,或更优选小于5微英寸,以减少场增强发射的缺陷产生。 该粒度范围优选通过将铜靶材料的纯度水平限制在小于99.9999%,优选在99.995%至99.9999%之间的范围内,同时降低特定杂质水平来实现。

    Target for use in magnetron sputtering of nickel for forming
metallization films having consistent uniformity through life
    6.
    发明授权
    Target for use in magnetron sputtering of nickel for forming metallization films having consistent uniformity through life 失效
    用于镍的磁控溅射的目标,用于形成具有一致均匀性的金属化膜

    公开(公告)号:US6086725A

    公开(公告)日:2000-07-11

    申请号:US54067

    申请日:1998-04-02

    IPC分类号: C23C14/34 C23C14/35 C23C14/54

    摘要: Improved targets for use in DC magnetron sputtering of nickel or like ferromagnetic face-centered cubic (FCC) metals are disclosed for forming metallization films having effective edge-to-edge deposition uniformity of 5%(3.sigma.) or better. Such targets may be characterized as having: (a) a homogeneous texture mix that is at least 20% of a texture content and less than 50% of a texture content, (b) an initial pass-through flux factor (% PTF) of about 30% or greater; and (c) a homogeneous grain size of about 200 .mu.m or less.

    摘要翻译: 公开了用于镍或类似铁磁面心立方(FCC)金属的直流磁控溅射的改进目标,用于形成具有5%(3西格玛)或更好的边缘到边缘沉积均匀度的金属化膜。 这样的目标可以被表征为具有:(a)均匀纹理混合物,其具有至少20%的质感含量和小于50%的<111>质地含量,(b)初始直通通量 因子(%PTF)约30%以上; 和(c)约200μm以下的均匀粒径。

    Continuous, non-agglomerated adhesion of a seed layer to a barrier layer
    8.
    发明授权
    Continuous, non-agglomerated adhesion of a seed layer to a barrier layer 有权
    种子层与阻挡层的连续的非团聚粘附

    公开(公告)号:US06627542B1

    公开(公告)日:2003-09-30

    申请号:US09604858

    申请日:2000-06-27

    IPC分类号: H01L2144

    摘要: A method and apparatus is provided for improving adherence of metal seed layers to barrier layers in electrochemical deposition techniques. The method includes depositing an adhesion layer continuously or semi-continuously without agglomeration onto a barrier layer prior to depositing a seed layer by controlling the substrate temperature, the chamber pressure, and/or the power delivered to a deposition chamber. Deposition of the adhesion layer prevents layer delamination which leads to agglomeration of the deposited layers and formation of voids in the high aspect ratio features.

    摘要翻译: 提供了一种用于在电化学沉积技术中改善金属种子层对阻挡层的粘附性的方法和装置。 该方法包括通过控制衬底温度,室压力和/或输送到沉积室的功率沉积种子层之前将粘附层连续地或半连续地沉积在阻挡层上。 粘附层的沉积防止了层析层,导致沉积层的聚集和高纵横比特征形成空隙。

    Method for manufacturing metal sputtering target for use in DC magnetron so that target has reduced number of conduction anomalies
    9.
    发明授权
    Method for manufacturing metal sputtering target for use in DC magnetron so that target has reduced number of conduction anomalies 有权
    用于制造用于直流磁控管的金属溅射靶的方法,使得目标具有减少的导通异常的数量

    公开(公告)号:US06228186B1

    公开(公告)日:2001-05-08

    申请号:US09418672

    申请日:1999-10-14

    IPC分类号: C22F100

    摘要: Improved targets for use in DC_magnetron sputtering of aluminum or like metals are disclosed for forming metallization films having low defect densities. Methods for manufacturing and using such targets are also disclosed. Conductivity anomalies such as those composed of metal oxide inclusions can induce arcing between the target surface and the plasma. The arcing can lead to production of excessive deposition material in the form of splats or blobs. Reducing the content of conductivity anomalies and strengthening the to-be-deposited material is seen to reduce production of such splats or blobs. Other splat limiting steps include smooth finishing of the target surface and low-stress ramp up of the plasma.

    摘要翻译: 公开了用于形成具有低缺陷密度的金属化膜的改进的用于铝或类似金属的DC_磁控溅射的靶。 还公开了制造和使用这些靶的方法。 诸如由金属氧化物夹杂物组成的电导率异常可以引起目标表面和等离子体之间的电弧。 电弧会导致过剩的沉积材料以斑块或斑点的形式产生。 减少电导率异常的含量和加强待沉积材料可以减少这种斑块或斑点的产生。 其它限制步骤包括平滑地对目标表面进行精加工和等离子体的低应力升高。

    Selective metal via plug growth technology for deep sub-micrometer ULSI

    公开(公告)号:US5539247A

    公开(公告)日:1996-07-23

    申请号:US447870

    申请日:1995-05-24

    IPC分类号: H01L21/768 H01L23/48

    CPC分类号: H01L21/76879

    摘要: Metal pillars (18) having diameters of less than about 1.0 .mu.m are grown in vias (16) in dielectric layers (14) between metal layers (12, 22) by a process comprising: (a) forming a first metal layer (12) at a first temperature and patterning the metal layer; (b) forming the dielectric layer to encapsulate the first patterned metal layer, the dielectric layer having a compressive stress of at least about 100 MegaPascal and being formed at a second temperature; (c) opening vias in the dielectric layer to exposed underlying portions of the patterned metal layer, the vias being less than about 1.0 .mu.m in diameter; (d) heating the semiconductor wafer at a temperature that is greater than either the first or second temperatures to induce growth of metal in the vias from the metal layer; and (e) forming the second metal layer (22) over the dielectric layer to make contact with the metal pillars.