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    Method for producing oligomers
    1.
    发明授权
    Method for producing oligomers 失效
    生产低聚物的方法

    公开(公告)号：US06852898B2

    公开(公告)日：2005-02-08

    申请号：US10221168

    申请日：2001-03-22

    申请人： Ralf Schulz ,  Thomas Heidemann ,  Peter Schwab ,  Peter Zehner

    发明人： Ralf Schulz ,  Thomas Heidemann ,  Peter Schwab ,  Peter Zehner

    IPC分类号： B01J19/24 ,  C07B61/00 ,  C07C2/08 ,  C07C2/10 ,  C07C2/24 ,  C07C11/02 ,  C07C2/06

    CPC分类号： C07C2/10 ,  B01J19/2465 ,  C07C2/08

    摘要： In a process for preparing essentially unbranched oligomers of alkenes having from 4 to 6 carbon atoms starting from the alkenes or a hydrocarbon stream comprising such alkenes over a nickel-containing heterogeneous catalyst in an adiabatically operated reactor at from 20 to 300° C. and pressures of from 1 to 100 bar, a first substream of the output from the reactor is worked up to isolate the oligomers and the second substream is recirculated together with fresh alkene or a fresh hydrocarbon stream comprising such alkenes to the reactor.

    摘要翻译： 在从20-300℃绝热操作的反应器中，在烯烃或含有这种烯烃的含烃非均相催化剂的基础上制备基本上未分支的具有4-6个碳原子的烯烃低聚物的方法， 1至100巴，将来自反应器的输出的第一子流排除以分离低聚物，并将第二子流与新鲜的烯烃或包含这种烯烃的新鲜烃物流一起再循环到反应器中。

    Reactor for carrying out gas-liquid, liquid, liquid-liquid or gas-liquid-solid chemical reactions
    2.
    发明授权
    Reactor for carrying out gas-liquid, liquid, liquid-liquid or gas-liquid-solid chemical reactions 失效
    用于进行气液，液体，液体或液体 - 液体 - 固体化学反应的反应器

    公开(公告)号：US06838061B1

    公开(公告)日：2005-01-04

    申请号：US09831402

    申请日：1999-11-23

    申请人： Stefan Berg ,  Peter Zehner ,  Regina Benfer ,  Jörn Müller ,  Michael Nilles ,  Ralf Schulz ,  Dieter Stützer

    发明人： Stefan Berg ,  Peter Zehner ,  Regina Benfer ,  Jörn Müller ,  Michael Nilles ,  Ralf Schulz ,  Dieter Stützer

    IPC分类号： B01J8/22 ,  B01J10/00 ,  B01J19/00 ,  B01J19/24 ,  B01J19/26 ,  C07B61/00 ,  C07C45/72 ,  C07C51/235 ,  C07C53/122 ,  F28D7/00

    CPC分类号： C07C45/72 ,  B01J8/226 ,  B01J8/228 ,  B01J10/002 ,  B01J19/006 ,  B01J19/246 ,  B01J19/2465 ,  B01J2208/00123 ,  B01J2219/00078 ,  B01J2219/00777

    摘要： A reactor (1) of high cylindrical construction for continuously carrying out gas-liquid, liquid-liquid or gas-liquid-solid reactions, provided with a downward-directed jet nozzle (2) via which the starting materials and the reaction mixture are fed in and which is located in the upper region of the reactor, and provided with an offtake (3), preferably in the lower region of the reactor, via which the reaction mixture is conveyed via an external circuit back to the jet nozzle (2) by means of a pump (P), wherein a guide tube (4) which extends essentially over the total length of the reactor (1) with the exception of the reactor ends and has a cross-sectional area in the range from one tenth to one half of the cross-sectional area of the reactor (1) is located concentrically in the reactor (1), and the jet nozzle (2) is located above the upper end of the guide tube (4), preferably at a distance of from one eighth of the guide tube diameter to one guide tube diameter, or projects into the guide tube (4) to a depth up to a plurality of guide tube diameters is proposed. A heat exchanger, in particular a heat exchanger having heat exchange tubes (6), preferably running parallel to the guide tube, welded in between plates (5), is integrated into the annular space.

    摘要翻译： 一种高筒形结构的反应器（1），用于连续地进行气液，液 - 液或气 - 液 - 固反应，设有向下的喷射喷嘴（2），原料和反应混合物通过该喷嘴 并且其位于反应器的上部区域中，并且优选地在反应器的下部区域中设置有出料口（3），经由该反应混合物经由外部回路将反应混合物输送回到喷嘴（2） 通过泵（P），其中除了反应器端部之外基本上延伸到反应器（1）的总长度上的导管（4），并且横截面积在十分之一到 反应器（1）的横截面积的一半是同心地位于反应器（1）中，并且喷嘴（2）位于导管（4）的上端之上，优选距离 从引导管直径的八分之一到一个导管直径，或投入到 引导管（4）的深度达到多个导管直径。 热交换器，特别是具有焊接在板（5）之间的平行于引导管的热交换管（6）的换热器（6）整合到环形空间中。

    PROCESS FOR PREPARING ISOCYANATES
    4.
    发明申请
    PROCESS FOR PREPARING ISOCYANATES 有权
    制备异氰酸酯的方法

    公开(公告)号：US20120172621A1

    公开(公告)日：2012-07-05

    申请号：US13394647

    申请日：2010-09-09

    申请人： Torsten Mattke ,  Matthias Kloetzer ,  Eckhard Stroefer ,  Bernhard Geissler ,  Peter Zehner

    发明人： Torsten Mattke ,  Matthias Kloetzer ,  Eckhard Stroefer ,  Bernhard Geissler ,  Peter Zehner

    IPC分类号： C07C263/06

    CPC分类号： C07C263/04 ,  C07C263/06 ,  C07C265/14

    摘要： The invention relates to a multistage process for the continuous preparation of organic, distillable polyisocyanates, preferably diisocyanates, particularly preferably aliphatic or cycloaliphatic diisocyanates, by reaction of the corresponding organic polyamines with carbonic acid derivatives and alcohols to form low molecular weight monomeric polyurethanes and thermal dissociation of the latter, in which the polyisocyanates produced and unusable residues are separated off at particular stages of the reaction and reusable by-products and intermediates are recirculated to preceding stages.

    摘要翻译： 本发明涉及通过相应的有机多胺与碳酸衍生物和醇的反应连续制备有机，可蒸馏的多异氰酸酯，优选二异氰酸酯，特别优选脂族或脂环族二异氰酸酯的多级方法，以形成低分子量单体聚氨酯和热解离 其中多异氰酸酯产生和不可用的残余物在反应的特定阶段被分离，并且可重复使用的副产物和中间体再循环到前面的阶段。

    Hydroformylation
    8.
    发明授权
    Hydroformylation 有权
    加氢甲酰化

    公开(公告)号：US07351384B2

    公开(公告)日：2008-04-01

    申请号：US11218532

    申请日：2005-09-06

    申请人： Peter Zehner ,  Michael Nilles

    发明人： Peter Zehner ,  Michael Nilles

    IPC分类号： B01J10/00 ,  B01J19/00

    CPC分类号： C07C45/50 ,  B01J19/006 ,  B01J19/2435 ,  B01J19/246 ,  B01J2219/00033 ,  B01J2219/00083 ,  B01J2219/00108 ,  B01J2219/0011 ,  B01J2219/00182 ,  B01J2219/00777 ,  C07C47/12

    摘要： Olefins having at least 6 carbon atoms are bydroformylated in the presence of a homogenous catalyst in a continuous process in which a) a vertical tall cylindrical reactor (1) whose interior space is divided by means of internals (2). into at least two reaction chambers which extend essentially in the longitudinal direction of the reactor is used, b) at least one olefin is introduced into the reactor together with synthesis gas at the lower end of the first reaction chamber, c) a partially reacted reaction mixture is conveyed from the upper end of a reaction chamber to the lower end of a next reaction chamber; and d) the hydroformylated olefin is taken off at the upper end of the last reaction chamber. The process allows a high conversion at a given reactor volume.

    摘要翻译： 具有至少6个碳原子的烯烃在连续过程中在均匀催化剂存在下加氢甲酰化，其中a）垂直的高柱形反应器（1），其内部空间通过内件（2）分成至少两个反应室 使用基本上在反应器的纵向延伸的方法，b）至少一种烯烃与第一反应室下端的合成气一起引入反应器，c）部分反应的反应混合物从上部 反应室的末端到下一个反应室的下端; 和d）加氢甲酰化烯烃在最后反应室的上端取出。 该方法允许在给定反应器体积下的高转化率。

    Method for producing aldehydes and/or alcohols or amines
    10.
    发明授权
    Method for producing aldehydes and/or alcohols or amines 有权
    醛和/或醇或胺的制备方法

    公开(公告)号：US06642420B1

    公开(公告)日：2003-11-04

    申请号：US09762425

    申请日：2001-02-07

    申请人： Peter Zehner ,  Armin Ulonska ,  Rocco Paciello

    发明人： Peter Zehner ,  Armin Ulonska ,  Rocco Paciello

    IPC分类号： C07C4549

    CPC分类号： C07C209/60 ,  B01J10/002 ,  B01J19/006 ,  B01J19/246 ,  B01J19/26 ,  B01J2219/00103 ,  B01J2219/0011 ,  B01J2219/00162 ,  B01J2219/00777 ,  C07C45/50 ,  C07C47/02

    摘要： A process for the preparation of aldehydes and/or alcohols or amines by reacting olefins in the liquid phase with carbon monoxide and hydrogen, a part of these gases being dispersed in the form of gas bubbles in the reaction liquid and another part being dissolved in the reaction liquid, in the presence or absence of a primary or secondary amine and in the presence of a cobalt carbonyl, rhodium carbonyl, palladium carbonyl or ruthenium carbonyl complex dissolved homogeneously in the reaction liquid and having a phosphorus-, arsenic-, antimony- or nitrogen-containing ligand, at elevated temperatures and at 1 to 100 bar, wherein the reaction is carried out in a vertically arranged, tubular reactor comprising a reactor body and at least one circulation line, a part of the reaction liquid is fed continuously via the circulation line to at least one nozzle which is mounted in the upper part of the reactor body and is coordinated with a guide member, open at the top and bottom and bounded by parallel walls, in the interior of the reactor and with a baffle present below the lower opening of the guide member, and a downward-directed liquid stream containing dispersed gas bubbles is produced by means of this nozzle in this guide member and, after leaving the guide member, is deflected into a stream flowing upward in the space between the wall of the guide member and the wall of the reactor body and is sucked into the guide member at the upper end of the guide member by the jet of the nozzle coordinated with the guide member.

    摘要翻译： 通过使液相中的烯烃与一氧化碳和氢气反应制备醛和/或醇或胺的方法，其中一部分气体以气泡的形式分散在反应液体中，另一部分溶于 在存在或不存在伯胺或仲胺的情况下和在羰基，羰基铑羰基，羰基钯或羰基钌羰基络合物存在下，均匀地溶解在反应液中并具有磷，砷，锑或 含氮配体，在升高的温度和1至100巴，其中反应在垂直布置的管式反应器中进行，其包括反应器主体和至少一个循环管线，部分反应液体经由 循环管线至少一个喷嘴，其安装在反应器主体的上部并与引导构件配合，导向构件在顶部和底部开口并且由 在反应器内部具有平行的壁，并且在引导构件的下开口下方存在挡板，并且在该引导构件中通过该喷嘴产生包含分散气泡的向下指向的液体流，并且在离开 引导构件被偏转到在引导构件的壁和反应器主体的壁之间的空间中向上流动的流中，并且通过与引导构件的喷嘴配合的喷嘴的喷嘴被吸入引导构件的上端处的引导构件 导向件。