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    Combinatorial preparation and testing of heterogeneous catalysts
    1.
    发明申请
    Combinatorial preparation and testing of heterogeneous catalysts 审中-公开
    组合制备和非均相催化剂的试验

    公开(公告)号：US20060127287A1

    公开(公告)日：2006-06-15

    申请号：US11336843

    申请日：2006-01-23

    申请人： Hartmut Hibst ,  Andreas Tenten ,  Dirk Demuth ,  Ferdi Schueth ,  Stephan Schunk

    发明人： Hartmut Hibst ,  Andreas Tenten ,  Dirk Demuth ,  Ferdi Schueth ,  Stephan Schunk

    IPC分类号： D21C11/00

    CPC分类号： B01J19/0046 ,  B01J37/0215 ,  B01J37/0217 ,  B01J2219/00286 ,  B01J2219/00306 ,  B01J2219/00511 ,  B01J2219/00585 ,  B01J2219/0059 ,  B01J2219/00599 ,  B01J2219/00747

    摘要： The array of heterogeneous catalysts and/or their precursors, is made up of a body which has, preferably parallel, through-channels and in which at least n channels comprise n different heterogeneous catalysts and/or their precursors, where n is 2, preferably 10, particularly preferably 100, in particular 1000, especially 10,000. A process for preparing arrays comprising the following steps: a1) preparing solutions, emulsions and/or dispersions of elements and/or element compounds of the elements present in the catalyst and/or catalyst precursor and, if appropriate preparing dispersions of inorganic support materials, a2) if appropriate introducing adhesion promoters, binders, viscosity regulators, pH regulators and/or solid inorganic supports into the solutions, emulsions and/or dispersions, a3) simultaneously or successively coating the channels of the body with the solutions, emulsions and/or dispersions, a predetermined amount of the solutions, emulsions and/or dispersions being introduced into each channel to obtain a predetermined composition and a4) if appropriate heating the coated body in the presence or absence of inert gases or reactive gases to a temperature in the range from 20 to 1500° C. to dry, with or without sintering or calcining, the catalysts and/or catalyst precursors.

    摘要翻译： 非均相催化剂和/或其前体的阵列由具有优选平行的通道的主体组成，其中至少n个通道包含n个不同的非均相催化剂和/或其前体，其中n为2，优选为 10，特别优选100，特别是1000，特别是10,000。 一种制备阵列的方法，包括以下步骤：a1）制备存在于催化剂和/或催化剂前体中的元素和/或元素化合物的溶液，乳液和/或分散体，以及如果合适的话，制备无机载体材料的分散体， a2）如果合适，将粘合促进剂，粘合剂，粘度调节剂，pH调节剂和/或固体无机载体引入溶液，乳液和/或分散体中，a3）用溶液，乳液和/或分散体同时或连续地涂覆身体的通道 分散体，预定量的溶液，乳液和/或分散体被引入每个通道以获得预定的组合物和a）如果在存在或不存在惰性气体或反应气体的情况下适当地加热涂覆体到达该范围内的温度 20至1500℃，用或不用烧结或煅烧来干燥催化剂和/或催化剂前体。

    Preparation of phthalic anhydride by gas phase oxidation of O-xylene in a main reactor and postreactor
    8.
    发明授权
    Preparation of phthalic anhydride by gas phase oxidation of O-xylene in a main reactor and postreactor 有权
    在主反应器和后反应器中通过气相氧化邻二甲苯制备邻苯二甲酸酐

    公开(公告)号：US08106220B2

    公开(公告)日：2012-01-31

    申请号：US12301370

    申请日：2007-05-18

    申请人： Thomas Mackewitz ,  Frank Rosowski ,  Andreas Tenten

    发明人： Thomas Mackewitz ,  Frank Rosowski ,  Andreas Tenten

    IPC分类号： C07D307/89

    CPC分类号： C07D307/89 ,  C07C51/265 ,  C07C63/16

    摘要： A process is described for preparing phthalic anhydride by catalytic gas phase oxidation of o-xylene, in which a gaseous mixture of o-xylene and an oxygenous gas is converted in a main reactor to a gaseous intermediate reaction product which comprises unconverted o-xylene, phthalic anhydride underoxidation products and phthalic anhydride, the heat of reaction which arises in the main reactor being removed at least partly by indirect cooling with a heat carrier medium, and the intermediate reaction product being introduced into a postreactor. The concentration of unconverted o-xylene in the intermediate reaction product is at least 1% by weight, and the sum of the concentrations of phthalic anhydride underoxidation products in the intermediate reaction product is at least 0.5% by weight. The process allows an increase in the overall yield of phthalic anhydride without or without significant deterioration in the product quality.

    摘要翻译： 描述了通过邻二甲苯的催化气相氧化制备邻苯二甲酸酐的方法，其中邻二甲苯和氧气的气体混合物在主反应器中转化为包含未转化的邻二甲苯的气态中间体反应产物， 邻苯二甲酸酐脱氧产物和邻苯二甲酸酐，至少部分通过用载热介质间接冷却除去主反应器中产生的反应热，并将中间反应产物引入后反应器中。 中间反应产物中未转化的邻二甲苯的浓度为至少1重量％，中间反应产物中邻苯二甲酸酐未氧化产物的浓度之和为至少0.5重量％。 该方法允许邻苯二甲酸酐的总产率提高，而不会产生质量的显着劣化。