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    Methods of preparation of an olefin oligomerization catalyst
    1.
    发明授权
    Methods of preparation of an olefin oligomerization catalyst 有权
    制备烯烃低聚催化剂的方法

    公开(公告)号：US07910670B2

    公开(公告)日：2011-03-22

    申请号：US12534536

    申请日：2009-08-03

    申请人： Ronald D. Knudsen ,  Ronald G. Abbott ,  Bruce E. Kreischer ,  Eduardo J. Baralt ,  Brooke L. Small

    发明人： Ronald D. Knudsen ,  Ronald G. Abbott ,  Bruce E. Kreischer ,  Eduardo J. Baralt ,  Brooke L. Small

    IPC分类号： C08F4/69

    CPC分类号： C07C2/32 ,  B01J31/04 ,  B01J31/128 ,  B01J31/143 ,  B01J31/18 ,  B01J31/181 ,  B01J31/2226 ,  B01J31/4092 ,  B01J2231/20 ,  B01J2531/62 ,  C07C2527/125 ,  C07C2531/22 ,  C08F10/00 ,  Y02P20/584 ,  C08F4/69

    摘要： A method of making an olefin oligomerization catalyst, comprising contacting a chromium-containing compound, a heteroatomic ligand, and a metal alkyl, wherein the chromium-containing compound comprises less than about 5 weight percent chromium oligomers. A method of making an olefin oligomerization catalyst comprising a chromium-containing compound, a nitrogen-containing compound, and a metal alkyl, the method comprising adding a composition comprising the chromium-containing compound to a composition comprising the metal alkyl. A method of making an olefin oligomerization catalyst comprising a chromium-containing compound, a nitrogen-containing compound, and a metal alkyl, the method comprising abating all or a portion of water, acidic protons, or both from a composition comprising the chromium-containing compound, a composition comprising the nitrogen-containing compound, or combinations thereof prior to or during the preparation of the catalyst. Methods of oligomerizing olefins by contacting such catalysts with an alpha olefin.

    摘要翻译： 一种制备烯烃低聚催化剂的方法，包括使含铬化合物，杂原子配体和金属烷基接触，其中所述含铬化合物包含小于约5重量％的铬低聚物。 一种制备包含含铬化合物，含氮化合物和金属烷基的烯烃低聚催化剂的方法，所述方法包括将含有所述含铬化合物的组合物加入到包含所述金属烷基的组合物中。 一种制备包含含铬化合物，含氮化合物和金属烷基的烯烃低聚催化剂的方法，该方法包括从包含含铬化合物的组合物中减少全部或一部分水，酸性质子或两者 化合物，包含含氮化合物的组合物或其组合在制备催化剂之前或期间。 通过使这种催化剂与α-烯烃接触来使烯烃低聚的方法。

    Methods of Preparation of an Olefin Oligomerization Catalyst
    4.
    发明申请
    Methods of Preparation of an Olefin Oligomerization Catalyst 有权
    烯烃低聚催化剂的制备方法

    公开(公告)号：US20090292090A1

    公开(公告)日：2009-11-26

    申请号：US12534536

    申请日：2009-08-03

    申请人： Ronald D. Knudsen ,  Ronald G. Abbott ,  Bruce E. Kreischer ,  Eduardo J. Baralt ,  Brooke L. Small

    发明人： Ronald D. Knudsen ,  Ronald G. Abbott ,  Bruce E. Kreischer ,  Eduardo J. Baralt ,  Brooke L. Small

    IPC分类号： C08F4/42 ,  B01J31/04 ,  B01J31/12

    CPC分类号： C07C2/32 ,  B01J31/04 ,  B01J31/128 ,  B01J31/143 ,  B01J31/18 ,  B01J31/181 ,  B01J31/2226 ,  B01J31/4092 ,  B01J2231/20 ,  B01J2531/62 ,  C07C2527/125 ,  C07C2531/22 ,  C08F10/00 ,  Y02P20/584 ,  C08F4/69

    摘要： A method of making an olefin oligomerization catalyst, comprising contacting a chromium-containing compound, a heteroatomic ligand, and a metal alkyl, wherein the chromium-containing compound comprises less than about 5 weight percent chromium oligomers. A method of making an olefin oligomerization catalyst comprising a chromium-containing compound, a nitrogen-containing compound, and a metal alkyl, the method comprising adding a composition comprising the chromium-containing compound to a composition comprising the metal alkyl. A method of making an olefin oligomerization catalyst comprising a chromium-containing compound, a nitrogen-containing compound, and a metal alkyl, the method comprising abating all or a portion of water, acidic protons, or both from a composition comprising the chromium-containing compound, a composition comprising the nitrogen-containing compound, or combinations thereof prior to or during the preparation of the catalyst. Methods of oligomerizing olefins by contacting such catalysts with an alpha olefin.

    摘要翻译： 一种制备烯烃低聚催化剂的方法，包括使含铬化合物，杂原子配体和金属烷基接触，其中所述含铬化合物包含小于约5重量％的铬低聚物。 一种制备包含含铬化合物，含氮化合物和金属烷基的烯烃低聚催化剂的方法，所述方法包括将含有所述含铬化合物的组合物加入到包含所述金属烷基的组合物中。 一种制备包含含铬化合物，含氮化合物和金属烷基的烯烃低聚催化剂的方法，该方法包括从包含含铬化合物的组合物中减少全部或一部分水，酸性质子或两者 化合物，包含含氮化合物的组合物或其组合在制备催化剂之前或期间。 通过使这种催化剂与α-烯烃接触来使烯烃低聚的方法。

    Linear alpha-olefin dimers possessing substantial linearity
    6.
    发明授权
    Linear alpha-olefin dimers possessing substantial linearity 有权
    线性α-烯烃二聚体具有很大的线性

    公开(公告)号：US07223893B2

    公开(公告)日：2007-05-29

    申请号：US10056137

    申请日：2002-01-24

    申请人： Brooke L. Small ,  Eduardo J Baralt

    发明人： Brooke L. Small ,  Eduardo J Baralt

    IPC分类号： C07C13/00

    CPC分类号： C07C2/32 ,  C07C11/02 ,  C07C2531/22 ,  C07C2531/26

    摘要： Linear 1-butene dimers and other linear alpha-olefin dimers are manufactured in high yield and with high selectivity by coupling of alpha-olefins. The coupling is accomplished by contacting alpha olefins with an iron-based catalyst activated with an aluminum-based co-catalyst. The catalyst is structured to preclude formation of multiple dimer products, and the byproducts of the olefin coupling consist almost exclusively of methyl branched olefin dimers. The dimers have potentially diverse use in areas stretching form pharmaceuticals to plastics. Linear 1-butene dimers may be particularly useful in the production of plasticizer alcohols which may in turn be used to manufacture high quality plastics with reduced leaching.

    摘要翻译： 线性1-丁烯二聚体和其它直链α-烯烃二聚体以高产率和高选择性通过α-烯烃的偶联制备。 通过使α-烯烃与用铝基助催化剂活化的铁基催化剂接触来实现偶合。 该催化剂被构造成排除多个二聚体产物的形成，并且烯烃偶联的副产物几乎完全由甲基支链烯烃二聚体组成。 二聚体在从药物到塑料中拉伸的领域中具有潜在的多种用途。 线性1-丁烯二聚体可以特别用于生产增塑剂醇，其可以用于制造具有减少浸出的高质量塑料。