公开(公告)号：US06011083A

公开(公告)日：2000-01-04

申请号：US874633

申请日：1997-06-13

申请人： Sadanao Okuda ,  Masato Ishikawa ,  Takashi Suzuki ,  Takahiro Wakayama ,  Yoshihiro Hayashi

发明人： Sadanao Okuda ,  Masato Ishikawa ,  Takashi Suzuki ,  Takahiro Wakayama ,  Yoshihiro Hayashi

IPC分类号： C09D11/00 ,  C09D11/02 ,  C09D11/0235 ,  C09D11/033 ,  C09D11/037 ,  C09D11/10 ,  C09D11/103 ,  C09D11/104 ,  C09D11/106 ,  C09D11/107 ,  C09D11/108 ,  C09D5/00

CPC分类号： C09D11/0235

摘要： A water-in-oil (W/O) emulsion ink for stencil printing is provided, which is excellent in emulsion stability and drying, high in printing density and low in blurring and seep through. The W/O emulsion ink has an oil phase and a water phase, in which an acid anhydride containing water-soluble polymer is contained together with a water-insoluble colorant in said water phase. The acid anhydride containing water-soluble polymer is preferably an acid anhydride containing olefin copolymer, more specifically, an isobutylene-maleic anhydride copolymer, or an acid anhydride containing vinyl copolymer, more specifically, a styrene-maleic anhydride copolymer. Preferably, the oil phase comprises at least a solvent and an emulsifier, and the water phase comprises a water-in-oil (O/W) emulsion of resin and/or a water-soluble resin.

摘要翻译： 提供用于模版印刷的油包水（W / O）乳液油墨，其乳化稳定性和干燥性优异，印刷密度高，模糊和渗透低。 W / O乳液油墨具有油相和水相，其中含有水溶性聚合物的酸酐与所述水相中的水不溶性着色剂一起被包含。 含酸酐的水溶性聚合物优选为含酸酐的烯烃共聚物，更具体地说是异丁烯 - 马来酸酐共聚物，或含酸酐的乙烯基共聚物，更具体地说，苯乙烯 - 马来酸酐共聚物。 优选地，油相至少包含溶剂和乳化剂，水相包含树脂和/或水溶性树脂的油包水（O / W）乳液。

公开(公告)号：US5904759A

公开(公告)日：1999-05-18

申请号：US987780

申请日：1997-12-09

申请人： Sadanao Okuda ,  Masato Ishikawa ,  Takashi Suzuki ,  Yoshihiro Hayashi

发明人： Sadanao Okuda ,  Masato Ishikawa ,  Takashi Suzuki ,  Yoshihiro Hayashi

IPC分类号： B01F13/10 ,  C09D11/02 ,  C09D11/0235 ,  C09D11/037

CPC分类号： C09D11/0235 ,  B01F3/0811 ,  B01F3/088

摘要： A process for preparing a stencil printing emulsion ink which is a water-in-oil (W/O) emulsion having an oil phase and a water phase and containing a water-insoluble colorant in the water phase, is provided. The process comprises the steps of preparing an aqueous dispersion of said water-insoluble colorant separately from water or an aqueous solution of the remaining water phase components, and adding said aqueous dispersion and water or said aqueous solution separately to said oil phase for emulsification. The process is suitable to produce emulsion inks of various colors, particularly of mixed colors containing two or more colorants in the water phase with a fixed formulation of the oil phase.

摘要翻译： 提供了一种制备蜡纸印刷乳液油墨的方法，该油墨是具有油相和水相的水包油（W / O）乳液，并且在水相中含有水不溶性着色剂。 该方法包括以下步骤：分别从水或剩余水相组分的水溶液中制备所述水不溶性着色剂的水分散体，并将所述水分散体和水或所述水溶液分别加入所述油相中进行乳化。 该方法适用于生产各种颜色的乳液油墨，特别是在水相中含有两种或更多种着色剂的混合颜色，其具有油相的固定配方。

公开(公告)号：US5759245A

公开(公告)日：1998-06-02

申请号：US806077

申请日：1997-02-25

申请人： Sadanao Okuda ,  Masato Ishikawa ,  Takashi Suzuki ,  Yoshihiro Hayashi

发明人： Sadanao Okuda ,  Masato Ishikawa ,  Takashi Suzuki ,  Yoshihiro Hayashi

IPC分类号： C09D11/00 ,  C09D11/02 ,  C09D11/0235 ,  C09D11/033 ,  C09D11/037

CPC分类号： C09D11/0235

摘要： An water-in-oil (W/O) emulsion ink for stencil printing is provided, which is excellent in emulsion stability. The water-in-oil (W/O) emulsion ink has an oil phase and a water phase, in which a water-insoluble colorant is contained in said water phase, and said water-insoluble colorant comprises an insoluble azo pigment. The insoluble azo pigment contained in the water phase preferably has an average particle size of 1 .mu.m or less. The emulsion ink is preferably formed by use of an emulsifier having an HLB of 1.5-6.0, and the water phase preferably has a maximum particle diameter of 10 .mu.m or less.

摘要翻译： 提供用于模版印刷的油包水（W / O）乳液油墨，其乳液稳定性优异。 油包水（W / O）乳液油墨具有油相和水相，其中在所述水相中含有水不溶性着色剂，所述水不溶性着色剂包含不溶性偶氮颜料。 水相中含有的不溶性偶氮颜料的平均粒径优选为1μm以下。 乳液油墨优选通过使用HLB为1.5-6.0的乳化剂形成，水相优选具有10μm以下的最大粒径。

公开(公告)号：US5718748A

公开(公告)日：1998-02-17

申请号：US785834

申请日：1997-01-15

申请人： Takashi Suzuki ,  Masato Ishikawa ,  Yoshihiro Hayashi ,  Sadanao Okuda

发明人： Takashi Suzuki ,  Masato Ishikawa ,  Yoshihiro Hayashi ,  Sadanao Okuda

IPC分类号： B41M1/12 ,  C09D11/00 ,  C09D11/02 ,  C09D11/0235 ,  C09D11/033

CPC分类号： C09D11/0235

摘要： An water-in-oil (W/O) emulsion ink for stencil printing is provided, which is excellent in emulsion stability and drying, high in printing density and low in blurring and seep through. The W/O emulsion ink has an oil phase and a water phase, in which a water-insoluble colorant is contained in said water phase, and said oil phase comprises a solvent and an agent for thickening said solvent. The oil phase preferably has a viscosity at 23.degree. C. of 5-20,000 cps, more preferably 15-2,000 cps. The thickening agent may be a resin in an amount of 1-30%, preferably 2-25% by weight of the total of the ink, or may be oil-insoluble particulates or powders in an amount of 0.01-10%, preferably 0.1-5% by weight of the total of the ink.

摘要翻译： 提供了用于模版印刷的油包水（W / O）乳液油墨，其乳化稳定性和干燥性优异，印刷密度高，模糊和渗透低。 W / O乳液油墨具有油相和水相，其中在所述水相中含有水不溶性着色剂，所述油相包含溶剂和用于增稠所述溶剂的试剂。 油相优选在23℃下的粘度为5-20,000cps，更优选为15-2,000cps。 增稠剂可以是总量为1-30重量％，优选2-25重量％的树脂，或者可以是0.01-10重量％，优选为0.1重量％的不溶于油的微粒或粉末 -5％的油墨总重量。

公开(公告)号：US5776232A

公开(公告)日：1998-07-07

申请号：US818720

申请日：1997-03-14

申请人： Sadanao Okuda ,  Masato Ishikawa ,  Takashi Suzuki ,  Yoshihiro Hayashi

发明人： Sadanao Okuda ,  Masato Ishikawa ,  Takashi Suzuki ,  Yoshihiro Hayashi

IPC分类号： C09D11/00 ,  C09D11/02 ,  C09D11/0235 ,  C09D11/033 ,  C09D11/037

CPC分类号： C09D11/0235

摘要： A water-in-oil (W/O) emulsion ink for stencil printing is provided, which contains a water-insoluble colorant in the water phase, has the water phase dispersed finely and stably in the oil phase, and can provide prints high in printing density and glossiness. The water-insoluble colorant has an average particle size of 1 .mu.m or less, and is constituted by particles of 1 .mu.m or less in particle size in an amount of 50% or more on area basis of the total of the water-insoluble colorant. The emulsion ink is preferably formed by use of an emulsifier having an HLB of 1.5-6.0, and preferably contains a tertiary amine compound in the water phase as a dispersant for the water-insoluble colorant.

摘要翻译： 提供了一种用于模版印刷的油包水（W / O）乳液油墨，其在水相中含有水不溶性着色剂，水相在油相中精细稳定地分散，并且可以提供高的 印刷密度和光泽度。 水不溶性着色剂的平均粒径为1μm以下，由不溶于水的着色剂的总面积的50％以上的粒径的1μm以上的粒子构成 着色剂。 乳液油墨优选通过使用HLB为1.5-6.0的乳化剂形成，并且优选在水相中含有叔胺化合物作为水不溶性着色剂的分散剂。

公开(公告)号：US5637137A

公开(公告)日：1997-06-10

申请号：US597984

申请日：1996-02-07

申请人： Sadanao Okuda ,  Yoshihiro Hayashi

发明人： Sadanao Okuda ,  Yoshihiro Hayashi

IPC分类号： C09D11/00 ,  C09D11/02 ,  C09D11/0235 ,  C09D11/033 ,  C09D11/037

CPC分类号： C09D11/0235

摘要： An emulsion ink for stencil printing of a water-in-oil (W/O) having an oil phase and a water phase is disclosed which emulsion ink is characterized in that the water phase contains an extender pigment. The emulsion ink can provide printed images having a high print concentration and a constant quality without causing strike through, offset, and bleeding of ink.

摘要翻译： 公开了一种具有油相和水相的油包水（W / O）的蜡纸印刷用乳液油墨，乳液油墨的特征在于水相含有增量颜料。 乳液油墨可以提供具有高印刷浓度和恒定质量的印刷图像，而不会引起油墨的渗透，偏移和渗色。

公开(公告)号：US5667570A

公开(公告)日：1997-09-16

申请号：US640192

申请日：1996-04-30

申请人： Sadanao Okuda ,  Yoshihiro Hayashi

发明人： Sadanao Okuda ,  Yoshihiro Hayashi

IPC分类号： C09D11/00 ,  C09D11/02 ,  C09D11/0235 ,  C09D11/033 ,  C09D11/037 ,  C09D11/10 ,  C09D11/103 ,  C09D11/104 ,  C09D11/106 ,  C09D11/107 ,  C09D11/108 ,  C09D11/08

CPC分类号： C09D11/0235

摘要： An emulsion ink for stencil printing is provided, which affords a printed image having a high density and a constant quality, without being influenced by kinds of printing paper used, and by the presence or absence of projections and depressions on the surface of printing paper used, has a superior drying property of ink and does not cause any exudation, seeping-through and offsetting, which emulsion ink for stencil printing comprises an oil phase and an aqueous phase to form a Water-in-oil(W/O) type emulsion ink, wherein a extender pigment is contained in the oil phase of the emulsion ink.

摘要翻译： 提供了一种用于模板印刷的乳液油墨，其不受所使用的打印纸的种类的影响，以及在使用的打印纸的表面上是否存在凸起和凹陷，从而提供具有高密度和恒定品质的印刷图像 具有优异的油墨干燥性能，并且不会引起任何渗出，渗透和粘合，用于模板印刷的乳液油墨包含油相和水相以形成油包水（W / O）型乳液 油墨，其中在乳液油墨的油相中含有增量颜料。

公开(公告)号：US5738715A

公开(公告)日：1998-04-14

申请号：US759630

申请日：1996-12-05

申请人： Sadanao Okuda ,  Yoshihiro Hayashi

发明人： Sadanao Okuda ,  Yoshihiro Hayashi

IPC分类号： C09D11/00 ,  C09D11/02 ,  C09D11/033 ,  C09D11/037

CPC分类号： C09D11/0235

摘要： A water-in-oil (W/O) emulsion ink for stencil printing, high in printing density, low in seep through and blurring and excellent in temperature stability, is provided, which contains carbon black as a water-insoluble colorant in the water phase, in which said carbon black has a pH value of 6 to 10. The carbon black is preferably 10 .mu.m or less in average particle diameter. The water phase may contain an oil-in-water (O/W) emulsion of resin and/or a water-soluble resin to improve dispersion of carbon black in water and its fixation to prints. The oil phase may be free from any resinous component.

摘要翻译： 提供了一种用于模板印刷的油包水（W / O）乳液油墨，具有高的印刷密度，低渗透性和模糊性以及优异的温度稳定性，其在水中含有作为水不溶性着色剂的炭黑 所述炭黑的pH值为6〜10。所述炭黑的平均粒径优选为10μm以下。 水相可以含有树脂和/或水溶性树脂的水包油（O / W）乳液，以改善炭黑在水中的分散和其对印刷品的固着。 油相可以不含任何树脂成分。

公开(公告)号：US08937023B2

公开(公告)日：2015-01-20

申请号：US13363638

申请日：2012-02-01

申请人： Fuminori Ito ,  Yoshihiro Hayashi

发明人： Fuminori Ito ,  Yoshihiro Hayashi

IPC分类号： H01L23/48 ,  H01L21/316 ,  C23C16/40 ,  C23C18/12 ,  C23C18/14 ,  H01L21/02

CPC分类号： H01L21/31695 ,  C23C16/401 ,  C23C18/1212 ,  C23C18/122 ,  C23C18/14 ,  H01L21/02126 ,  H01L21/02203 ,  H01L21/02216 ,  H01L21/02274 ,  H01L21/02348 ,  H01L21/02362

摘要： A method includes forming an insulating film over a substrate by introducing a cyclic siloxane compound having a cyclic siloxane as a skeleton and having at least one volatile hydrocarbon group bonded to a side chain, and a silicon-containing compound into a plasma, and converting the insulating film to a porous insulating film by adding energy to the insulating film. The silicon-containing compound is decomposed using less energy as compared with the skeleton of the cyclic siloxane compound, the volatile hydrocarbon group, and the bond between the cyclic siloxane compound and the volatile hydrocarbon group.

摘要翻译： 一种方法包括通过引入具有环状硅氧烷作为骨架并具有至少一个与侧链结合的挥发性烃基的环状硅氧烷化合物，将含硅化合物引入等离子体中，在基板上形成绝缘膜， 通过向绝缘膜添加能量将绝缘膜与多孔绝缘膜接合。 与环状硅氧烷化合物，挥发性烃基，环状硅氧烷化合物和挥发性烃基的键相比，含硅化合物的分解能力较少。

公开(公告)号：US08648441B2

公开(公告)日：2014-02-11

申请号：US13106590

申请日：2011-05-12

申请人： Kenichiro Hijioka ,  Ippei Kume ,  Naoya Inoue ,  Hiroki Shirai ,  Jun Kawahara ,  Yoshihiro Hayashi

发明人： Kenichiro Hijioka ,  Ippei Kume ,  Naoya Inoue ,  Hiroki Shirai ,  Jun Kawahara ,  Yoshihiro Hayashi

IPC分类号： H01L21/02

CPC分类号： H01L27/10894 ,  H01L21/76811 ,  H01L23/5223 ,  H01L27/10852 ,  H01L28/75 ,  H01L28/91 ,  H01L2924/0002 ,  H01L2924/00

摘要： A semiconductor device has a substrate; a multi-layered interconnect formed on the substrate, and having a plurality of interconnect layers, each of which being configured by an interconnect and an insulating layer, stacked therein; a memory circuit formed in a memory circuit region on the substrate in a plan view, and having a peripheral circuit and at least one capacitor element embedded in the multi-layered interconnect; and a logic circuit formed in a logic circuit region on the substrate, wherein the capacitor element is configured by a lower electrode, a capacitor insulating film, an upper electrode, an embedded electrode and an upper interconnect; the top surface of the upper interconnect, and the top surface of the interconnect configuring the logic circuit formed in the same interconnect layer with the upper interconnect, are aligned to the same plane.

摘要翻译： 半导体器件具有基板; 形成在所述基板上的多层互连，并且具有多个互连层，每个互连层由布置在其中的互连和绝缘层构成; 在平面图形成在基板上的存储器电路区域中的存储电路，并且具有外围电路和嵌入多层互连中的至少一个电容元件; 以及形成在所述基板上的逻辑电路区域中的逻辑电路，其中所述电容器元件由下电极，电容器绝缘膜，上电极，嵌入电极和上互连构成; 上互连的顶表面和构成与上互连的同一互连层中形成的逻辑电路的互连的顶表面与同一平面对准。