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公开(公告)号：US20100003179A1
公开(公告)日：2010-01-07
申请号：US12303468
申请日：2007-05-16
CPC分类号： C01G9/02 , C01B13/20 , C01F5/04 , C01F17/0043 , C01G1/02 , C01G9/03 , C01P2002/52 , C01P2006/12
摘要： Process for preparing a metal oxide powder, in which starting materials are evaporated and oxidized, wherein a metal melt in the form of droplets and one or more combustion gases are fed to the evaporation zone of a reactor, where the metal melt is evaporated completely under nonoxidizing conditions, subsequently, the mixture flowing out of the evaporation zone is reacted in the oxidation zone of this reactor with a stream of a supplied oxygen-containing gas whose oxygen content is at least sufficient to oxidize the metal and the combustion gases completely.
摘要翻译： 制备金属氧化物粉末的方法，其中起始材料被蒸发和氧化，其中将液滴形式的一种或多种燃烧气体的金属熔体进料到反应器的蒸发区，其中金属熔体完全蒸发掉 非氧化条件随后，从蒸发区流出的混合物在该反应器的氧化区中与供氧的含氧气体流反应，其氧含量至少足以使金属和燃烧气体完全氧化。
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公开(公告)号：US20090087496A1
公开(公告)日：2009-04-02
申请号：US12299232
申请日：2007-05-09
申请人： Stipan Katusic , Guido Zimmermann , Michael Kraemer , Peter Kress , Horst Miess
发明人： Stipan Katusic , Guido Zimmermann , Michael Kraemer , Peter Kress , Horst Miess
IPC分类号： A61K33/32 , C04B14/30 , C09K3/00 , C04B35/453 , B01J23/34
CPC分类号： C01G1/02 , C01G9/00 , C01G9/03 , C01P2002/52 , C01P2002/54 , C01P2006/12 , C04B35/01 , C04B35/053 , C04B35/057 , C04B35/453 , C04B35/457 , C04B35/62665 , C04B35/6325 , C04B2235/3201 , C04B2235/3206 , C04B2235/3217 , C04B2235/3229 , C04B2235/3232 , C04B2235/3262 , C04B2235/3279 , C04B2235/3281 , C04B2235/3284 , C04B2235/40 , C04B2235/401 , C04B2235/405 , C04B2235/449 , C04B2235/5409 , C04B2235/5436
摘要： Process for preparing a mixed metal oxide powder, in which oxidizable starting materials are evaporated and oxidized, the reaction mixture is cooled after the reaction and the pulverulent solids are removed from gaseous substances, wherein as starting materials, at least one pulverulent metal and at least one metal compound, the metal and the metal component of the metal compound being different and the proportion of metal being at least 80% by weight based on the sum of metal and metal component from metal compound, together with one or more combustion gases, are fed to an evaporation zone of a reactor, where metal and metal compound are evaporated completely under nonoxidizing conditions, subsequently, the mixture flowing out of the evaporation zone is reacted in the oxidation zone of this reactor with a stream of a supplied oxygen-containing gas whose oxygen content is at least sufficient to oxidize the starting materials and combustion gases completely.
摘要翻译： 制备混合金属氧化物粉末的方法，其中可氧化原料被蒸发和氧化，反应混合物在反应后冷却，并从气态物质中除去粉状固体，其中作为原料，至少一种粉状金属和至少 一种金属化合物，金属化合物的金属和金属组分不同，并且金属比例为至少80重量％，基于来自金属化合物的金属和金属组分的总和与一种或多种燃烧气体一起是 进料到反应器的蒸发区，其中金属和金属化合物在非氧化条件下完全蒸发，随后将从蒸发区流出的混合物在该反应器的氧化区中与供给的含氧气体流 其氧含量至少足以使原料和燃烧气体完全氧化。
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公开(公告)号：US08048398B2
公开(公告)日：2011-11-01
申请号：US12299232
申请日：2007-05-09
申请人： Stipan Katusic , Guido Zimmermann , Michael Kraemer , Peter Kress , Horst Miess
发明人： Stipan Katusic , Guido Zimmermann , Michael Kraemer , Peter Kress , Horst Miess
IPC分类号： C01B13/00 , C01B13/14 , C01C1/00 , C01G49/00 , C01G25/00 , C01G41/00 , C01G9/00 , C01G23/047 , C01G30/00 , C01G28/00 , B01J23/00 , B01J21/00
CPC分类号： C01G1/02 , C01G9/00 , C01G9/03 , C01P2002/52 , C01P2002/54 , C01P2006/12 , C04B35/01 , C04B35/053 , C04B35/057 , C04B35/453 , C04B35/457 , C04B35/62665 , C04B35/6325 , C04B2235/3201 , C04B2235/3206 , C04B2235/3217 , C04B2235/3229 , C04B2235/3232 , C04B2235/3262 , C04B2235/3279 , C04B2235/3281 , C04B2235/3284 , C04B2235/40 , C04B2235/401 , C04B2235/405 , C04B2235/449 , C04B2235/5409 , C04B2235/5436
摘要： Process for preparing a mixed metal oxide powder, in which oxidizable starting materials are evaporated and oxidized, the reaction mixture is cooled after the reaction and the pulverulent solids are removed from gaseous substances, wherein as starting materials, at least one pulverulent metal and at least one metal compound, the metal and the metal component of the metal compound being different and the proportion of metal being at least 80% by weight based on the sum of metal and metal component from metal compound, together with one or more combustion gases, are fed to an evaporation zone of a reactor, where metal and metal compound are evaporated completely under nonoxidizing conditions, subsequently, the mixture flowing out of the evaporation zone is reacted in the oxidation zone of this reactor with a stream of a supplied oxygen-containing gas whose oxygen content is at least sufficient to oxidize the starting materials and combustion gases completely.
摘要翻译： 制备混合金属氧化物粉末的方法，其中可氧化原料被蒸发和氧化，反应混合物在反应后冷却，并从气态物质中除去粉状固体，其中作为原料，至少一种粉状金属和至少 一种金属化合物，金属化合物的金属和金属组分不同，并且金属比例为至少80重量％，基于来自金属化合物的金属和金属组分的总和与一种或多种燃烧气体一起是 进料到反应器的蒸发区，其中金属和金属化合物在非氧化条件下完全蒸发，随后将从蒸发区流出的混合物在该反应器的氧化区中与供给的含氧气体流 其氧含量至少足以使原料和燃烧气体完全氧化。
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4.发明授权Zinc oxide powder aggregates present in circular, ellipsoidal, linear and branched form 有权呈圆形，椭圆形，线形和分枝状的氧化锌粉末聚集体公开(公告)号：US07371337B2
公开(公告)日：2008-05-13
申请号：US10572936
申请日：2004-09-02
申请人： Stipan Katusic , Michael Kraemer , Peter Kress , Horst Miess , Guido Zimmermann , Peter Albers
发明人： Stipan Katusic , Michael Kraemer , Peter Kress , Horst Miess , Guido Zimmermann , Peter Albers
CPC分类号： C09C1/043 , C01G9/03 , C01P2004/04 , C01P2006/11
摘要： Pyrogenically prepared zinc oxide powder having a BET surface area of from 10 to 200 m2/g, which is in the form of aggregates, the aggregates being composed of particles having different morphologies, and 0-10% of the aggregates being in a circular form, 30-50% being in an ellipsoidal form, 30-50% being in a linear form and 20-30% being in a branched form. It is prepared by reacting a starting mixture containing zinc vapour, a combustible gas and steam or a mixture of steam and carbon dioxide in a flame with an oxygen-containing gas in an oxidation zone, cooling the hot reaction mixture in a quenching zone and separating the solid material from the gas stream, the amount of oxygen in the oxidation zone being greater than the amount necessary for the complete oxidation of the combustible gas and the zinc vapour. The zinc oxide powder can be used as a constituent of sun protection compositions for protection against UV radiation.
摘要翻译： 热解制备的氧化锌粉末，其BET表面积为10至200m 2 / g，其为聚集体形式，聚集体由具有不同形态的颗粒组成，并且0-10％ 的聚集体为圆形，30-50％为椭圆形，30-50％为直线形式，20-30％为分支形式。 通过在氧化区中将含有锌蒸汽，可燃气体和蒸汽或蒸汽和二氧化碳的混合物在火焰中与含氧气体的起始混合物反应制备，在淬火区域中冷却热反应混合物并分离 来自气流的固体材料，氧化区中的氧的量大于可燃气体和锌蒸汽的完全氧化所需的量。 氧化锌粉末可用作防紫外线辐射防晒组合物的组分。
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5.发明申请SILICA COATED ZINC OXIDE PARTICLES OBTAINABLE BY A FLAME PYROLYSIS PROCESS 审中-公开二氧化硅涂覆的氧化锌颗粒可以通过火焰热解过程获得公开(公告)号：US20100008872A1
公开(公告)日：2010-01-14
申请号：US12375062
申请日：2007-06-26
申请人： Stipan Katusic , Sven Hill , Michael Kroell , Guido Zimmermann , Peter Kress
发明人： Stipan Katusic , Sven Hill , Michael Kroell , Guido Zimmermann , Peter Kress
CPC分类号： C09C1/043 , A61K8/0275 , A61K8/25 , A61K8/27 , A61K2800/413 , A61K2800/621 , A61Q17/04 , B82Y30/00 , C01G9/03 , C01P2002/72 , C01P2002/84 , C01P2002/88 , C01P2004/04 , C01P2004/64 , C01P2006/12 , C08K3/22 , C08K9/02 , C09D7/62 , C09D7/67 , Y10T428/2995
摘要： Zinc silicon oxide particles with a core-shell structure which have a Zn/Si ratio of from 2 to 75, in atom %/atom %, whose fraction of Zn, Si and O is at least 99% by weight, based on the zinc silicon oxide particles, which have a BET surface area of from 10 to 60 m2/g, a weight-averaged primary particle diameter of from 10 to 75 nm an average aggregate area of less than 40 000 nm2 and an average aggregate diameter (ECD) of less than 200 nm, whose core is crystalline and consists of aggregated primary particles of zinc oxide and whose shell surrounds the aggregated zinc oxide primary particles and consists of one or more compounds containing the elements Si and O. Dispersion, coating composition and sunscreen formulation comprise the zinc silicon oxide particles.
摘要翻译： 具有核 - 壳结构的氧化锌颗粒，其Zn / Si比为2至75，原子％/原子％，其Zn，Si和O的分数为至少99重量％，基于锌 具有10至60m 2 / g的BET表面积，10至75nm的平均聚集面积小于40 000nm 2的平均聚集体直径（ECD）的二氧化硅颗粒， 小于200nm，其核心是结晶的，由氧化锌的聚集的初级颗粒组成，并且其外壳围绕聚集的氧化锌一次颗粒，并由含有元素Si和O的一种或多种化合物组成。分散体，涂料组合物和防晒配方 包括氧化锌微粒。
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公开(公告)号：US20060073092A1
公开(公告)日：2006-04-06
申请号：US10522778
申请日：2003-07-07
申请人： Stipan Katusic , Guenther Michael , Peter Kress , Guido Zimmermann , Andreas Gutsch , Geoffrey Varga
发明人： Stipan Katusic , Guenther Michael , Peter Kress , Guido Zimmermann , Andreas Gutsch , Geoffrey Varga
IPC分类号： C01G9/02
CPC分类号： B82Y30/00 , A61K8/27 , A61Q17/04 , C01G9/00 , C01G9/03 , C01P2002/50 , C01P2004/54 , C01P2004/64 , C01P2006/12 , C01P2006/40 , C09C1/04 , C09C1/043 , Y10T428/2982 , Y10T428/2991 , Y10T428/2993 , Y10T428/2995 , Y10T428/2996
摘要： Pyrogenically prepared, doped zinc oxide powder, wherein the doping component comprises at least one oxide from the group aluminum, gallium, indium, germanium, tin and is present in the doped zinc oxide powder in an amount of from 0.005 to 15 wt. %, and wherein the doped zinc oxide powder is in the form of aggregates of primary particles having a mean maximum diameter of from 30 to 400 nm. It is prepared by oxidation from zinc powder and at least one doping agent, wherein the process zones vaporisation, nucleation, oxidation and quenching are passed through and the doping agent is metered in in the nucleation zone, in which the temperature is below the boiling temperature of zinc. The doped zinc oxide powder can be used in electrically conductive lacquers and coatings.
摘要翻译： 热解制备的掺杂氧化锌粉末，其中所述掺杂组分包括来自铝，镓，铟，锗，锡的至少一种氧化物，并且掺杂的氧化锌粉末以0.005至15重量％的量存在。 ％，并且其中所述掺杂的氧化锌粉末是平均最大直径为30至400nm的初级颗粒的聚集体的形式。 它是通过从锌粉和至少一种掺杂剂的氧化制备的，其中过程区蒸发，成核，氧化和淬灭通过，掺杂剂在成核区计量，其中温度低于沸点 的锌。 掺杂的氧化锌粉末可用于导电漆和涂层。
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公开(公告)号：US07235298B2
公开(公告)日：2007-06-26
申请号：US10522778
申请日：2003-07-07
申请人： Stipan Katusic , Guenther Michael , Peter Kress , Guido Zimmermann , Andreas Gutsch , Geoffrey J. Varga
发明人： Stipan Katusic , Guenther Michael , Peter Kress , Guido Zimmermann , Andreas Gutsch , Geoffrey J. Varga
IPC分类号： B32B5/66
CPC分类号： B82Y30/00 , A61K8/27 , A61Q17/04 , C01G9/00 , C01G9/03 , C01P2002/50 , C01P2004/54 , C01P2004/64 , C01P2006/12 , C01P2006/40 , C09C1/04 , C09C1/043 , Y10T428/2982 , Y10T428/2991 , Y10T428/2993 , Y10T428/2995 , Y10T428/2996
摘要： Pyrogenically prepared, doped zinc oxide powder, wherein the doping component comprises at least one oxide from the group aluminum, gallium, indium, germanium, tin and is present in the doped zinc oxide powder in an amount of from 0.005 to 15 wt. %, and wherein the doped zinc oxide powder is in the form of aggregates of primary particles having a mean maximum diameter of from 30 to 400 nm. It is prepared by oxidation from zinc powder and at least one doping agent, wherein the process zones vaporisation, nucleation, oxidation and quenching are passed through and the doping agent is metered in in the nucleation zone, in which the temperature is below the boiling temperature of zinc. The doped zinc oxide powder can be used in electrically conductive lacquers and coatings.
摘要翻译： 热解制备的掺杂氧化锌粉末，其中所述掺杂组分包括来自铝，镓，铟，锗，锡的至少一种氧化物，并且掺杂的氧化锌粉末以0.005至15重量％的量存在。 ％，并且其中所述掺杂的氧化锌粉末是平均最大直径为30至400nm的初级颗粒的聚集体的形式。 它是通过从锌粉和至少一种掺杂剂的氧化制备的，其中过程区蒸发，成核，氧化和淬灭通过，掺杂剂在成核区计量，其中温度低于沸点 的锌。 掺杂的氧化锌粉末可用于导电漆和涂层。
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8.发明申请Zinc oxide powder aggregates present in circular ellipsoidal, linear and branched form 有权氧化锌粉末聚集体存在于圆形椭圆形，直链和支链形式中公开(公告)号：US20070037699A1
公开(公告)日：2007-02-15
申请号：US10572936
申请日：2004-09-02
申请人： Stipan Katusic , Michael Kramer , Peter Kress , Horst Miess , Guido Zimmermann , Peter Albers
发明人： Stipan Katusic , Michael Kramer , Peter Kress , Horst Miess , Guido Zimmermann , Peter Albers
IPC分类号： B01J23/00
CPC分类号： C09C1/043 , C01G9/03 , C01P2004/04 , C01P2006/11
摘要： Pyrogenically prepared zinc oxide powder having a BET surface area of from 10 to 200 m2/g, which is in the form of aggregates, the aggregates being composed of particles having different morphologies, and 0-10% of the aggregates being in a circular form, 30-50% being in an ellipsoidal form, 30-50% being in a linear form and 20-30% being in a branched form. It is prepared by reacting a starting mixture containing zinc vapour, a combustible gas and steam or a mixture of steam and carbon dioxide in a flame with an oxygen-containing gas in an oxidation zone, cooling the hot reaction mixture in a quenching zone and separating the solid material from the gas stream, the amount of oxygen in the oxidation zone being greater than the amount necessary for the complete oxidation of the combustible gas and the zinc vapour. The zinc oxide powder can be used as a constituent of sun protection compositions for protection against UV radiation.
摘要翻译： 热解制备的氧化锌粉末，其BET表面积为10至200m 2 / g，其为聚集体形式，聚集体由具有不同形态的颗粒组成，并且0-10％ 的聚集体为圆形，30-50％为椭圆形，30-50％为直线形式，20-30％为分支形式。 通过在氧化区中将含有锌蒸汽，可燃气体和蒸汽或蒸汽和二氧化碳的混合物在火焰中与含氧气体的起始混合物反应制备，在淬火区域中冷却热反应混合物并分离 来自气流的固体材料，氧化区中的氧的量大于可燃气体和锌蒸汽的完全氧化所需的量。 氧化锌粉末可用作防紫外线辐射防晒组合物的组分。
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公开(公告)号：US20110244387A1
公开(公告)日：2011-10-06
申请号：US13133316
申请日：2009-11-09
CPC分类号： C01B33/18 , C01P2006/12 , C09C1/3081
摘要： Fumed silicon dioxide powder with a BET surface area of 20 to 35 m2/g, characterized in that a) the number-based median particle diameter is 60 to 150 nm, and b) the proportion of particles with a diameter of 200 nm or more is at most 10%, and c) the proportion of particles with a diameter of up to 60 nm is at most 20%, based in each case on the total number of particles.
摘要翻译： BET表面积为20〜35m 2 / g的煅制二氧化硅粉末，其特征在于a）数均中值粒径为60〜150nm，b）直径为200nm以上的粒子的比例 至多为10％，c）直径高达60nm的颗粒的比例至多为20％，基于每种情况下的颗粒总数。
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公开(公告)号：US20100092411A1
公开(公告)日：2010-04-15
申请号：US12445474
申请日：2007-08-01
申请人： Stipan Katusic , Guido Zimmermann , Juergen Meyer
发明人： Stipan Katusic , Guido Zimmermann , Juergen Meyer
IPC分类号： A61K8/27
CPC分类号： C09C1/043 , B82Y30/00 , C01P2004/04 , C01P2004/10 , C01P2004/62 , C01P2004/64 , C01P2006/11 , C01P2006/12 , C01P2006/80
摘要： Hydrophobic zinc oxide powder in the form of partially or completely coated aggregates of zinc oxide primary particles having a carbon content of from 0.4 to 1.5% by weight, based on the hydrophobic zinc oxide powder, and a BET surface area of from 25 to 100 m2/g, where the coated aggregates are present to 0 to
摘要翻译： 氧化锌一次粒子的部分或完全涂覆的聚集体形式的疏水性氧化锌粉末，基于疏水性氧化锌粉末，碳含量为0.4至1.5重量％，BET表面积为25-100平方米 / g，其中涂覆的聚集体以圆形形式存在0至<10％，以椭圆形形式存在为15至<30％，以线形形式为<30％，分支形式为40至<70％，以及 不同形式的总和为15 100％，并且涂层包含化学键合的具有1至20个碳原子的直链和/或支链单烷基甲硅烷基硅烷基和/或二烷基甲硅烷基Si-（烷基）2。
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