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    Butadiene-based rubber composition
    1.
    发明授权
    Butadiene-based rubber composition 失效
    丁二烯橡胶组合物

    公开(公告)号：US4824908A

    公开(公告)日：1989-04-25

    申请号：US29558

    申请日：1987-03-24

    申请人： Fumio Tsutsumi ,  Mitsuhiko Sakakibara ,  Noboru Shimada ,  Yoshihisa Fujinaga ,  Noboru Oshima ,  Tatsuro Hamada ,  Tatsuo Fujimaki

    发明人： Fumio Tsutsumi ,  Mitsuhiko Sakakibara ,  Noboru Shimada ,  Yoshihisa Fujinaga ,  Noboru Oshima ,  Tatsuro Hamada ,  Tatsuo Fujimaki

    IPC分类号： B60C1/00 ,  C08C19/44 ,  C08L9/00 ,  C08L21/00 ,  C08L7/00 ,  C08L9/06 ,  C08L53/02

    CPC分类号： B60C1/0025 ,  B60C1/0016 ,  C08C19/44 ,  C08L9/00 ,  Y10S152/905 ,  Y10T152/10846

    摘要： A butadiene-based rubber composition is disclosed, which contains not less than 20% by weight of a butadiene-based homopolymer or copolymer having a glass transition temperature (Tg) of not less than -105.degree. C., but less than -70.degree. C. and a Mooney viscosity (ML.sub.1+4, 100.degree. C.) of 10 to 150. The butadiene-based homopolymer or copolymer is obtained by polymerizing butadiene or random-copolymerizing butadiene with at least one kind of a monomer selected from the group consisting of another conjugated diene and an aromatic vinyl compound, and then reacting polymerization-active terminals thereof with an isocyanate compound and/or an isothiocyanate compound. The butadiene-based rubber composition has excellent resilience, fracture strength, and wear resistance as a vulcanizate as well as excellent processability as an unvulcanized rubber, and can be used as tire applications such as tire treads, undertreads, sidewalls, bead portions, etc. as well as vibration insulating rubber, hoses, belts and other industrial articles.

    摘要翻译： 公开了一种丁二烯基橡胶组合物，其含有不少于20重量％的玻璃化转变温度（Tg）不低于-105℃但小于-70℃的丁二烯基均聚物或共聚物 丁二烯类均聚物或共聚物是通过将丁二烯或无规共聚丁二烯与至少一种选自以下的单体进行聚合而获得的：丁二烯类均聚物或共聚物 由另一种共轭二烯和芳族乙烯基化合物组成，然后使其聚合活性末端与异氰酸酯化合物和/或异硫氰酸酯化合物反应。 丁二烯类橡胶组合物作为硫化橡胶具有优异的回弹性，断裂强度和耐磨性以及作为未硫化橡胶的优异加工性，并且可以用作轮胎胎面，胎面，胎侧，胎圈部等轮胎用途。 以及隔振橡胶，软管，皮带等工业用品。

    Rubber composition for use in tire tread comprising a rubber component, carbon black and process oil
    2.
    发明授权
    Rubber composition for use in tire tread comprising a rubber component, carbon black and process oil 失效
    用于轮胎胎面的橡胶组合物，其包含橡胶组分，炭黑和加工油

    公开(公告)号：US4791178A

    公开(公告)日：1988-12-13

    申请号：US117346

    申请日：1987-10-27

    申请人： Tatsuo Fujimaki ,  Noboru Oshima

    发明人： Tatsuo Fujimaki ,  Noboru Oshima

    IPC分类号： C08L7/00 ,  B60C1/00 ,  C08K3/00 ,  C08L9/06 ,  C08L21/00 ,  C08L33/00 ,  C08L33/02 ,  C08C19/20 ,  C08F8/34

    CPC分类号： C08K3/04 ,  B60C1/0016 ,  C08K5/01 ,  C08L9/06 ,  C08L2205/02 ,  C08L9/08 ,  Y10S152/905

    摘要： A rubber composition for use in tire is disclosed which contains at least 30% by weight, relative to the entire rubber component, of a conjugated diene-monovinyl aromatic hydrocarbon copolymer which uses an organic lithium compound as an initiator. A percentage of vinyl bonds in conjugated diene units in the copolymer molecules is from 50 to 95% and the content of the monovinyl aromatic hydrocarbon units is from 10 to 50% by weight. As physical properties of the vulcanized rubber of the rubber composition, aromatic hydrocarbon copolymer, 200% tensile modulus is from 5 to 50 kgf/cm.sup.2 and a temperture integrated value of a loss tangent, ##EQU1## is from 16 to 56. The tread rubber composition is suitable for a tread of high performance tires, and is excellent in fracture strength, thermal resistance, wear resistance, and road gripping property.

    摘要翻译： 公开了一种用于轮胎的橡胶组合物，其相对于整个橡胶组分含有至少30重量％的使用有机锂化合物作为引发剂的共轭二烯 - 单乙烯基芳族烃共聚物。 共聚物分子中共轭二烯单元中的乙烯基键的百分比为50〜95％，单乙烯基芳烃单元的含量为10〜50重量％。 作为橡胶组合物的硫化橡胶的物理性质，芳族烃共聚物的200％拉伸弹性模量为5〜50kgf / cm 2，损耗角正切值的温度积分值为16〜56。胎面橡胶 组合物适用于高性能轮胎的胎面，并且断裂强度，耐热性，耐磨性和道路抓地性优异。

    Vulcanized rubber composition
    5.
    发明授权
    Vulcanized rubber composition 失效
    硫化橡胶组合物

    公开(公告)号：US5011888A

    公开(公告)日：1991-04-30

    申请号：US449308

    申请日：1989-12-06

    申请人： Fumio Tsutsumi ,  Akihiko Morikawa ,  Mitsuhiko Sakakibara ,  Noboru Oshima ,  Tatsuro Hamada ,  Tatsuo Fujimaki ,  Masayuki Ohashi

    发明人： Fumio Tsutsumi ,  Akihiko Morikawa ,  Mitsuhiko Sakakibara ,  Noboru Oshima ,  Tatsuro Hamada ,  Tatsuo Fujimaki ,  Masayuki Ohashi

    IPC分类号： C08L9/06 ,  B60C1/00 ,  C08F297/04 ,  C08G18/69 ,  C08L21/00 ,  C08L53/00 ,  C08L53/02

    CPC分类号： C08L53/02 ,  B60C1/0016 ,  C08G18/69 ,  C08L21/00 ,  C08G2380/00

    摘要： A rubber composition is disclosed which contains not less than 20% by weight in a rubber component of a block copolymer composed of polymer or copolymer block units (A) and a random copolymer block units (B). The polymer or copolymer block units (A) are obtained by singly polymerizing a conjugated diolefine or copolymerizing the conjugated diolefine and a monovinyl aromatic hydrocarbon with use of a lithium initiator and contains not more than 10% by weight of the bound monovinyl aromatic hydrocarbon. The random copolymer block unit (B) are obtained by copolymerizing the conjugated diolefine and the monovinyl aromatic hydrocarbon and contain 15 to 80% by weight of the bound monovinyl aromatic hydrocarbon. In the block copolymer, (i) the block copolymer contains not less than 10% by weight of each of the block units (A) and the block units (B); (ii) the total content of the bound monovinyl aromatic hydrocarbon is from 10 to 40% by weight; (iii) the average content of the vinyl bonds in the conjugated diolefine portions is from 20 to 70%; and (iv) polymerizable terminals of the block copolymer are reacted with an isocyanate compound.

    摘要翻译： 公开了在由聚合物或共聚物嵌段单元（A）和无规共聚物嵌段单元（B）组成的嵌段共聚物的橡胶组分中不少于20重量％的橡胶组合物。 聚合物或共聚物嵌段单元（A）是通过使共轭二烯烃单独聚合或使用锂引发剂共轭共轭二烯和单乙烯基芳族烃而得到的，并且含有不超过10重量％的结合的单乙烯基芳烃。 无规共聚物嵌段单元（B）通过使共轭二烯烃和单乙烯基芳族烃共聚而得到，并含有15〜80重量％的结合的单乙烯基芳烃。 在嵌段共聚物中，（i）嵌段共聚物含有不少于块单元（A）和嵌段单元（B）的10重量％。 （ii）结合的单乙烯基芳烃的总含量为10〜40重量％ （iii）共轭二烯烃部分中的乙烯基键的平均含量为20〜70％。 和（iv）嵌段共聚物的可聚合端与异氰酸酯化合物反应。

    Rubber composition comprising a styrene-butadiene block copolymer having two kinds of blocks
    6.
    发明授权
    Rubber composition comprising a styrene-butadiene block copolymer having two kinds of blocks 失效
    包含具有两种嵌段的苯乙烯 - 丁二烯嵌段共聚物的橡胶组合物

    公开(公告)号：US4782119A

    公开(公告)日：1988-11-01

    申请号：US769923

    申请日：1985-08-27

    申请人： Fumio Tsutsumi ,  Akio Iakashima ,  Mitsuhiko Sakakibara ,  Noboru Oshima ,  Tatsuo Fujimaki ,  Yoshiyuki Morimoto

    发明人： Fumio Tsutsumi ,  Akio Iakashima ,  Mitsuhiko Sakakibara ,  Noboru Oshima ,  Tatsuo Fujimaki ,  Yoshiyuki Morimoto

    IPC分类号： C08L7/00 ,  B60C1/00 ,  C08F297/04 ,  C08L1/00 ,  C08L9/06 ,  C08L21/00 ,  C08L23/00 ,  C08L27/00 ,  C08L51/00 ,  C08L51/02 ,  C08L53/00 ,  C08L53/02 ,  C08L77/00 ,  C08L101/00

    CPC分类号： B60C1/0016 ,  C08F297/044 ,  Y10S525/914

    摘要： A rubber composition containing at least 20% by weight of a styrene-butadiene block copolymer consisting of a block (A) and a block (B) characterized in that: (i) the block (A) is a styrene-butadiene copolymer block having the content of styrene of 10-80% by weight and the average content of the vinyl bonds in the butadiene portion of 30-70% by weight; (ii) the block (B) is a polybutadiene block with the average content of the vinyl bonds in the butadiene portion being not more than 60% by weight (iii) the styrene-butadiene block copolymer contains at least 20% by weight of each of the block (A) and the block (B); (iv) the average content of the vinyl bonds in the butadiene portion of the block (A) is greater by at least 5% by weight than that of the block (B); (v) the glass transition temperature of the block (A) is higher by at least 30.degree. C. than that of the block (B); (vi) the whole content of the bound styrene in the above block copolymer is 5-40% by weight; (vii) the ratio Mw/Mn between the weight average molecular weight Mw and the number average molecular weight Mn of the block copolymer is 1.8-5.0 when calculated as polystyrene according to the gel permeation chromatogram; and (viii) the Mooney's viscosity (ML.sub.1+4.sup.100.degree. C.) of the block copolymer is 20-150.

    摘要翻译： 一种含有至少20重量％由嵌段（A）和嵌段（B）组成的苯乙烯 - 丁二烯嵌段共聚物的橡胶组合物，其特征在于：（i）嵌段（A）是苯乙烯 - 丁二烯共聚物嵌段，其具有 苯乙烯含量为10-80重量％，丁二烯部分中乙烯基键的平均含量为30-70重量％; （ii）嵌段（B）是丁二烯部分中乙烯基键的平均含量不大于60重量％的聚丁二烯嵌段（iii）苯乙烯 - 丁二烯嵌段共聚物含有至少20重量％ （A）和块（B）; （iv）嵌段（A）的丁二烯部分中的乙烯基键的平均含量比块（B）的平均含量高至少5重量％。 （v）嵌段（A）的玻璃化转变温度比嵌段（B）的玻璃化转变温度高至少30℃; （vi）上述嵌段共聚物中的结合苯乙烯的全部含量为5-40重量％ （vii）根据凝胶渗透色谱法计算，当以聚苯乙烯计算时，嵌段共聚物的重均分子量Mw与数均分子量Mn之比Mw / Mn为1.8-5.0; 和（viii）嵌段共聚物的门尼粘度（ML1 + 4100℃）为20-150℃。

    Butadiene copolymer rubber composition
    8.
    发明授权
    Butadiene copolymer rubber composition 失效
    丁二烯共聚物橡胶组合物

    公开(公告)号：US5164450A

    公开(公告)日：1992-11-17

    申请号：US582810

    申请日：1990-09-14

    申请人： Fumio Tsutsumi ,  Mitsuhiko Sakakibara ,  Yoshihisa Fujinaga ,  Noboru Oshima ,  Tatsuo Fujimaki

    发明人： Fumio Tsutsumi ,  Mitsuhiko Sakakibara ,  Yoshihisa Fujinaga ,  Noboru Oshima ,  Tatsuo Fujimaki

    IPC分类号： C08C19/44 ,  C08F236/10 ,  C08L9/06

    CPC分类号： C08F236/10 ,  C08C19/44 ,  C08L9/06

    摘要： Disclosure is herein made of a rubber composition containing at least 30% by weight of a butadiene copolymer which is characterized in that: (i) the content of vinyl bonds in a polybutadiene portion is from 40 to 70%; (ii) the content of bound vinyl aromatic compound is from 25 to 50% by weight: (iii) the ratio Mw/Mn between the weight average molecular weight (Mw) and the number average molecular weight (Mn) when calculated as polystyrene according to the gel permeation chromatograph (GPC) method is from 1.8 to 5, and the distribution of the molecular weight is unimodal; (iv) the rate of the copolymer having the weight average molecular weight of not more than 100,000 when calculated as polystyrene is from 10 to 30%; (v) the rate of the copolymer having the weight average molecular weight of not less than 2,000,000 when calculated as polystyrene is from 10 to 30%; and (vi) the Mooney viscosity (ML.sub.1+4 100.degree. C.) is from 20 to 100.

    摘要翻译： 本文公开了含有至少30重量％的丁二烯共聚物的橡胶组合物，其特征在于：（i）聚丁二烯部分中的乙烯基键含量为40至70％; （ii）结合的乙烯基芳族化合物的含量为25〜50重量％：（iii）以聚苯乙烯换算时的重均分子量（Mw）与数均分子量（Mn）之比Mw / Mn 凝胶渗透色谱（GPC）法为1.8〜5，分子量分布为单峰; （iv）当以聚苯乙烯计算时，重均分子量不大于100,000的共聚物的比例为10-30％; （v）当以聚苯乙烯计算时，重均分子量不小于200万的共聚物的比例为10至30％; 和（vi）门尼粘度（ML1 + 4 100℃）为20-100。

    Styrene-butadiene copolymer rubber composition
    9.
    发明授权
    Styrene-butadiene copolymer rubber composition 失效
    苯乙烯 - 丁二烯共聚物橡胶组合物

    公开(公告)号：US4575534A

    公开(公告)日：1986-03-11

    申请号：US597635

    申请日：1984-04-06

    申请人： Noboru Oshima ,  Isamu Shimizu ,  Mikio Takeuchi ,  Tatsuo Fujimaki ,  Shinsuke Yamaguchi

    发明人： Noboru Oshima ,  Isamu Shimizu ,  Mikio Takeuchi ,  Tatsuo Fujimaki ,  Shinsuke Yamaguchi

    IPC分类号： C08L7/00 ,  C08C19/44 ,  C08L9/06 ,  C08L21/00 ,  C08L23/00 ,  C08L51/00 ,  C08L51/02 ,  C08L77/00 ,  C08L101/00 ,  C08L9/00 ,  C08L53/00

    CPC分类号： C08C19/44 ,  C08L21/00

    摘要： Disclosed herein is a rubber composition comprising at least 20% by weight of styrene-butadiene copolymer based on the total weight of the rubber content. The styrene-butadiene copolymer is obtained by randomly copolymerizing styrene with 1,3-butadiene in a hydrocarbon solvent in the presence of an organolithium compound as an initiator and then subjecting to a coupling reaction with a polyfunctional coupling agent, and contains 30-70% by weight of branched polymers therein, and has the following properties:(a) a content of bound styrene in the copolymer 3-15% by weight;(b) a content of vinyl bonds contained in the butadiene units is 15-30% by weight;(c) a Mooney viscosity (ML.sub.1+4.sup.100.degree. C.) is 15-50; and(d) a molecular weight distribution of the copolymer is bimodal at a ratio Mw/Mn of 1.4-2.2 in which Mw is a weight-average molecular weight and Mn is a number-average molecular weight.

    摘要翻译： 本文公开了一种橡胶组合物，其包含基于橡胶含量的总重量的至少20重量％的苯乙烯 - 丁二烯共聚物。 苯乙烯 - 丁二烯共聚物通过在有机锂化合物作为引发剂的存在下在烃溶剂中将苯乙烯与1,3-丁二烯无规共聚而得到，然后与多官能偶联剂进行偶联反应，并含有30-70％ （a）共聚物中结合苯乙烯含量3-15％（重量）; （b）丁二烯单元中所含的乙烯基键的含量为15〜30重量％ （c）门尼粘度（ML1 + 4100℃）为15-50; 和（d）共聚物的分子量分布是双峰的，比率＆upbar＆Mw /＆lt;上升＆Mn为1.4-2.2，其中＆Upbar＆Mw为重均分子量，＆lt;上升＆Mn为数均分子量。

    Rubber composition for high-performance tire tread
    10.
    发明授权
    Rubber composition for high-performance tire tread 失效
    用于高性能轮胎胎面的橡胶组合物

    公开(公告)号：US4866131A

    公开(公告)日：1989-09-12

    申请号：US093156

    申请日：1987-09-02

    申请人： Tatsuo Fujimaki ,  Noboru Oshima

    发明人： Tatsuo Fujimaki ,  Noboru Oshima

    IPC分类号： C08L7/00 ,  C08L9/06 ,  C08L21/00 ,  C08L23/00 ,  C08L33/00 ,  C08L33/02 ,  C08L51/00 ,  C08L51/02 ,  C08L77/00 ,  C08L101/00

    CPC分类号： C08L9/02 ,  C08L11/00 ,  C08L21/00 ,  C08L9/06 ,  C08K5/01

    摘要： Disclosed is a novel rubber composition for the treads of high-performance tires including racing tires. The elastomer component of the rubber composition consists essentially of 10-60 wt % of a low molecular weight copolymer of an aliphatic diene, e.g. butadiene, and an aromatic vinyl compound, e.g. styrene, and the balance of a conventional diene rubber such as a high styrene styrene-butadiene rubber. The copolymer is the product of solution copolymerization reaction of the aliphatic and aromatic monomers in a hydrocarbon solvent using an organic lithium compound as the initiator, and the molecular weight of the copolymer is from about 2000 to about 50000. The rubber composition provides very high road gripping ability and is sufficiently high also in rupture strength, heat resistance and wear resistance.

    摘要翻译： 公开了一种用于高性能轮胎胎面的新型橡胶组合物，包括赛车轮胎。 橡胶组合物的弹性体组分基本上由10-60重量％的低分子量脂族二烯烃共聚物组成。 丁二烯和芳族乙烯基化合物，例如 苯乙烯，以及常规的二烯橡胶如高苯乙烯 - 丁二烯橡胶的余量。 共聚物是使用有机锂化合物作为引发剂的脂族和芳族单体在烃溶剂中的溶液共聚反应的产物，共聚物的分子量为约2000至约50000.橡胶组合物提供非常高的路面 并且在断裂强度，耐热性和耐磨性方面也足够高。