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1.发明授权Addition type imide resin prepolymer, manufacturing method thereof, prepreg and laminate thereof 失效加成型酰亚胺树脂预聚物，其制造方法，预浸料及其层压体
公开(公告)号：US5136015A
公开(公告)日：1992-08-04
申请号：US506956
申请日：1990-04-10
申请人： Tatsuo Yonemoto , Masahiro Matsumura , Yoshihisa Sugawa , Eiichiro Saito , Hiroshi Yamamoto , Keiko Kashihara
发明人： Tatsuo Yonemoto , Masahiro Matsumura , Yoshihisa Sugawa , Eiichiro Saito , Hiroshi Yamamoto , Keiko Kashihara
CPC分类号： C08J5/24 , B32B27/04 , C08G73/121 , H05K1/0346 , C08J2379/08 , Y10T428/31721
摘要： An addition type imide resin prepolymer is obtained by a reaction of unsaturated bisimide of 1.0 mol to diamine of 0.25 to 0.43 mol and an addition of polyamine having three or more benzene rings. The prepolymer is thereby made to contain substantially no unreacted diamine component which affects human body of operators, and to have remarkably excellent heat resistance and adhesive properties, while effective to restrain a production of any component of a molecular weight exceeding 15,000.
摘要翻译： 通过使1.0摩尔的不饱和双酰亚胺与二胺的摩尔比为0.25〜0.43摩尔，加入具有3个以上苯环的多胺，可以得到加成型酰亚胺树脂预聚物。 从而使预聚物基本上不含有影响操作者的人体的未反应的二胺成分，并且具有显着优异的耐热性和粘合性，同时有效地抑制任何分子量超过15,000的成分的生产。
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2.发明授权Process for producing unsaturated mono and dicarboxylic acid imide compound 失效制备不饱和单羧酸和二羧酸酰亚胺化合物的方法
公开(公告)号：US5112989A
公开(公告)日：1992-05-12
申请号：US325807
申请日：1989-03-20
IPC分类号： C07D207/44 , C07D207/448 , C07D207/452 , C07D209/48 , C08F22/36 , C08F22/40
CPC分类号： C07D207/448 , C07D207/452
摘要： A process for producing an unsaturated dicarboxylic acid imide compound of formula (I): ##STR1## wherein D represents a divalent organic group having at least one carbon/carbon double bond; R.sup.1 represents an n-valent organic group having at least one carbon atom; and n is an integer of 1 or above, which comprises reacting an unsaturated amide acid compound of formula (II): ##STR2## wherein D, R.sup.1, and n are as defined above, with an orthoester of formula (III): ##STR3## wherein R.sup.2 and R.sup.3, which may be the same or different, each represents a monovalent organic group having at least one carbon atom, to form an unsaturated dicarboxylic acid amide acid ester compound of formula (IV): ##STR4## wherein D, R.sup.1, R.sup.3, and n are as defined above, and then imidating the compound of formula (IV).
摘要翻译： 制备式（I）的不饱和二羧酸酰亚胺化合物的方法：其中D表示具有至少一个碳/碳双键的二价有机基团; R1表示具有至少一个碳原子的n价有机基团; 其中n为1以上的整数，其包括使式（II）的不饱和酰胺酸化合物：其中D，R1和n如上所定义的式（II）与式（III）的原酸酯反应， ：R2-C [-OR3] 3（III）其中R2和R3可以相同或不同，表示具有至少一个碳原子的一价有机基团，形成式（I）的不饱和二羧酸酰胺酸酯化合物 （IV）：其中D，R1，R3和n如上所定义，然后酰亚胺化式（IV）化合物。
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公开(公告)号：US07684041B2
公开(公告)日：2010-03-23
申请号：US11795707
申请日：2006-03-29
IPC分类号： G01J3/50
CPC分类号： G01J3/50 , G01J3/0208 , G01J3/0291 , G01J3/46 , G01J3/463 , G01N21/25 , G01N33/36
摘要： A color inspection system capable of making a determination on pass or failure with accuracy equivalent to that for the case of a visual inspection even in the case of inspecting various textile products as measurement targets, such as raised cloth, cloth with printed patterns such as a marbled pattern, moire pattern and detailed pattern is provided. With the color inspection system, an illuminant is set to shine a light on the surface of a textile product placed on the top surface of a measuring platform to thereby make measurements from a direction at an angle of 45 degrees from the surface of a measuring region of the textile product by use of a spectroradiometer of a measuring unit. The spectroradiometer is provided with a wide range lens attached thereto to thereby expand a measuring region. The results of measurement by the spectroradiometer are inputted to an information processor of a determination unit. The information processor computes color values for the whole measuring region to be compared with standard color values stored in a memory to thereby make a determination on pass or fail.
摘要翻译： 即使在检查作为测量对象的各种纺织品的情况下，即使是具有印刷图案的布等布料也能够进行与目视检查相同的准确度的通过或者失败的颜色检查系统。 提供大理石图案，莫尔图案和详细图案。 通过颜色检查系统，设置发光体以将光照射在放置在测量平台顶表面上的纺织品的表面上，从而从与测量区域的表面成45度角的方向进行测量 的纺织品通过使用测量单元的光谱辐射计。 该分光辐射计设置有附接到其上的宽范围透镜，从而扩大测量区域。 通过光谱辐射计的测量结果被输入到确定单元的信息处理器。 信息处理器计算要与存储在存储器中的标准颜色值进行比较的整个测量区域的颜色值，从而进行通过或失败的确定。
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4.发明授权
公开(公告)号：US5633042A
公开(公告)日：1997-05-27
申请号：US654168
申请日：1996-05-28
申请人： Yoshihiko Nakamura , Masahiro Matsumura , Yasuo Fukuhara , Yukio Hatta , Masaharu Yamamoto , Makizi Miyao , Kiyohiro Nagao , Takayuki Fukuda , Hiroshi Toshima , Shigekazu Takanohashi , Akihiro Atsumi
发明人： Yoshihiko Nakamura , Masahiro Matsumura , Yasuo Fukuhara , Yukio Hatta , Masaharu Yamamoto , Makizi Miyao , Kiyohiro Nagao , Takayuki Fukuda , Hiroshi Toshima , Shigekazu Takanohashi , Akihiro Atsumi
CPC分类号： C08J3/226 , B29B15/122 , B29C70/50 , C08J5/24 , B29C35/08 , C08J2363/00 , C08J2463/00
摘要： In a process for manufacturing a prepreg for use as an electrically insulating material, a main epoxy resin composition and a subsidiary resin composition containing a hardener which have been separately filtered and metered are quickly mixed into a mixture resin composition, a reinforcing member is coated with a uniformly thin film of the mixture resin composition by a die coater under specific temperature, average residence time and low shear conditions, the coated reinforcing member is heated in non-contact manner by an infrared ray heater to have the member impregnated with the resin composition of the film, the member is further heated in non-contact manner by a floating dryer to have the resin composition semi-hardened, and the member is unified through compaction rolls, whereby the prepreg in the form of a sheet-shaped fiber reinforced composite material is continuously manufactured.
摘要翻译： 在制造用作电绝缘材料的预浸料的方法中，将主要环氧树脂组合物和含有已分别过滤和计量的固化剂的辅助树脂组合物快速混合到混合树脂组合物中，加强构件涂覆 通过模具涂布机在特定温度，平均停留时间和低剪切条件下的混合树脂组合物的均匀薄膜，通过红外线加热器以非接触的方式加热涂覆的加强部件，以使该部件浸渍有树脂组合物 通过浮动干燥器以非接触方式进一步加热构件，使树脂组合物半硬化，并且通过压实辊将构件一体化，由此形成片状纤维增强复合材料形式的预浸料 材料连续制造。
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5.发明授权Polyimide prepolymer composition from unsaturated bisimide and diamine containing unreacted reactants 失效不饱和双酰亚胺和含有未反应的反应物的二胺的聚酰亚胺预聚物组合物
公开(公告)号：US4680377A
公开(公告)日：1987-07-14
申请号：US805989
申请日：1985-12-05
IPC分类号： B32B15/08 , B32B15/088 , B32B27/04 , C08G73/00 , C08G73/12 , C08J5/24 , C08K5/18 , C08K5/3415 , C08L79/08 , H01L23/538 , H05K1/03 , C08G73/10
CPC分类号： C08J5/24 , C08G73/121 , C08L79/08 , C08J2379/08 , H05K1/0346
摘要： Superior polyimide prepolymers particularly suitable for fabrication of multi-layer printed boards are produced by reacting unsaturated bisimides with diamines to consist essentially of 41-55% of unreacted reactants, 39-54% of components having a molecular weight of between 400 and 15,000, and 3.0-6.8% of components having a molecular weight of more than 15,000. The resulting prepolymers enable the preparation of their solution having enough working life for successfully impregnating a given substrate therewith in the preparation of prepregs. The prepregs, prepared from the above prepolymers in such a way as to contain within the resin content thereof 29-35% of unreacted reactants, 51-65% of the components having a molecular weight of between 400 and 15,000, and 5-14% of the components having a molecular weight of more than 15,000, allow the fabrication of laminate products with remarkable dimension stability under a low molding pressure to eliminate the presence of voids in the products, in addition to that the prepregs ensure a high bond strength as well as elongated working life which is responsible for prevention of a blister in the finished laminate and for easy control of the laminate forming process.
摘要翻译： 特别适用于制造多层印刷电路板的优异的聚酰亚胺预聚物是通过使不饱和双酰亚胺与二胺反应制得的，基本上由41-55％的未反应的反应物组成，39-54％的分子量为400至15,000的组分，以及 3.0-6.8％的分子量大于15,000的组分。 得到的预聚物使得它们的溶液的制备具有足够的使用寿命，用于在预浸料的制备中成功地浸渍给定的基材。 由上述预聚物制备的预浸料以含有29-35％未反应的反应物的树脂含量，51-65％的分子量为400至15,000的组分和5-14％ 的分子量大于15,000的组分，允许在低成型压力下制造具有显着尺寸稳定性的层压产品，以消除产品中空隙的存在，此外，预浸料还确保了高的粘结强度 作为延长的工作寿命，其负责防止成品层压体中的起泡，并且易于控制层压体形成过程。
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公开(公告)号：US20090190132A1
公开(公告)日：2009-07-30
申请号：US11795707
申请日：2006-03-29
CPC分类号： G01J3/50 , G01J3/0208 , G01J3/0291 , G01J3/46 , G01J3/463 , G01N21/25 , G01N33/36
摘要： The objective of the invention is to provide a color inspection system capable of making determination on pass or failure with accuracy equivalent to that for the case of visual inspection even in the case of inspecting various textile products as measurement targets, such as a raised cloth, cloth with printed patterns such as marbled pattern, moire pattern and detailed pattern, and so forth. With a color inspection system, an illuminant is set to shine light on the surface of a textile product M placed on the top surface of a measuring platform to thereby make measurements from a direction at an angle of 45 degrees from the surface of a measuring region of the textile product M by use of a spectroradiometer of a measuring unit. The spectroradiometer is provided with a wide range lens attached thereto to thereby expand a measuring region. The results of measurement by the spectroradiometer are inputted to an information processor of a determination unit. The information processor computes color values for the whole measuring region to be compared with standard color values stored in a memory to thereby make determination on pass or fail.
摘要翻译： 本发明的目的是提供一种能够在对作为测量对象的各种纺织产品进行检查的情况下，即使在目视检查的情况下的精度等同于通过或者失败的测定的颜色检查系统，例如凸起的布， 具有印刷图案的布，例如大理石图案，莫尔图案和详细图案等。 通过颜色检查系统，设置发光体以将光照射在放置在测量平台的上表面上的纺织品M的表面上，从而从与测量区域的表面成45度角的方向进行测量 的纺织品M通过使用测量单元的光谱辐射计。 该分光辐射计设置有附接到其上的宽范围透镜，从而扩大测量区域。 通过光谱辐射计的测量结果被输入到确定单元的信息处理器。 信息处理器计算要与存储在存储器中的标准色彩值进行比较的整个测量区域的颜色值，从而确定通过或失败。
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公开(公告)号：US06231959B1
公开(公告)日：2001-05-15
申请号：US09225500
申请日：1999-01-06
IPC分类号： B32B1704
CPC分类号： C08G59/686 , C08G59/5086 , C08G59/621 , H05K1/0326 , Y10T428/24994 , Y10T428/31511
摘要： An epoxy resin composition featured in containing, in a matrix of an epoxy resin having more than two epoxy groups in each molecule, a phenolic hardening agent having more than two phenolic hydroxyl groups in each molecule, an organobis(N-dialkylurea) hardening promotion agent, a solvent for the hardening promotion agent, and a guanamine compound, and capable of obtaining a prepreg excellent in the preservation stability and, less causing a solvency errosion (halo phenomenon) due to an infiltration of plating solution along boundaries between a printed copper circuit formed in an inner-layered circuit board and a resin forming the prepreg, is realized.
摘要翻译： 一种环氧树脂组合物，其特征在于，在每个分子中具有多于两个环氧基的环氧树脂的基质中含有每个分子中具有多于两个酚羟基的酚类硬化剂，有机双（N-二烷基脲）硬化促进剂 ，硬化促进剂的溶剂和胍胺化合物，并且能够获得保存稳定性优异的预浸料，并且由于电镀液沿着印刷铜电路之间的边界渗入而导致溶解性腐蚀（光晕现象） 形成在内层电路板和形成预浸料的树脂中。
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公开(公告)号：US5585147A
公开(公告)日：1996-12-17
申请号：US446476
申请日：1995-05-22
CPC分类号： C03C25/1095 , H05K1/0366
摘要： A surface treatment of a glass fabric used for a fiber reinforced composite such as multilayer circuit boards comprises the steps of exposing the glass fabric to an atmospheric pressure plasma of a mixture gas to obtain a plasma-treated surface of the glass fabric, and coating an organosilane compound on the plasma-treated surface. The mixture gas contains as a reaction gas at least one of an oxidative gas and a fluorine-containing gas, and a rare gas as a carrier of the reaction gas. The mixture gas is pre-heated prior to the plasma excitation thereof. When the glass fabric includes an organic compound as a sizing agent, the organic compound can be efficiently removed from the glass fabric by the exposing step. For example, the organosilane compound can be coated on the plasma-treated surface by exposing the plasma-treated surface to a second atmospheric pressure plasma of a second mixture gas containing an organosilane monomer. The surface treatment of the present invention is useful to efficiently produce a multilayer circuit board having excellent adhesion between the glass fabric and a resin, and resistance to CAF (Conductive Anodic Filaments).
摘要翻译： 用于诸如多层电路板的纤维增强复合材料的玻璃织物的表面处理包括将玻璃织物暴露于混合气体的大气压等离子体以获得玻璃织物的等离子体处理表面的步骤， 在等离子体处理的表面上的有机硅烷化合物。 混合气体作为反应气体含有氧化性气体和含氟气体中的至少一种，作为反应气体的载体的稀有气体。 混合气在其等离子体激发之前被预热。 当玻璃织物包含作为施胶剂的有机化合物时，可以通过曝光步骤从玻璃织物中有效地除去有机化合物。 例如，通过将等离子体处理的表面暴露于含有有机硅烷单体的第二混合气体的第二大气压等离子体中，可以将有机硅烷化合物涂覆在等离子体处理的表面上。 本发明的表面处理可有效地制造玻璃织物和树脂之间具有优异粘合性和耐CAF（导电阳极丝）的多层电路板。
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公开(公告)号：US4399257A
公开(公告)日：1983-08-16
申请号：US261908
申请日：1981-05-08
CPC分类号： C08J5/24 , C08K5/00 , C08L63/00 , H05K1/0373 , C08J2363/00 , H05K2201/0239 , H05K2203/121 , Y10T428/31525
摘要： An epoxy resin composition containing one or a mixture thereof selected from the group consisting of poly-p-vinyl phenol and its halides, and a compound selected from the group consisting of the following compounds: (a) Sn salt of organic acid wherein at least one organic group is bonded with Sn atom; (b) alcoxy-containing silane compound represented by the general formula, (R'--).sub.n --Si--(--OR).sub.4-n, wherein R' denotes the alkyl group or the allyl group, R denotes the normal chain or branched alkyl group, and n denotes 0 or an integer of 1-4; and (c) aluminic acid ester represented by the general formula, [Al(OR).sub.3 ].sub.n, wherein n denotes an integer of 1-5, and R denotes the alkyl group or allyl group. The present invention further includes a method for preparing an epoxy resin prepreg using the above epoxy resin composition.
摘要翻译： 含有选自聚对乙烯基苯酚及其卤化物中的一种或其混合物的环氧树脂组合物和选自以下化合物的化合物：（a）有机酸的Sn盐，其中至少 一个有机基团与Sn原子键合; （b）由通式表示的含烷氧基的硅烷化合物（R' - ）n-Si - （ - OR）4-n，其中R'表示烷基或烯丙基，R表示正链或支链 烷基，n表示0或1-4的整数; 和（c）由通式[Al（OR）3] n表示的铝酸酯，其中n表示1-5的整数，R表示烷基或烯丙基。 本发明还包括使用上述环氧树脂组合物制备环氧树脂预浸料的方法。
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