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    OXIDE SUPERCONDUCTING THIN FILM AND METHOD OF MANUFACTURING THE SAME
    1.
    发明申请
    OXIDE SUPERCONDUCTING THIN FILM AND METHOD OF MANUFACTURING THE SAME 审中-公开
    氧化物超导薄膜及其制造方法

    公开(公告)号：US20150105261A1

    公开(公告)日：2015-04-16

    申请号：US14403706

    申请日：2012-05-31

    申请人： Tatsuoki Nagaishi ,  Genki Honda ,  Iwao Yamaguchi ,  Takaaki Manabe ,  Takeshi Hikata ,  Hiroaki Matsui ,  Wakichi Kondo ,  Hirofumi Yamasaki ,  Toshiya Kumagai

    发明人： Tatsuoki Nagaishi ,  Genki Honda ,  Iwao Yamaguchi ,  Takaaki Manabe ,  Takeshi Hikata ,  Hiroaki Matsui ,  Wakichi Kondo ,  Hirofumi Yamasaki ,  Toshiya Kumagai

    IPC分类号： H01B12/06 ,  H01B13/30

    CPC分类号： H01B12/06 ,  H01B13/30 ,  H01L39/2425 ,  H01L39/2483

    摘要： An oxide superconducting thin film wherein nanoparticles functioning as flux pins are dispersed in the film is provided. The oxide superconducting thin film wherein the nanoparticles in the oxide superconducting thin film have a dispersing density of 1020 particles/m3 to 1024 particles/m3 is provided. The oxide superconducting thin film wherein the nanoparticles have a particle diameter of 5 nm to 100 nm is provided. A method of manufacturing an oxide superconducting thin film wherein a predetermined amount of a solution obtained by dissolving nanoparticles functioning as flux pins in a solvent is added to a solution obtained by dissolving an organometallic compound in a solvent to prepare a source material solution for an oxide superconducting thin film, and the source material solution is used to manufacture the oxide superconducting thin film through a coating-pyrolysis process is provided.

    摘要翻译： 提供了其中作为磁通引脚的纳米颗粒分散在膜中的氧化物超导薄膜。 提供氧化物超导薄膜中的氧化物超导薄膜的分散密度为1020粒子/ m 3至1024个/ m3的氧化物超导薄膜。 提供其中纳米颗粒具有5nm至100nm的粒径的氧化物超导薄膜。 一种制造氧化物超导薄膜的方法，其中将通过将用作助熔剂针的纳米颗粒溶解在溶剂中而获得的预定量的溶液加入到通过将有机金属化合物溶解在溶剂中而获得的溶液中，以制备用于氧化物的源材料溶液 超导薄膜和源材料溶液用于通过涂层热解制备氧化物超导薄膜。

    Method for preparing dense, epitaxial metal oxide film
    2.
    发明授权
    Method for preparing dense, epitaxial metal oxide film 失效
    制备密集的外延金属氧化物膜的方法

    公开(公告)号：US06183554B2

    公开(公告)日：2001-02-06

    申请号：US09272564

    申请日：1999-03-19

    申请人： Susumu Mizuta ,  Iwao Yamaguchi ,  Toshiya Kumagai ,  Takaaki Manabe ,  Wakichi Kondo ,  Tadao Shimizu ,  Tsuyoshi Terayama

    发明人： Susumu Mizuta ,  Iwao Yamaguchi ,  Toshiya Kumagai ,  Takaaki Manabe ,  Wakichi Kondo ,  Tadao Shimizu ,  Tsuyoshi Terayama

    IPC分类号： C30B702

    CPC分类号： C23C18/1216 ,  C23C18/04

    摘要： A process for forming a dense, epitaxial metal oxide film on a single crystal substrate, including cleaning the surface of the single crystal substrate, contacting the cleaned surface with a polar organic compound such as a small molecular weight alcohol, so that the cleaned surface adsorbs the polar organic compound, then applying a hydrocarbon solvent solution containing at least one organic group-containing metal compound on the polar organic compound-adsorbed surface, and then heating the substrate to decompose the organic group-containing metal compound and to form a dense epitaxial metal oxide film on the substrate.

    摘要翻译： 一种用于在单晶衬底上形成致密的外延金属氧化物膜的方法，包括清洗单晶衬底的表面，使清洁的表面与极小的有机化合物如小分子量醇接触，使得清洁的表面吸附 极性有机化合物，然后在极性有机化合物吸附表面上施加含有至少一种含有机基团的金属化合物的烃溶剂溶液，然后加热底物以分解含有机基团的金属化合物并形成致密的外延 金属氧化物膜在基板上。

    SOLUTION FOR FORMING RARE-EARTH SUPERCONDUCTIVE FILM AND PRODUCTION METHOD THEREOF
    3.
    发明申请
    SOLUTION FOR FORMING RARE-EARTH SUPERCONDUCTIVE FILM AND PRODUCTION METHOD THEREOF 有权
    形成稀土超导薄膜的方法及其制备方法

    公开(公告)号：US20120270738A1

    公开(公告)日：2012-10-25

    申请号：US13514139

    申请日：2010-12-09

    申请人： Takaaki Manabe ,  Iwao Yamaguchi ,  Toshiya Kumagai ,  Mitsugu Sohma ,  Wakichi Kondou ,  Kenichi Tsukada

    发明人： Takaaki Manabe ,  Iwao Yamaguchi ,  Toshiya Kumagai ,  Mitsugu Sohma ,  Wakichi Kondou ,  Kenichi Tsukada

    IPC分类号： H01L39/12

    CPC分类号： C01G3/006 ,  H01L39/2425

    摘要： Provided is a coating solution where, upon producing a rare-earth superconductive composite metal oxide film by means of a coating-pyrolysis method, cracks are not generated in the heat treatment process for eliminating organic components, even when the thickness of the rare-earth superconductive film produced in a single coating is 500 nm or more, and without having to repeat the coating and annealing process. A solution for producing a rare-earth superconductive film which is made into a homogeneous solution by dissolving, in a solvent formed by adding a polyhydric alcohol to a univalent linear alcohol having a carbon number of 1 to 8 and/or water, a metal complex coordinated, relative to metal ions of a metallic species containing rare-earth elements, barium and copper, with pyridine and/or at least one type of tertiary amine, at least one type of carboxylic acid having a carbon number of 1 to 8, and, as needed, an acetylacetonato group.

    摘要翻译： 提供一种涂布溶液，其中通过涂布 - 热解法在制备稀土超导复合金属氧化物膜时，即使在稀土元素的厚度方面，在用于消除有机组分的热处理过程中也不会产生裂纹 在单个涂层中制造的超导膜为500nm以上，不必重复涂布和退火处理。 一种制备稀土超导膜的方法，该稀土超导膜通过将溶解在通过将多元醇加入到碳原子数1至8的一价直链醇和/或水形成的溶剂中，形成均匀溶液，金属络合物 相对于含有稀土元素的金属物质，钡和铜与吡啶和/或至少一种叔胺，至少一种碳原子数为1至8的羧酸的金属离子相互配位，以及 根据需要，可以使用乙酰丙酮化合物。

    Solution for forming rare-earth superconductive film and production method thereof
    4.
    发明授权
    Solution for forming rare-earth superconductive film and production method thereof 有权
    稀土超导薄膜的制造方法及其制造方法

    公开(公告)号：US08865628B2

    公开(公告)日：2014-10-21

    申请号：US13514139

    申请日：2010-12-09

    申请人： Takaaki Manabe ,  Iwao Yamaguchi ,  Toshiya Kumagai ,  Mitsugu Sohma ,  Wakichi Kondou ,  Kenichi Tsukada

    发明人： Takaaki Manabe ,  Iwao Yamaguchi ,  Toshiya Kumagai ,  Mitsugu Sohma ,  Wakichi Kondou ,  Kenichi Tsukada

    IPC分类号： H01L39/12 ,  H01L39/24 ,  C01G3/00

    CPC分类号： C01G3/006 ,  H01L39/2425

    摘要： Provided is a coating solution where, upon producing a rare-earth superconductive composite metal oxide film by means of a coating-pyrolysis method, cracks are not generated in the heat treatment process for eliminating organic components, even when the thickness of the rare-earth superconductive film produced in a single coating is 500 nm or more, and without having to repeat the coating and annealing process. A solution for producing a rare-earth superconductive film which is made into a homogeneous solution by dissolving, in a solvent formed by adding a polyhydric alcohol to a univalent linear alcohol having a carbon number of 1 to 8 and/or water, a metal complex coordinated, relative to metal ions of a metallic species containing rare-earth elements, barium and copper, with pyridine and/or at least one type of tertiary amine, at least one type of carboxylic acid having a carbon number of 1 to 8, and, as needed, an acetylacetonato group.

    摘要翻译： 提供一种涂布溶液，其中通过涂布 - 热解法在制备稀土超导复合金属氧化物膜时，即使在稀土元素的厚度方面，在用于消除有机组分的热处理过程中也不会产生裂纹 在单个涂层中制造的超导膜为500nm以上，不必重复涂布和退火处理。 一种制备稀土超导膜的方法，该稀土超导膜通过将溶解在通过将多元醇加入到碳原子数1至8的一价直链醇和/或水形成的溶剂中，形成均匀溶液，金属络合物 相对于含有稀土元素的金属物质，钡和铜与吡啶和/或至少一种叔胺，至少一种碳原子数为1至8的羧酸的金属离子相互配位，以及 根据需要，可以使用乙酰丙酮化合物。

    Method for producing a metal oxide and method for forming a minute pattern
    6.
    发明授权
    Method for producing a metal oxide and method for forming a minute pattern 失效
    金属氧化物的制造方法及形成微小图案的方法

    公开(公告)号：US06576302B1

    公开(公告)日：2003-06-10

    申请号：US09513814

    申请日：2000-02-25

    申请人： Susumu Mizuta ,  Tetsuo Tsuchiya ,  Akio Watanabe ,  Yoji Imai ,  Iwao Yamaguchi ,  Toshiya Kumagai ,  Takaaki Manabe ,  Hiroyuki Niino ,  Akira Yabe

    发明人： Susumu Mizuta ,  Tetsuo Tsuchiya ,  Akio Watanabe ,  Yoji Imai ,  Iwao Yamaguchi ,  Toshiya Kumagai ,  Takaaki Manabe ,  Hiroyuki Niino ,  Akira Yabe

    IPC分类号： C08J718

    CPC分类号： C23C18/14 ,  C23C18/06 ,  C23C18/1216

    摘要： There is disclosed a method for producing a metal oxide, which comprises the steps of: dissolving a metal organic compound (e.g. a metal organic acid salt, a metal acetylacetonato complex, and a metal alkoxide having an organic group with 6 or more carbon atoms) in a solvent to provide a state of solution, applying the solution onto a substrate, drying the solution, and subjecting the resultant substrate to irradiation with a laser light of a 400 nm or less wavelength, to form a metal oxide on the substrate. According to that method, a metal oxide can be produced without applying a heat treatment at a high temperature of the degree adopted in the conventionally known application thermal decomposition method.

    摘要翻译： 公开了一种金属氧化物的制造方法，该方法包括以下步骤：将金属有机化合物（例如金属有机酸盐，金属乙酰丙酮络合物和具有6个或更多个碳原子的有机基团的金属醇盐） 在溶剂中以提供溶液状态，将溶液施加到基材上，干燥溶液，并使所得基板对波长为400nm以下的激光进行照射，以在基板上形成金属氧化物。 根据该方法，可以在常规已知的应用热分解方法中采用的高温下进行金属氧化物而不进行热处理。