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1.发明授权Rheology modified relatively high melt strength polyethylene compositions and methods of making pipes, films, sheets, and blow-molded articles 有权流变改性相对较高的熔体强度聚乙烯组合物和制造管，膜，片和吹塑制品的方法公开(公告)号：US08920891B2
公开(公告)日：2014-12-30
申请号：US11721388
申请日：2005-12-09
申请人： William J. Michie, Jr. , Dane Chang , Anthony C. Neubauer , Mridula Kapur , Todd A. Hogan , Felipe B. Martinez , Stephane Costeux
发明人： William J. Michie, Jr. , Dane Chang , Anthony C. Neubauer , Mridula Kapur , Todd A. Hogan , Felipe B. Martinez , Stephane Costeux
CPC分类号： C08K5/43 , C08L23/0807 , C08L2205/02 , Y10T428/1352 , Y10T428/139 , C08L23/08 , C08L2666/06
摘要： A polymer composition comprises a low-molecular-weight (LMW) ethylene polymer component and a high-molecular-weight (HMW) ethylene polymer component coupled with a polysulfonyl azide. Preferably, the LMW polyethylene component and the HMW polyethylene component co-crystallize in the composition such that it exhibits a single or substantially single peak in a lamella thickness distribution (LTD) curve. The ethylene polymer for the LMW and the HMW polyethylene components can be either homopolymer or ethylene copolymer. Preferably, both components are an ethylene copolymer of the same, or different, composition (that is, with the same or different comonomers). A method of making a pipe that includes selecting a polymer composition having a substantially single peak in the LTD curve is described. Compositions comprising a chromium-catalyzed ethylene polymer, coupled with a polysulfonyl azide are also described herein.
摘要翻译： 聚合物组合物包含与聚磺酰叠氮基偶联的低分子量（LMW）乙烯聚合物组分和高分子量（HMW）乙烯聚合物组分。 优选地，LMW聚乙烯组分和HMW聚乙烯组分在组合物中共结晶，使得其在薄片厚度分布（LTD）曲线中表现出单一或基本上单峰。 用于LMW和HMW聚乙烯组分的乙烯聚合物可以是均聚物或乙烯共聚物。 优选地，两种组分都是相同或不同组成（即相同或不同的共聚单体）的乙烯共聚物。 描述了制造管道的方法，其包括选择在LTD曲线中具有基本单峰的聚合物组合物。 本文还描述了包含铬催化的乙烯聚合物与聚磺酰叠氮化物偶联的组合物。
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2.发明申请公开(公告)号：US20090246433A1
公开(公告)日：2009-10-01
申请号：US11721388
申请日：2005-12-09
申请人： William J. Michie , Dane Chang , Anthony C. Neubauer , Mridula Kapur , Todd A. Hogan , Felipe B. Martinez , Stephane Costeux
发明人： William J. Michie , Dane Chang , Anthony C. Neubauer , Mridula Kapur , Todd A. Hogan , Felipe B. Martinez , Stephane Costeux
CPC分类号： C08K5/43 , C08L23/0807 , C08L2205/02 , Y10T428/1352 , Y10T428/139 , C08L23/08 , C08L2666/06
摘要： A polymer composition comprises a low-molecular-weight (LMW) ethylene polymer component and a high-molecular-weight (HMW) ethylene polymer component coupled with a polysulfonyl azide. Preferably, the LMW polyethylene component and the HMW polyethylene component co-crystallize in the composition such that it exhibits a single or substantially single peak in a lamella thickness distribution (LTD) curve. The ethylene polymer for the LMW and the HMW polyethylene components can be either homopolymer or ethylene copolymer. Preferably, both components are an ethylene copolymer of the same, or different, composition (that is, with the same or different comonomers). A method of making a pipe that includes selecting a polymer composition having a substantially single peak in the LTD curve is described. Compositions comprising a chromium-catalyzed ethylene polymer, coupled with a polysulfonyl azide are also described herein.
摘要翻译： 聚合物组合物包含与聚磺酰叠氮基偶联的低分子量（LMW）乙烯聚合物组分和高分子量（HMW）乙烯聚合物组分。 优选地，LMW聚乙烯组分和HMW聚乙烯组分在组合物中共结晶，使得其在薄片厚度分布（LTD）曲线中表现出单一或基本上单峰。 用于LMW和HMW聚乙烯组分的乙烯聚合物可以是均聚物或乙烯共聚物。 优选地，两种组分都是相同或不同组成（即相同或不同的共聚单体）的乙烯共聚物。 描述了制造管道的方法，其包括选择在LTD曲线中具有基本单峰的聚合物组合物。 本文还描述了包含铬催化的乙烯聚合物与聚磺酰叠氮化物偶联的组合物。
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公开(公告)号：US20120100357A1
公开(公告)日：2012-04-26
申请号：US12282223
申请日：2007-03-09
申请人： William J. Michie, JR. , Todd A. Hogan , Felipe Martinez Barreneche , Anthony C. Neubauer , Stephane Costeux
发明人： William J. Michie, JR. , Todd A. Hogan , Felipe Martinez Barreneche , Anthony C. Neubauer , Stephane Costeux
IPC分类号： B32B3/00 , D01F1/02 , B29C47/92 , C08F110/02
CPC分类号： B29C47/0869 , B29C47/0004 , B29C47/1072 , B29C47/92 , B29C2947/922 , B29C2947/92266 , B29C2947/92485 , B29C2947/92761 , B29C2947/92933 , B29K2023/065 , C08J5/18 , C08J2323/08
摘要： This invention relates to coupling of polyethylene resins, more specifically coupling of polyethylene resins for use in extruded profiles, especially extruded profiles for sheet extrusion and cut sheet thermoforming applications and geomembranes. The process involves conveying a HDPE resin through an extruder, wherein the extruder comprises a feed zone, a first melt zone downstream of the feed zone, a second melt zone downstream of the first melt zone, and a third melt zone downstream of the second melt zone. The resin is melted in the first zone, contacted with oxygen in the second melt zone, and contacted antioxidant in the third melt zone.
摘要翻译： 本发明涉及聚乙烯树脂的偶联，更具体地说，用于挤出型材的聚乙烯树脂的偶联，特别是用于片材挤出和切割片材热成型应用的挤出型材以及土工膜。 该方法包括将HDPE树脂输送通过挤出机，其中挤出机包括进料区，进料区下游的第一熔融区，第一熔融区下游的第二熔融区，第二熔体下游的第三熔融区 区。 树脂在第一区域熔化，与第二熔融区域中的氧气接触，并在第三熔融区域中与抗氧化剂接触。
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公开(公告)号：US09492963B2
公开(公告)日：2016-11-15
申请号：US12282223
申请日：2007-03-09
申请人： William J. Michie, Jr. , Todd A. Hogan , Felipe Martinez Barreneche , Anthony C. Neubauer , Stephane Costeux
发明人： William J. Michie, Jr. , Todd A. Hogan , Felipe Martinez Barreneche , Anthony C. Neubauer , Stephane Costeux
CPC分类号： B29C47/0869 , B29C47/0004 , B29C47/1072 , B29C47/92 , B29C2947/922 , B29C2947/92266 , B29C2947/92485 , B29C2947/92761 , B29C2947/92933 , B29K2023/065 , C08J5/18 , C08J2323/08
摘要： This invention relates to coupling of polyethylene resins, more specifically coupling of polyethylene resins for use in extruded profiles, especially extruded profiles for sheet extrusion and cut sheet thermoforming applications and geomembranes. The process involves conveying a HDPE resin through an extruder, wherein the extruder comprises a feed zone, a first melt zone downstream of the feed zone, a second melt zone downstream of the first melt zone, and a third melt zone downstream of the second melt zone. The resin is melted in the first zone, contacted with oxygen in the second melt zone, and contacted antioxidant in the third melt zone.
摘要翻译： 本发明涉及聚乙烯树脂的偶联，更具体地说，用于挤出型材的聚乙烯树脂的偶联，特别是用于片材挤出和切割片材热成型应用的挤出型材以及土工膜。 该方法包括将HDPE树脂输送通过挤出机，其中挤出机包括进料区，进料区下游的第一熔融区，第一熔融区下游的第二熔融区，第二熔体下游的第三熔融区 区。 树脂在第一区域熔化，与第二熔融区域中的氧气接触，并在第三熔融区域中与抗氧化剂接触。
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公开(公告)号：US20100086798A1
公开(公告)日：2010-04-08
申请号：US12571689
申请日：2009-10-01
CPC分类号： C08L53/02 , B28B5/02 , B32B27/32 , C08F8/30 , C08F8/34 , C08J11/06 , C08L9/00 , C08L21/00 , C08L23/14 , C08L23/142 , C08L23/286 , C08L53/025 , Y02P20/582 , Y10T428/31913 , C08F210/06 , C08L2666/02 , C08L2666/04
摘要： The present disclosure is directed to polymeric compositions which form gloss resins suitable for thermoforming applications. The polymeric compositions include a reaction product composed of a clarified random propylene/α-olefin copolymer, a coupling agent, and optionally an elastomer. Methods for adjusting the melt flow rate of the gloss resin are also disclosed. Adjustment of the gloss resin melt flow rate advantageously enables scrap thermoplastic material containing the gloss resin to be recycled in a thermoforming operation.
摘要翻译： 本公开涉及形成适于热成型应用的光泽树脂的聚合物组合物。 聚合物组合物包括由澄清的无规丙烯/α-烯烃共聚物，偶联剂和任选的弹性体组成的反应产物。 还公开了调节光泽树脂的熔体流动速率的方法。 光泽树脂熔体流动速率的调整有利地使含有光泽树脂的废塑料材料在热成型操作中被再循环。
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公开(公告)号：US08603639B2
公开(公告)日：2013-12-10
申请号：US12571689
申请日：2009-10-01
IPC分类号： B32B27/08
CPC分类号： C08L53/02 , B28B5/02 , B32B27/32 , C08F8/30 , C08F8/34 , C08J11/06 , C08L9/00 , C08L21/00 , C08L23/14 , C08L23/142 , C08L23/286 , C08L53/025 , Y02P20/582 , Y10T428/31913 , C08F210/06 , C08L2666/02 , C08L2666/04
摘要： The present disclosure is directed to polymeric compositions which form gloss resins suitable for thermoforming applications. The polymeric compositions include a reaction product composed of a clarified random propylene/α-olefin copolymer, a coupling agent, and optionally an elastomer. Methods for adjusting the melt flow rate of the gloss resin are also disclosed. Adjustment of the gloss resin melt flow rate advantageously enables scrap thermoplastic material containing the gloss resin to be recycled in a thermoforming operation.
摘要翻译： 本公开涉及形成适于热成型应用的光泽树脂的聚合物组合物。 聚合物组合物包括由澄清的无规丙烯/α-烯烃共聚物，偶联剂和任选的弹性体组成的反应产物。 还公开了调节光泽树脂的熔体流动速率的方法。 光泽树脂熔体流动速率的调整有利地使含有光泽树脂的废塑料材料在热成型操作中被再循环。
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7.发明授权Polypropylene composition, a method of producing the same, and articles made therefrom 有权聚丙烯组合物，其制造方法和由其制成的制品公开(公告)号：US08436089B2
公开(公告)日：2013-05-07
申请号：US12532346
申请日：2008-02-27
CPC分类号： C08L23/10 , C08K3/013 , C08K5/0083 , C08K5/43 , C08L21/00 , C08L23/0815 , C08L2023/44 , C08L2666/06 , C08L2666/04
摘要： The instant invention is a polypropylene composition, a method of producing the same, and articles made therefrom. The polypropylene composition according to instant invention includes the reactive melt blending product of a high crystalline polypropylene having a crystallinity of at least 64 percent, an elastomer, a coupling agent, and optionally a filler. The polypropylene composition according to instant invention has a melt flow rate in the range of less than 1 g/10 minutes measured at 230° C. under a load of 2.16 kg in accordance with ASTM-D 1238.
摘要翻译： 本发明是聚丙烯组合物，其制造方法和由其制成的制品。 根据本发明的聚丙烯组合物包括具有至少64％的结晶度的高结晶聚丙烯的反应性熔融共混产物，弹性体，偶联剂和任选的填料。 根据本发明的聚丙烯组合物，根据ASTM-D 1238，在230℃，2.16kg负载下测定的熔体流动速率小于1g / 10分钟。
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8.发明申请A POLYPROPYLENE COMPOSITION, A METHOD OF PRODUCING THE SAME, AND ARTICLES MADE THEREFROM 有权聚丙烯组合物，其制造方法及其制造方法公开(公告)号：US20100048792A1
公开(公告)日：2010-02-25
申请号：US12532346
申请日：2008-02-27
CPC分类号： C08L23/10 , C08K3/013 , C08K5/0083 , C08K5/43 , C08L21/00 , C08L23/0815 , C08L2023/44 , C08L2666/06 , C08L2666/04
摘要： The instant invention is a polypropylene composition, a method of producing the same, and articles made therefrom. The polypropylene composition according to instant invention includes the reactive melt blending product of a high crystalline polypropylene having a crystallinity of at least 64 percent, an elastomer, a coupling agent, and optionally a filler. The polypropylene composition according to instant invention has a melt flow rate in the range of less than 1 g/10 minutes measured at 230° C. under a load of 2.16 kg in accordance with ASTM-D 1238. The method of producing a polypropylene composition according to instant invention includes the following steps: (1) reactive melt blending a high crystalline polypropylene having a crystallinity of at least 64 percent, an elastomer, and optionally a filler in the presence of a coupling agent; and (2) thereby producing the polypropylene composition having a melt flow rate in the range of less than 1 g/10 minutes measured at 230° C. under a load of 2.16 kg in accordance with ASTM-D 1238. The articles according to instant invention include the inventive polypropylene composition including the reactive melt blending product of a high crystalline polypropylene having a crystallinity of at least 64 percent, an elastomer, a coupling agent, and optionally a filler.
摘要翻译： 本发明是聚丙烯组合物，其制造方法和由其制成的制品。 根据本发明的聚丙烯组合物包括具有至少64％的结晶度的高结晶聚丙烯的反应性熔融共混产物，弹性体，偶联剂和任选的填料。 根据本发明的聚丙烯组合物根据ASTM-D 1238，在230℃，2.16kg负荷下测量的熔体流动速率在小于1g / 10分钟的范围内。制备聚丙烯组合物的方法 根据本发明包括以下步骤：（1）在偶联剂存在下，反应性熔体共混结晶度至少为64％的高结晶聚丙烯，弹性体和任选的填料; 根据ASTM-D 1238，在230℃，2.16kg负荷下测定熔体流动速率在小于1g / 10分钟范围内的聚丙烯组合物。 本发明包括本发明的聚丙烯组合物，其包括结晶度至少为64％的高结晶聚丙烯的反应性熔融共混产物，弹性体，偶联剂和任选的填料。
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公开(公告)号：US20110052930A1
公开(公告)日：2011-03-03
申请号：US12861146
申请日：2010-08-23
申请人： Jinder Jow , Michael S. Broadway , Malcolm F. Finlayson , Todd A. Hogan , Drew A. Davidock , Angel S. Mendez
发明人： Jinder Jow , Michael S. Broadway , Malcolm F. Finlayson , Todd A. Hogan , Drew A. Davidock , Angel S. Mendez
IPC分类号： B32B27/08 , C08F110/06 , C08J5/00 , B29C47/06
CPC分类号： B32B27/32 , B29C48/03 , B29C48/08 , B29C48/21 , B29C51/002 , B29K2023/12 , B29K2995/0022 , B32B25/08 , B32B25/14 , B32B27/08 , B32B27/20 , B32B2250/24 , B32B2270/00 , B32B2307/406 , B32B2307/412 , B32B2307/738 , C08F210/06 , C08J2323/06 , Y10T428/31913 , C08F210/16 , C08F2500/12
摘要： The present disclosure is directed to a thermoforming process and thermoformed articles produced therefrom. The thermoforming process includes heating a structure with a gloss layer composed of a propylene-based polymer having a melt flow rate from about 0.1 g/10 min to about 1.5 g/10 min, and producing a thermoformed article wherein the gloss layer has a post-thermoformed Gardner gloss value within 25% of the pre-thermoformed Gardner gloss value for the gloss layer. The thermoformed article may have a gloss layer with a post-thermoformed Gardner gloss value greater than or equal to about 60.
摘要翻译： 本公开涉及一种热成型工艺和由其制备的热成型制品。 热成型工艺包括加热具有由熔体流动速率为约0.1g / 10min至约1.5g / 10min的丙烯基聚合物组成的光泽层的结构，并且制备热成型制品，其中光泽层具有柱 热成型加德纳光泽值在光泽层预热成型加德纳光泽值的25％以内。 热成型制品可以具有光泽层，其具有大于或等于约60°的后热成型加德纳光泽值。
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