Epoxy compound, method for producing the same, epoxy resin composition, and cured product thereof

    公开(公告)号:US10329231B2

    公开(公告)日:2019-06-25

    申请号:US15647386

    申请日:2017-07-12

    申请人: DIC Corporation

    摘要: The present invention provides an epoxy compound which is 2,2′,7,7′-tetraglycidyloxy-1,1′-binaphthalene. Also, the present invention provides a method for producing [1,1′-binaphthalene]-2,2′,7,7′-tetraol, the method including a step of bringing a crude product produced by dimerization reaction of naphthalene-2,7-diol or a naphthalene-2,7-diol derivative into contact with an aromatic solvent; a step of separating [1,1′-binaphthalene]-2,2′,7,7′-tetraol dissolved in the aromatic solvent from insoluble substances; and a step of removing the solvent from a solution of [1,1′-binaphthalene]-2,2′,7,7′-tetraol. The present invention also provides a method for producing an epoxy compound, the method including reacting [1,1′-binaphthalene]-2,2′,7,7′-tetraol or [1,1′-binaphthalene]-2,2′,7,7′-tetraol monohydrate with epihalohydrin.

    Vertical continuous reactor and process for liquid epoxy resin
    6.
    发明授权
    Vertical continuous reactor and process for liquid epoxy resin 失效
    液态环氧树脂立式连续反应器和工艺

    公开(公告)号:US5310955A

    公开(公告)日:1994-05-10

    申请号:US107400

    申请日:1993-08-16

    摘要: A vertical reactor system having a plurality of substantially vertically aligned reaction compartments one on top of the other, the reactant materials (and catalyst and solvent, if desired), flowable from a first top compartment through intermediate compartments, if any, to a bottom compartment from which a desired product of a reaction of the reactant materials is withdrawn, the compartments having inlets for the addition of additional reactants, catalysts, or solvents and outlets for withdrawing by-products, vapors, and water from any compartment, and processes for producing products using such a system. In one embodiment the product is a liquid epoxy resin. Stirring impellers may be provided in any compartment. A liquid seal may be provided on a shaft for the impellers and, in one embodiment the seals in each compartment may be elevated above the liquid in the compartments.

    摘要翻译: 一种垂直反应器系统,其具有多个基本上垂直排列的反应室,一个在另一个的顶部上,反应物材料(和催化剂和溶剂,如果需要),可从第一顶部隔室通过中间隔室(如果有的话)流到底部隔室 反应物料反应的期望产物从中排出,具有用于添加另外的反应物,催化剂或溶剂的入口的隔室和用于从任何隔室取出副产物,蒸汽和水的出口,以及用于生产 产品使用这样的系统。 在一个实施方案中,产物是液体环氧树脂。 搅拌叶轮可以设在任何隔间。 液体密封件可以设置在用于叶轮的轴上,并且在一个实施例中,每个隔室中的密封件可以在隔室中的液体上方升高。