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    PIMARIC TYPE RESIN ACID PRODUCT, AND METHOD OF PREPARING THE SAME
    4.
    发明申请
    PIMARIC TYPE RESIN ACID PRODUCT, AND METHOD OF PREPARING THE SAME 审中-公开
    PIMARIC型树脂酸产品及其制备方法

    公开(公告)号：US20140148572A1

    公开(公告)日：2014-05-29

    申请号：US14170038

    申请日：2014-01-31

    申请人： INSTITUTE OF CHEMICAL INDUSTRY OF FOREST PRODUCTS, CAF

    发明人： Zhendong Zhao ,  Yuxiang Chen ,  Liangwu Bi ,  Yan Gu ,  Dongmei Li ,  Jing Wang ,  Yanju Lu

    IPC分类号： C08H99/00

    CPC分类号： C08H99/00 ,  C07B41/08 ,  C07C2603/26 ,  C08H8/00

    摘要： A method for preparing pimaric acid type resin acids includes: step (1) adding refined resin acid, turpentine, or rosin along with maleic anhydride at a mass ratio of 1:0.3-1.5 into a reaction bottle, dissolving the ingredients into a C1-C10 lower fatty acid solvent, the mass ratio of the C1-C10 low fatty acid to refined resin acid is 0.05-30:1, then carrying out additional reaction by heating directly or with assistance of a microwave, subsequently cooling, crystallizing, filtering, and washing; and step (2) combining the filtrates collected in step (1), stripping the solvent by vacuum distillation to obtain pimaric acid type resin acid coarse product, dissolving the resulting coarse product in NaOH aqueous solution to prepare aqueous solution of pimaric acid type resin acid salt, adjusting the pH to 6-14 with a mineral acid or an organic acid, and either directly purifying or acidifying followed by purifying to obtain the final product.

    摘要翻译： 制备海松酸型树脂酸的方法包括：步骤（1）将质量比为1:0.3-1.5的精制树脂酸，松节油或松香与马来酸酐加入到反应瓶中，将成分溶解在C1- C10低级脂肪酸溶剂，C1-C10低级脂肪酸与精制树脂酸的质量比为0.05-30:1，然后直接加热或在微波辅助下进行附加反应，随后冷却，结晶，过滤， 洗涤; 和步骤（2）将步骤（1）中收集的滤液合并，通过真空蒸馏除去溶剂，得到海松酸型树脂酸粗产物，将所得粗产物溶解在NaOH水溶液中，制备海松酸型树脂酸水溶液 盐，用无机酸或有机酸将pH调节至6-14，直接纯化或酸化，然后纯化，得到最终产物。

    Method for producing humic acid salts
    6.
    发明申请
    Method for producing humic acid salts 失效
    腐殖酸盐的生产方法

    公开(公告)号：US20050069974A1

    公开(公告)日：2005-03-31

    申请号：US10498776

    申请日：2002-12-16

    申请人： Oleg Gladkov ,  Rodion Poloskin ,  Yuri Polyakov ,  Irina Sokolova ,  Nicolay Sorokin ,  Aleksey Glebov

    发明人： Oleg Gladkov ,  Rodion Poloskin ,  Yuri Polyakov ,  Irina Sokolova ,  Nicolay Sorokin ,  Aleksey Glebov

    IPC分类号： C05F11/00 ,  C05F11/02 ,  C08H99/00 ,  C12P1/00 ,  C08L97/00

    CPC分类号： C08H6/00 ,  C05F11/02 ,  C08H99/00

    摘要： Humic acid salts are produced, with a high output of useful products, by a liquid-phase oxidation of the mixture of an alkaline agent with a lignin-containing plant raw material having the total content of dry substances of 12-20%, said oxidation being carried out in two stages. In a first stage, pre-oxidation is carried out at a temperature of 50-190 DEG C. and a pressure of 0.5-3 MPa associated with simultaneous treatment with an oxygen-containing gas until a pH of 10.5-12 is reached. The second stage, i.e. oxidation is carried out in the similar conditions at a temperature of 170-200 DEG C. until a pH of 8.5-10 is reached. The by-product of cellulose production by a sulphite process, i.e. concentrated solutions of lignosulphonate or lignin is used as a lignin-containing plant raw material, said lignin being a by-product of hydrolysis production being continuously oxidised by air oxygen in two stages. In order to additionally activate the mixture of the raw material with alkali, operating in cavitation mode, a circulation pump provided with an ejector for stream ejection of air is used. In order to reduce the pre-oxidation time, the first stage can be carried out using peroxide, or by supplying the raw material and alkali directly to a pipeline prior to an ejector and the mixture thereof with an oxidising agent.

    摘要翻译： 通过将碱性物质与含有干物质总含量为12-20％的含木质素的植物原料的混合物进行液相氧化，产生具有高产量有用产物的腐殖酸盐，所述氧化 分两个阶段进行。 在第一阶段中，预氧化在50-190℃的温度和0.5-3MPa的压力下进行，同时用含氧气体处理直至达到10.5-12的pH。 第二阶段，即在类似的条件下，在170-200℃的温度下进行氧化，直至pH达到8.5-10。 使用亚硫酸盐法生产纤维素的副产物，即木质素磺酸盐或木质素的浓缩溶液作为含木质素的植物原料，所述木质素是水解产物的副产物，由两个阶段的空气氧持续氧化。 为了额外地激活原料与碱的混合物，在空化模式下操作，设置有用于空气流喷射的喷射器的循环泵。 为了减少预氧化时间，第一阶段可以使用过氧化物，或者在喷射器之前将原料和碱直接供给到管道，并且与氧化剂的混合物进行。

    Polyphenol derivative compositions and perparation thereof
    8.
    发明授权
    Polyphenol derivative compositions and perparation thereof 失效
    多酚衍生物组合物及其衍生物

    公开(公告)号：US5844061A

    公开(公告)日：1998-12-01

    申请号：US557179

    申请日：1995-12-13

    申请人： Joseph Vercauteren ,  Jean-Frederic Weber ,  Jean-Louis Bisson ,  Jean Bignon

    发明人： Joseph Vercauteren ,  Jean-Frederic Weber ,  Jean-Louis Bisson ,  Jean Bignon

    IPC分类号： A23L3/3517 ,  A61K8/49 ,  A61K8/60 ,  A61K31/35 ,  A61K31/352 ,  A61Q17/04 ,  A61Q19/00 ,  C07D311/62 ,  C08G61/00 ,  C08H99/00 ,  C09K15/08 ,  C08G18/32

    CPC分类号： C09K15/08 ,  A61K31/35 ,  A61K8/498 ,  A61K8/602 ,  A61Q17/00 ,  A61Q19/00 ,  C07D311/62 ,  C08G61/00 ,  A61Q17/04 ,  A61Q19/08

    摘要： Polyphenol derivative compositions including oligomer or polymer esters containing N+2 monomer moieties, whose monomer moieties correspond to the following formula ##STR1## in which N is a number from 0 to 100, A represents a group --OR, a hydrogen atom or a substituent R, at least a majority of the substituents R represent a group --COR.sub.1, R.sub.1 is a saturated or unsaturated, linear or branched alkyl radical of at least two carbon atoms, or an aryl, aralkyl or aralkylene radical, a remainder of the substituents R is a hydrogen atom, an alkyl group, an acyl group --CO--C.sub.6 H.sub.2 --(OH).sub.3, a monosaccharide or a polysaccharide, and n.sub.1 and n.sub.2, which are identical to or different from each other, are numbers from 1 to 3, corresponding to the number of substitutions on a ring, and the diastereoisomers and the regioisomers of said monomer moieties, whereby the monomer moieties are connected by carbon--carbon bonds or by ether bridges between the rings which make up a flavan ring system.

    摘要翻译： PCT No.PCT / FR94 / 00712 Sec。 371 1995年12月13日第 102（e）日期1995年12月13日PCT提交1994年6月14日PCT公布。 公开号WO94 / 29404 日期1994年12月22日多酚衍生物组合物包括含有N + 2单体部分的低聚物或聚合物酯，其单体部分对应于下列式（IMAGE），其中N为0至100的数，A表示-OR，a 氢原子或取代基R，至少大多数取代基R代表基团-COR1，R1是至少两个碳原子的饱和或不饱和的直链或支链烷基，或芳基，芳烷基或芳亚烷基， 取代基R的剩余部分为氢原子，烷基，酰基-CO-C6H2-（OH）3，单糖或多糖，n1和n2彼此相同或不同，为数字 1至3，对应于环上的取代数，以及所述单体部分的非对映异构体和区域异构体，由此单体部分通过碳 - 碳键或由构成黄烷环的环之间的醚桥连接 系统。

    Crosslinked tannin/inorganic oxide composites
    10.
    发明授权
    Crosslinked tannin/inorganic oxide composites 失效
    交联单宁/无机氧化物复合材料

    公开(公告)号：US5789467A

    公开(公告)日：1998-08-04

    申请号：US673402

    申请日：1996-06-28

    申请人： Demetrius Michos

    发明人： Demetrius Michos

    IPC分类号： A23L2/00 ,  C08G59/42 ,  C08H99/00 ,  C08K3/34 ,  C08L99/00 ,  C12H1/02 ,  C08K9/00

    CPC分类号： C08H99/00 ,  C12H1/02

    摘要： Epoxy-polymerized tannin/inorganic oxide composite particles are obtained by polymerizing the tannin with a polyepoxy crosslinking agent in situ on inorganic oxide particles. The compositions of the invention are capable of achieving the performance of tannin in beverage treatment applications without tannin's associated filtration disadvantages.

    摘要翻译： 环氧聚合单宁/无机氧化物复合颗粒是通过在无机氧化物颗粒上原位聚合具有聚环氧交联剂的单宁得到的。 本发明的组合物能够在没有单宁的相关过滤缺点的情况下实现饮料处理应用中单宁的性能。