Method for chromatographic purification of viscous loads

    公开(公告)号:US11987853B2

    公开(公告)日:2024-05-21

    申请号:US17047672

    申请日:2019-04-22

    摘要: The invention relates to a method for purifying a mixture to be separated, in a multicolumn chromatography system, the method comprising successively and cyclically:



    a step of collecting a raffinate, a step of injecting the mixture to be separated, a step of collecting an extract and an eluent injection step, at an operating temperature;
    wherein the mixture to be separated has a viscosity at 20° C. greater than or equal to 3 mPa·s; and wherein the dry matter mass concentration of the mixture to be separated is equal, within 5%, to a threshold concentration, said threshold concentration is such that:
    the viscosity of the mixture to be treated at a dry matter mass concentration equal to the threshold concentration and at the operating temperature, is equal to twice the viscosity of the mixture to be treated, at a dry matter mass concentration equal to 85% of the threshold concentration and at the operating temperature.

    Processing of lignocellulosic biomass

    公开(公告)号:US11920203B2

    公开(公告)日:2024-03-05

    申请号:US17250508

    申请日:2019-07-15

    IPC分类号: C13K1/02 C13K13/00

    CPC分类号: C13K1/02 C13K13/00

    摘要: Lignocellulosic biomass (11) is processed to produce organic chemicals by (a) subjecting the biomass to a first hydrolysis (14) to hydrolyse hemicellulose, to form a liquid component comprising the products of hemicellulose hydrolysis in solution, and a solid component comprising cellulose and lignin; (b) then subjecting the solid component to a second hydrolysis (20), so as to hydrolyse cellulose and vaporise the resulting products of cellulose hydrolysis; and (c) then condensing (22) the resulting vapours to form an aqueous solution (25) containing the products of cellulose hydrolysis. After the first hydrolysis (14) and before the second hydrolysis (20), the process also comprises subjecting the solid component to a washing step (16). In this washing step (16) the solid component is washed with the aqueous solution (25) that contains the products of cellulose hydrolysis. Hence the resultant solution contains the products of both the first and the second hydrolysis steps (14, 20).

    DRIED ALLULOSE CRYSTALS
    9.
    发明公开

    公开(公告)号:US20230374617A1

    公开(公告)日:2023-11-23

    申请号:US18220605

    申请日:2023-07-11

    IPC分类号: C13K13/00

    CPC分类号: C13K13/00

    摘要: The teachings herein relate to dried allulose crystals having low water content. The water content of the dried allulose crystals may be at most 0.1 weight percent. Preferably, the water content is at most 0.01 weight percent and more preferably at most 0.001 weight percent. The dried allulose crystals preferably are free flowing. The dried allulose crystals preferably have reduced hygroscopicity and/or improved sensory properties.

    DRYING OF ALLULOSE CRYSTALS
    10.
    发明公开

    公开(公告)号:US20230349013A1

    公开(公告)日:2023-11-02

    申请号:US18220603

    申请日:2023-07-11

    IPC分类号: C13K13/00

    CPC分类号: C13K13/00

    摘要: The teachings herein relate to a process for drying allulose crystals. The process includes a step of providing non-dried allulose crystals. The process includes temperature treating the crystals at a temperature in the range of about 25 to about 70° C. in a drying apparatus to form an intermediate product. The process includes conditioning the intermediate process. The conditioning may be for about 30 minutes to 7 hours at 40 to 70° C. The conditioning may be for about 15 to about 90 hours with air of a relative humidity of about 30 to about 60% at 25 to about 40° C.