TREATMENTS FOR CONTROLLING POROSITY IN ANTIREFLECTIVE COATINGS
    2.
    发明申请
    TREATMENTS FOR CONTROLLING POROSITY IN ANTIREFLECTIVE COATINGS 审中-公开
    用于控制抗反射涂层中的孔隙度的处理

    公开(公告)号:WO2014028320A3

    公开(公告)日:2015-07-16

    申请号:PCT/US2013054298

    申请日:2013-08-09

    IPC分类号: B05D3/02 B05D5/02 C09C3/12

    摘要: In some embodiments, the current invention discloses methods and apparatuses for making coated articles including a two step treatment process of a coated layer. The first step of the heat treatment involves a thermally assisted curing of the coated layer at a low temperature, which can strengthen the bond formation in the coated layer, leading to better layer stability during the subsequent heat treatment. The second step of the heat treatment involves annealing of the cured layer at a high temperature, which can control a porosity of the coated layer.

    摘要翻译: 在一些实施方案中,本发明公开了用于制备涂覆制品的方法和装置,包括涂层的两步处理工艺。 热处理的第一步包括在低温下热辅助固化涂层,这可以加强涂层中的结合形成,导致在随后的热处理期间更好的层稳定性。 热处理的第二步包括在高温下退火固化层,这可以控制涂层的孔隙率。

    METHOD OF DEPOSITING THIN METAL-ORGANIC FILMS
    3.
    发明申请
    METHOD OF DEPOSITING THIN METAL-ORGANIC FILMS 审中-公开
    沉积薄金属有机膜的方法

    公开(公告)号:WO2015038303A1

    公开(公告)日:2015-03-19

    申请号:PCT/US2014/051930

    申请日:2014-08-20

    摘要: Embodiments include systems, apparatuses, and methods of thin metal-organic film deposition with inkjet printheads. A method of depositing a metal-organic thin film over a substrate includes introducing chemical precursors into one or more piezoelectric printheads. The chemical precursors including a metallic compound and a reactive liquid or gas. The method further includes dispensing droplets or a stream of the chemical precursors with the piezoelectric printheads onto a surface of the substrate supported by a stage in a vacuum chamber.

    摘要翻译: 实施例包括用喷墨打印头薄金属 - 有机膜沉积的系统,装置和方法。 在衬底上沉积金属 - 有机薄膜的方法包括将化学前体引入到一个或多个压电打印头中。 化学前体包括金属化合物和反应性液体或气体。 该方法还包括将液滴或化学前体物流与压电打印头分配到由真空室中的载物台支撑的基底表面上。

    PHOTONIC DEVICES ON PLANAR AND CURVED SUBSTRATES AND METHODS FOR FABRICATION THEREOF
    5.
    发明申请
    PHOTONIC DEVICES ON PLANAR AND CURVED SUBSTRATES AND METHODS FOR FABRICATION THEREOF 审中-公开
    平面和弯曲基板上的光电装置及其制造方法

    公开(公告)号:WO2013130140A1

    公开(公告)日:2013-09-06

    申请号:PCT/US2012/067131

    申请日:2012-11-29

    IPC分类号: B05D3/02

    摘要: A versatile and rapid sol-gel technique for the fabrication of high quality one-dimensional photonic bandgap materials. For example, silica/titania multi-layer materials may be fabricated by a sol-gel chemistry route combined with dip-coating onto planar or curved substrate. A shock-cooling step immediately following the thin film heat-treatment process is introduced. This step was found important in the prevention of film crack formation - especially in silica/titania alternating stack materials with a high number of layers. The versatility of this sol-gel method is demonstrated by the fabrication of various Bragg stack-type materials with fine-tuned optical properties by tailoring the number and sequence of alternating layers, the film thickness and the effective refractive index of the deposited thin films. Measured optical properties show good agreement with theoretical simulations confirming the high quality of these sol-gel fabricated optical materials.

    摘要翻译: 一种用于制造高质量一维光子带隙材料的多功能和快速溶胶 - 凝胶技术。 例如,二氧化硅/二氧化钛多层材料可以通过将溶液 - 凝胶化学方法与浸涂在平面或弯曲基底上组合来制造。 介绍了薄膜热处理之后的冲击冷却步骤。 发现该步骤在防止膜裂纹形成方面是重要的,特别是在具有大量层的二氧化硅/二氧化钛交替堆叠材料中。 通过调整交替层的数量和顺序,沉积的薄膜的膜厚度和有效折射率,通过制备具有微调光学特性的各种布拉格堆叠材料来证明该溶胶 - 凝胶法的通用性。 测量的光学性能与理论模拟显示出良好的一致性,证实了这些溶胶 - 凝胶制造的光学材料的高质量。

    SOLUTION-PROCESSED SOL-GEL FILMS, DEVICES INCLUDING SAME, AND METHODS
    6.
    发明申请
    SOLUTION-PROCESSED SOL-GEL FILMS, DEVICES INCLUDING SAME, AND METHODS 审中-公开
    溶液处理溶胶膜,包括其的装置和方法

    公开(公告)号:WO2013085611A1

    公开(公告)日:2013-06-13

    申请号:PCT/US2012/059012

    申请日:2012-10-05

    申请人: QD VISION, INC.

    IPC分类号: H05B33/22 H05B33/10

    摘要: A method for preparing a sol-gel film is disclosed. The method comprises providing a sol-gel composition comprising one or more sol-gel film precursors and a crystallization aid, and processing the sol-gel composition by solution processing to form the sol-gel film. In certain embodiments, the sol-gel film comprises one or more metal oxides. A preferred crystallization aid includes triphenylphosphine oxide. A composition for making a sol-gel film, a sol-gel film, a device including a sol-gel film and a method for making such device are also disclosed.

    摘要翻译: 公开了一种制备溶胶 - 凝胶膜的方法。 该方法包括提供包含一种或多种溶胶 - 凝胶膜前体和结晶助剂的溶胶 - 凝胶组合物,并通过溶液处理加工溶胶 - 凝胶组合物以形成溶胶 - 凝胶膜。 在某些实施方案中,溶胶 - 凝胶膜包含一种或多种金属氧化物。 优选的结晶助剂包括三苯基氧化膦。 还公开了一种制备溶胶 - 凝胶膜的组合物,溶胶 - 凝胶膜,包括溶胶 - 凝胶膜的装置及其制造方法。

    ANTI-FOULING SPARK PLUG AND METHOD OF MAKING
    7.
    发明申请
    ANTI-FOULING SPARK PLUG AND METHOD OF MAKING 审中-公开
    防垢火花塞及制造方法

    公开(公告)号:WO2012078629A2

    公开(公告)日:2012-06-14

    申请号:PCT/US2011/063528

    申请日:2011-12-06

    IPC分类号: H01T13/20 H01T13/38

    摘要: Disclosed herein is a spark plug comprising an insulative sleeve having a central axial bore and an exterior surface and a center electrode extending through the central axial bore of the insulative sleeve. The insulating sleeve is positioned within, and secured to, a metal shell that serves as a mounting platform and interface to an internal combustion engine. The metal sleeve also supports a ground electrode that is positioned in a spaced relationship relative to the center electrode so as to generate a spark gap. The insulating sleeve includes a shaped tip portion that resides in a recessed end portion of the metal shell. A coating is disposed on the exterior surface of the shaped tip portion of the insulative sleeve. The coating comprises a metal oxide, a noble metal, late transition metal, or a combination comprising two or more of the foregoing metals.

    摘要翻译: 本文公开了一种火花塞,其包括具有中心轴向孔和外表面的绝缘套筒以及延伸穿过绝缘套筒的中心轴向孔的中心电极。 绝缘套管定位在金属壳体内并固定到金属壳体上,该金属壳体用作安装平台并与内燃机连接。 金属套筒还支撑相对于中心电极以间隔关系定位的接地电极,从而产生火花隙。 绝缘套筒包括位于金属壳体的凹入端部中的成形尖端部分。 涂层设置在绝缘套筒的成形尖端部分的外表面上。 该涂层包含金属氧化物,贵金属,后过渡金属或包含两种或更多种前述金属的组合。

    SOLD STATE ELECTROLYTES HAVING HIGH LITHIUM ION CONDUCTION
    9.
    发明申请
    SOLD STATE ELECTROLYTES HAVING HIGH LITHIUM ION CONDUCTION 审中-公开
    具有高氯离子电导率的状态电解质

    公开(公告)号:WO2011126558A1

    公开(公告)日:2011-10-13

    申请号:PCT/US2011/000599

    申请日:2011-04-04

    摘要: A method for making ion conducting films includes the use of primary inorganic chemicals, which are preferably water soluble; formulating the solution with appropriate solvent, preferably deionized water; and spray depositing the solid electrolyte matrix on a heated substrate, preferably at 100 to 400°C using a spray deposition system. The deposition step is then followed by lithiation or addition of lithium, then thermal processing, at temperatures preferably ranging between 100 and 500 °C, to obtain a high lithium ion conducting inorganic solid state electrolyte. The electrolyte is incorporated into a lithium ion battery. The Li ion battery comprises: a cathode comprising a material selected from the group consisting of : LiMn204, LiMnNiCoA/02, LiCo02, LiNiCo02, and LiFeP04; an anode comprising a material selected from the group consisting of :Li, Li alloys, and metal oxide doped with Li; and, a solid Li -ion conducting electrolyte selected from the group consisting of: LixAlz. y [GanBl - n] ySw (P04) c, LixAlz -y [GanBl -n] ySw (B03) c, LixGez -ySiySw (P04) c, and LixGe(z- y) SiySw (B03 ) c, where 4

    摘要翻译: 制造离子导电膜的方法包括使用优选水溶性的初级无机化学品; 用合适的溶剂配制溶液,优选去离子水; 并且使用喷雾沉积系统将固体电解质基质喷涂在加热的基底上,优选在100至400℃。 然后沉积步骤之后,锂化锂离子或加入,然后进行热处理,温度优选在100至500℃之间,以获得高的锂离子导电无机固态电解质。 将电解质结合到锂离子电池中。 锂离子电池包括:阴极,其包含选自LiMn204,LiMnNiCoA / 02,LiCoO2,LiNiCoO2和LiFePO4的材料; 包括选自Li,Li合金和掺杂Li的金属氧化物的材料的阳极; 和选自LixAlz的固体Li导电电解质。 y(G04B) - (n)ySw(P04)c,LixAlz -y [GanBl-n] ySw(B03)c,LixGez -ySiySw(P04)c和LixGe(z-y)SiySw(B03) w <20.3

    金属塩含有組成物、基板、基板の製造方法
    10.
    发明申请
    金属塩含有組成物、基板、基板の製造方法 审中-公开
    含金属盐的组合物,基材和生产基材的方法

    公开(公告)号:WO2011036730A1

    公开(公告)日:2011-03-31

    申请号:PCT/JP2009/004912

    申请日:2009-09-28

    IPC分类号: C01B13/14 C01B13/32

    摘要:  本発明は、多くの金属原料に応用可能であり、かつ、スパッタリング法と同程度の緻密で均一な金属酸化物被膜を形成するために使用しうる金属塩含有組成物と、当該金属塩含有組成物を用いて得られる金属複合体膜を表面に形成した基板、当該基板をさらに加熱することによって得られる金属複合体膜を表面に形成した基板の提供を目的とする。さらに、本発明は、そのような金属複合体膜を表面に形成した基板の製造方法の提供を目的とする。 本発明では、金属塩と、シス型構造を有する多価カルボン酸と、溶媒とを含有する金属塩含有組成物であって、金属塩に対する多価カルボン酸のモル比が0.5以上4.0以下であり、水分含有量0.05重量%以上である金属塩含有組成物を塗布法に使用して基板上に塗布する。その後、二段階の加熱処理を行う。

    摘要翻译: 本发明提供一种适用于多种金属原料的含金属盐的组合物,其可用于形成如通过溅射技术形成的致密且均匀的金属氧化物涂层。 还提供了一种基材,其具有在其表面上形成的金属复合膜,并且通过使用含金属盐的组合物和在其表面上具有金属复合膜的基材而获得,并且通过进一步加热获得 上述基材。 还提供了在其表面上制造具有这种金属复合膜的基板的方法。 含金属盐的组合物包含金属盐,具有顺式结构的多元羧酸和溶剂,其中多元羧酸与金属盐的摩尔比为0.5以上且4.0以​​下,水分含量 为0.05重量%以上。 通过涂布技术将含金属盐的组合物涂布在基材上,然后进行两阶段热处理。