スパッタリングターゲット
    1.
    发明申请
    スパッタリングターゲット 审中-公开
    溅射靶

    公开(公告)号:WO2017164168A1

    公开(公告)日:2017-09-28

    申请号:PCT/JP2017/011207

    申请日:2017-03-21

    CPC classification number: C04B35/45 C23C14/34

    Abstract: 金属銅相と酸化銅相とを有し、酸化銅相の体積率が80vol%を超えて90vol%以下の範囲内とされており、ターゲットスパッタ面における比抵抗値の平均値に対するばらつきが50%以下とされ、ターゲット組織中の前記金属銅相の粒径が10μm以上200μm以下の範囲内とされていることを特徴とする。また、p型半導体の性質を有していることが好ましい。

    Abstract translation: 具有金属铜相和氧化铜相,氧化铜相的体积分数在大于80体积%且小于或等于90体积%的范围内,比电阻值 为50%以下,靶结构中的金属铜相的粒径在10μm以上且200μm以下的范围内。 还优选具有p型半导体的特性。

    STRUCTURE AND METHOD FOR COMPACTION OF POWDER-LIKE MATERIALS
    5.
    发明申请
    STRUCTURE AND METHOD FOR COMPACTION OF POWDER-LIKE MATERIALS 审中-公开
    粉末状材料的结构与方法

    公开(公告)号:WO1998006525A2

    公开(公告)日:1998-02-19

    申请号:PCT/US1997010559

    申请日:1997-06-19

    Abstract: Structure and a method for producing very dense bodies of material from particulate materials. A particulate material is placed within an electrically conductive container. A solenoid or coil encompasses the electrically conductive container, and a large magnitude of electrical current is caused to flow through the solenoid or coil. As the electrical current flows through the solenoid or coil, large magnitudes of magnetic pressures are created upon the electrically conductive container, and the electrically conductive container is compressed, and the transverse dimension thereof is reduced. Thus, the particulate material within the electrically conductive container is very firmly compacted, and a rigid body of material is provided. Any one of numerous types of particulate material may be employed. For example, a body of electrical superconductive material of any desired size and shape can be produced by this method by the use of superconducting particulate material. A method and system for selecting various parameters which enable the material to be "over-pressure" and densified to densities in excess of 90 % of the material's maximum density is also illustrated in another embodiment of the invention. The various parameters include establishing a stand-off distance, a container wall density and thickness, a fill density and a compressibility value for the material. Once the various parameters are established and for a selected material, the material is magnetically compacted to over-pressure the material to a pressure level which exceeds the pressure applied by a wall of the container. This, in turn, enables the system and method to densify the material to densities in excess of 90 % of its maximum density.

    Abstract translation: 用于从颗粒材料生产非常致密的材料的结构和方法。 将颗粒材料放置在导电容器内。 电磁线圈或线圈包围导电容器,并且使大的电流流过螺线管或线圈。 当电流流过螺线管或线圈时,在导电容器上产生大的磁压力,并且导电容器被压缩,并且其横向尺寸减小。 因此,导电容器内的颗粒材料非常牢固地压实,并且提供了刚体材料。 可以使用多种类型的颗粒材料中的任何一种。 例如,通过使用超导颗粒材料,可以通过该方法制造任何所需尺寸和形状的电极超导材料体。 在本发明的另一个实施例中还示出了用于选择能使材料“超压”并且致密化到超过材料最大密度的90%的密度的各种参数的方法和系统。 各种参数包括确定材料的间隔距离,容器壁密度和厚度,填充密度和压缩性值。 一旦建立了各种参数并且对于所选择的材料,材料被磁力压实以将材料过压到超过由容器的壁施加的压力的压力水平。 这又使系统和方法使材料的密度达到其最大密度的90%以上。

    STRONGLY-LINKED OXIDE SUPERCONDUCTOR AND A METHOD OF ITS MANUFACTURE
    7.
    发明申请
    STRONGLY-LINKED OXIDE SUPERCONDUCTOR AND A METHOD OF ITS MANUFACTURE 审中-公开
    强连接氧化物超导体及其制造方法

    公开(公告)号:WO1993023884A1

    公开(公告)日:1993-11-25

    申请号:PCT/US1993003571

    申请日:1993-04-13

    Abstract: A strongly-linked polycrystalline oxide superconductor article includes an oxide superconductor selected from the group consisting of 124-type and 247-type oxide superconductors having fine, highly aligned oxide superconductor grains less than 50 mu m along a longest dimension. The oxide superconductor article has at least a 25 % retention of critical current density in a 0.1 Tesla field. A method for preparing a strongly-linked oxide superconductor includes shaping a finely divided metallic precursor of an oxide superconductor; oxidizing the finely divided metallic precursor to produce a finely divided sub-oxide species while avoiding conversion of an appreciable amount of the sub-oxide species into the oxide superconductor; annealing and deforming the article, in either order, the annealing carried out at a temperature and for a time sufficient to convert some of the sub-oxide species into fine grains of the oxide superconductor thereby forming a mixture of sub-oxide species and oxide superconductor and the deformation carried out such that the fine grains of oxide superconductor are rotated into alignment parallel to an intended current carrying direction of the article without fracturing or pulverization of the oxide superconductor grains; alternating annealing and deformation of the article until no further improvement in alignment is observed; and subjecting the aligned grains to a final anneal in order to react any remaining sub-oxide species and maximize the growth and sintering of existing aligned grains.

    Abstract translation: 强连接的多晶氧化物超导体制品包括选自124型和247型氧化物超导体的氧化物超导体,其具有沿着最长尺寸小于50微米的精细高度排列的氧化物超导体颗粒。 氧化物超导体制品在0.1特斯拉场中具有至少25%的临界电流密度保留。 一种制备强连接的氧化物超导体的方法包括使细分的氧化物超导体的金属前体成形; 氧化细碎的金属前体以产生细碎的亚氧化物物质,同时避免将相当数量的亚氧化物物质转化成氧化物超导体; 对制品进行退火和变形,以任何顺序进行退火,该退火在足以将一些氧化物种类转化为氧化物超导体的细晶粒的温度和时间下进行,从而形成次氧化物种类和氧化物超导体的混合物 并且进行变形,使得氧化物超导体的细晶粒在不破坏或粉碎氧化物超导体晶粒的同时使其平行于制品的预期电流方向旋转成对准; 交替退火和变形,直到观察不到进一步改善; 并使对准的晶粒进行最终退火,以使任何剩余的亚氧化物物质反应并使现有对准晶粒的生长和烧结最大化。

    HIGH-Tc SUPERCONDUCTING CERAMIC OXIDE PRODUCTS AND MACROSCOPIC AND MICROSCOPIC METHODS OF MAKING THE SAME
    8.
    发明申请
    HIGH-Tc SUPERCONDUCTING CERAMIC OXIDE PRODUCTS AND MACROSCOPIC AND MICROSCOPIC METHODS OF MAKING THE SAME 审中-公开
    高Tc超导陶瓷氧化物产品及其制备方法及其微观方法

    公开(公告)号:WO1992022931A1

    公开(公告)日:1992-12-23

    申请号:PCT/US1992004827

    申请日:1992-06-15

    Applicant: ZHOU, Dawei

    Abstract: The present invention relates to completely sealed high-Tc superconducting ceramic oxide products, and method for making such products. One method includes pressing a superconducting ceramic oxide powder (26) into a hollow body (24) of a material inert to oxygen; sintering the ceramic oxide powder; and then sealing any openings of the body. Optionally, a step of applying multiple pulses of alternate magnetic field to the powder during its sintering can be included. A second method includes making a high-Tc superconducting ceramic oxide thin film (100); optionally sintering the thin film in a furnace (102), while a magnetic field is applied through use of solenoids (106); and then removing partial oxygen content of the thin film through use of a scanning tunneling electron treatment machine (114, 116, 120) thereby forming an insulation layer between two high-Tc superconducting domains of the thin film.

    Abstract translation: 本发明涉及完全密封的高Tc超导陶瓷氧化物产品及其制造方法。 一种方法包括将超导陶瓷氧化物粉末(26)压入到对氧惰性的材料的中空体(24)中; 烧结陶瓷氧化物粉末; 然后密封身体的任何开口。 可选地,可以包括在其烧结期间向粉末施加多个交替磁场脉冲的步骤。 第二种方法包括制造高Tc超导陶瓷氧化物薄膜(100); 可选地在炉(102)中烧结薄膜,同时通过使用螺线管(106)施加磁场; 然后通过使用扫描隧道电子处理机(114,116,120)去除薄膜的部分氧含量,由此在薄膜的两个高Tc超导畴之间形成绝缘层。

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