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公开(公告)号：US10774195B2
公开(公告)日：2020-09-15
申请号：US16700205
申请日：2019-12-02
申请人： NanoXplore Inc.
摘要： Embodiments described herein relate generally to systems and methods for manufacturing a master batch with a graphitic material dispersed in a polymer matrix. In some embodiments, a method for manufacturing the master batch can include combining the graphitic material with a polymer, adding a supercritical fluid to the mixture, and depressurizing the supercritical fluid to remove the supercritical fluid. In some embodiments, the method includes mixing the graphitic material and the polymer for a first time period to form a first mixture and transferring the supercritical fluid to the first mixture to form a second mixture. In some embodiments, the method includes mixing the second mixture for a second time period and depressurizing the second mixture to allow the supercritical fluid to transition to a gas phase.
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公开(公告)号：US10519040B2
公开(公告)日：2019-12-31
申请号：US15854419
申请日：2017-12-26
申请人： NanoXplore Inc.
IPC分类号： C01B32/19 , C30B33/00 , C30B29/02 , C30B29/60 , C30B33/06 , C30B29/64 , C30B33/04 , C30B29/16 , H01G11/36 , H01M4/587 , C01B32/184 , C01B32/23 , B82Y30/00 , B82Y40/00
摘要： Embodiments described herein relate generally to the large scale production of functionalized graphene. In some embodiments, a method for producing functionalized graphene includes combining a crystalline graphite with a first electrolyte solution that includes at least one of a metal hydroxide salt, an oxidizer, and a surfactant. The crystalline graphite is then milled in the presence of the first electrolyte solution for a first time period to produce a thinned intermediate material. The thinned intermediate material is combined with a second electrolyte solution that includes a strong oxidizer and at least one of a metal hydroxide salt, a weak oxidizer, and a surfactant. The thinned intermediate material is then milled in the presence of the second electrolyte solution for a second time period to produce functionalized graphene.
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公开(公告)号：US09890046B2
公开(公告)日：2018-02-13
申请号：US15413804
申请日：2017-01-24
IPC分类号： C01B31/00 , C30B29/64 , H01M4/587 , H01G11/36 , C30B29/16 , C30B33/00 , C01B31/04 , B82Y30/00 , B82Y40/00
CPC分类号： C01B32/19 , B82Y30/00 , B82Y40/00 , C01B32/184 , C01B32/23 , C01B2204/04 , C01P2006/40 , C30B29/02 , C30B29/16 , C30B29/60 , C30B29/64 , C30B33/00 , C30B33/04 , C30B33/06 , H01G11/36 , H01M4/587 , Y10S977/734 , Y10S977/847 , Y10S977/948
摘要： Embodiments described herein relate generally to the large scale production of functionalized graphene. In some embodiments, a method for producing functionalized graphene includes combining a crystalline graphite with a first electrolyte solution that includes at least one of a metal hydroxide salt, an oxidizer, and a surfactant. The crystalline graphite is then milled in the presence of the first electrolyte solution for a first time period to produce a thinned intermediate material. The thinned intermediate material is combined with a second electrolyte solution that includes a strong oxidizer and at least one of a metal hydroxide salt, a weak oxidizer, and a surfactant. The thinned intermediate material is then milled in the presence of the second electrolyte solution for a second time period to produce functionalized graphene.
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4.发明授权Large scale production of thinned graphite, graphene, and graphite-graphene composites 有权大规模生产薄型石墨，石墨烯和石墨 - 石墨烯复合材料公开(公告)号：US09469542B2
公开(公告)日：2016-10-18
申请号：US14978566
申请日：2015-12-22
IPC分类号： C01B31/04 , C01B31/02 , H01B1/04 , B82Y30/00 , B82Y40/00 , C30B29/02 , B02C17/20 , B02C17/22 , C09K5/14
CPC分类号： C01B31/0446 , B02C17/20 , B02C17/22 , B82Y40/00 , C01B31/04 , C01B31/0423 , C01B32/184 , C01B32/20 , C01B32/225 , C01B2204/04 , C09D1/00 , C09D5/084 , C09D5/24 , C09K5/14 , C10M103/02 , C10M2201/0413 , C30B29/02 , C30B29/64 , C30B33/00 , H01B1/04
摘要： Embodiments described herein relate generally to large scale synthesis of thinned graphite and in particular, few layers of graphene sheets and graphene-graphite composites. In some embodiments, a method for producing thinned crystalline graphite from precursor crystalline graphite using wet ball milling processes is a disclosed herein. The method includes transferring crystalline graphite into a ball milling vessel that includes a grinding media. A first and a second solvent are transferred into the ball milling vessel and the ball milling vessel is rotated to cause the shearing of layers of the crystalline graphite to produce thinned crystalline graphite.
摘要翻译： 本文所述的实施方案一般涉及薄型石墨的大规模合成，特别是石墨烯片和石墨烯 - 石墨复合材料的层数较少。 在一些实施方案中，本文公开了一种使用湿式球磨法从前体晶体石墨生产薄化晶体石墨的方法。 该方法包括将结晶石墨转移到包括研磨介质的球磨容器中。 将第一和第二溶剂转移到球磨容器中，并且使球磨容器旋转以使晶体石墨层的剪切产生变薄的结晶石墨。
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公开(公告)号：US20230138169A1
公开(公告)日：2023-05-04
申请号：US17799338
申请日：2021-02-16
申请人： NanoXplore Inc.
发明人： Scott Murray , Allan James , Liya Wang
摘要： Graphene-modified polymeric foam materials are provided that are amenable to conventional foams to yield articles with superior properties relative to like articles absent the graphene cell modifier. Graphene-based cell modifiers are incorporated in the polymer before or during the foaming process to not only improve the mechanical, thermal, electrical, fire retardant, or barrier properties of the polymer matrix itself, but also help modify the size, density, and morphology of cells in the foam, thereby tailoring the properties of the final foam articles. The graphene-modified polymeric foam materials may be utilized for the manufacturing of articles for mechanical, thermal, noise reduction, or sound absorption applications. The graphene-modified foams and articles made thereof have the advantages higher mechanical strength, better thermal stability, and better sound absorption properties as compared to the conventional polymeric foams such as materials made by copolymer polyol.
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公开(公告)号：US20220194799A9
公开(公告)日：2022-06-23
申请号：US16692201
申请日：2019-11-22
申请人： NanoXplore Inc.
IPC分类号： C01B32/19 , C30B33/00 , C30B29/02 , C30B29/60 , C01B32/23 , C30B33/06 , C30B29/64 , C30B33/04 , C30B29/16 , H01G11/36 , H01M4/587 , C01B32/184
摘要： Embodiments described herein relate generally to the large scale production of functionalized graphene. In some embodiments, a method for producing functionalized graphene includes combining a crystalline graphite with a first electrolyte solution that includes at least one of a metal hydroxide salt, an oxidizer, and a surfactant. The crystalline graphite is then milled in the presence of the first electrolyte solution for a first time period to produce a thinned intermediate material. The thinned intermediate material is combined with a second electrolyte solution that includes a strong oxidizer and at least one of a metal hydroxide salt, a weak oxidizer, and a surfactant. The thinned intermediate material is then milled in the presence of the second electrolyte solution for a second time period to produce functionalized graphene.
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公开(公告)号：US20180155520A1
公开(公告)日：2018-06-07
申请号：US15877990
申请日：2018-01-23
申请人： NanoXplore Inc.
发明人： Soroush NAZARPOUR , Naiheng SONG
CPC分类号： C08K3/042 , B05D1/00 , B05D1/045 , B05D1/06 , B05D7/02 , B82Y30/00 , B82Y40/00 , C08J3/128 , C08J3/203 , C08J2323/06 , C08J2375/04 , C08J2377/06 , C08K7/00 , C08K2201/005 , C08K2201/011 , C09D7/70 , C09D7/80 , Y10S977/753 , Y10S977/842
摘要： Embodiments described herein relate generally to the production of graphene/polymer compounds. In some embodiments, a method for producing graphene/polymer compounds includes compounding graphene nanoflakes with non-conductive polymer hosts via electrospray coating techniques, taking advantage of the highly electrostatically chargeable properties of graphene to de-agglomerate and further exfoliate the graphene nanoflakes in-situ, and providing uniform and well-dispersed graphene nanoflake coating on various non-conductive polymer hosts, such as polymer fine particles, pellets, fibers, fabrics, non-woven, film, and formed articles. In some embodiments, the deposition of the graphene nanoflakes onto the hosts may be performed in combination with other components, such as but not limited to metal oxides and polymers. The method can be a batch or a continuous process, and is suitable for large scale production of graphene coated materials such as graphene/polymer compound, which can be further processed by, for example, extrusion, compression molding, or injection molding, to yield formed articles.
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8.发明申请公开(公告)号：US20170096343A1
公开(公告)日：2017-04-06
申请号：US15270855
申请日：2016-09-20
IPC分类号： C01B31/04 , C09D5/08 , C09D5/24 , C09K5/14 , C30B29/02 , C30B33/00 , C30B29/64 , H01B1/04 , C09D1/00 , C10M103/02
CPC分类号： C01B31/0446 , B02C17/20 , B02C17/22 , B82Y40/00 , C01B32/184 , C01B32/20 , C01B32/225 , C01B2204/04 , C09D1/00 , C09D5/084 , C09D5/24 , C09K5/14 , C10M103/02 , C10M2201/0413 , C30B29/02 , C30B29/64 , C30B33/00 , H01B1/04
摘要： Embodiments described herein relate generally to large scale synthesis of thinned graphite and in particular, few layers of graphene sheets and graphene-graphite composites. In some embodiments, a method for producing thinned crystalline graphite from precursor crystalline graphite using wet ball milling processes is disclosed herein. The method includes transferring crystalline graphite into a ball milling vessel that includes a grinding media. A first and a second solvent are transferred into the ball milling vessel and the ball milling vessel is rotated to cause the shearing of layers of the crystalline graphite to produce thinned crystalline graphite.
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公开(公告)号：US20230005638A1
公开(公告)日：2023-01-05
申请号：US17739949
申请日：2022-05-09
申请人： NanoXplore Inc.
IPC分类号： H01B1/04 , B02C17/20 , B02C17/22 , C01B32/20 , C01B32/225 , C01B32/21 , B82Y30/00 , C30B29/02 , C30B29/64 , C30B33/00 , C09K5/14 , C09D1/00 , C09D5/08 , C09D5/24 , C10M103/02 , C01B32/184
摘要： Embodiments described herein relate generally to large scale synthesis of thinned graphite and in particular, few layers of graphene sheets and graphene-graphite composites. In some embodiments, a method for producing thinned crystalline graphite from precursor crystalline graphite using wet ball milling processes is disclosed herein. The method includes transferring crystalline graphite into a ball milling vessel that includes a grinding media. A first and a second solvent are transferred into the ball milling vessel and the ball milling vessel is rotated to cause the shearing of layers of the crystalline graphite to produce thinned crystalline graphite.
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公开(公告)号：US11367540B2
公开(公告)日：2022-06-21
申请号：US16409153
申请日：2019-05-10
申请人： NanoXplore Inc.
IPC分类号： H01B1/04 , B82Y30/00 , B02C17/20 , B02C17/22 , C01B32/20 , C01B32/225 , C01B32/21 , C30B29/02 , C30B29/64 , C30B33/00 , C09K5/14 , C09D1/00 , C09D5/08 , C09D5/24 , C10M103/02 , C01B32/184 , B82Y40/00
摘要： Embodiments described herein relate generally to large scale synthesis of thinned graphite and in particular, few layers of graphene sheets and graphene-graphite composites. In some embodiments, a method for producing thinned crystalline graphite from precursor crystalline graphite using wet ball milling processes is disclosed herein. The method includes transferring crystalline graphite into a ball milling vessel that includes a grinding media. A first and a second solvent are transferred into the ball milling vessel and the ball milling vessel is rotated to cause the shearing of layers of the crystalline graphite to produce thinned crystalline graphite.
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