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公开(公告)号：US09475220B2
公开(公告)日：2016-10-25
申请号：US14176366
申请日：2014-02-10
Applicant: BASF SE
Inventor： Olaf Jacobmeier , Gunnar Kampf
CPC classification number: C08J9/08 , B29C44/321 , B29C44/326 , B29C44/461 , B32B3/266 , B32B15/046 , B32B2250/40 , B32B2266/0278 , B32B2419/00 , B32B2509/10
Abstract: The invention relates to an improved process for producing composite elements comprising at least one outer layer and at least one isocyanate-based rigid foam layer by means of a fixed applicator apparatus and in which the flowable starting material comprises the following components: A) at least one polyisocyanate, B) at least one compound which reacts with isocyanate groups to form urethane, C) at least one blowing agent, D) catalysts comprising at least one compound D1) which catalyzes isocyanurate formation and at least one compound D2) which catalyzes polyurethane formation, comprising at least one amino group, and E) optionally auxiliaries and additives, where the manner of use of component A) and of component B) is such that the isocyanate index is at least 180, and where the ratio by weight of the compound D2) to the compound D1) is from 0.75 to 8.
Abstract translation: 本发明涉及一种用于生产复合元件的改进方法，所述复合元件包括至少一个外层和至少一个异氰酸酯基硬质泡沫层，其中固定的施用装置，其中可流动起始材料包括以下组分：A）至少 一种多异氰酸酯，B）至少一种与异氰酸酯基团反应形成氨基甲酸酯的化合物，C）至少一种发泡剂，D）包含至少一种催化异氰脲酸酯形成的化合物D1）和至少一种催化聚氨酯的化合物D2） 形成，包含至少一个氨基，以及E）任选的助剂和添加剂，其中组分A）和组分B）的使用方式使得异氰酸酯指数为至少180，并且其中重量比 化合物D2）化合物D1）为0.75至8。
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公开(公告)号：US08895636B2
公开(公告)日：2014-11-25
申请号：US13731317
申请日：2012-12-31
Applicant: BASF SE
Inventor： Gunnar Kampf
CPC classification number: C08G18/34 , C08G18/225 , C08G18/4018 , C08G18/4288 , C08G18/7664 , C08G2101/0025 , C08G2105/02
Abstract: Rigid polyurethane foams or rigid polyisocyanurate foams with low brittleness are produced by the reaction of polyisocyanate polyetherester polyols based on aromatic dicarboxylic acids obtained by esterification of a dicarboxylic acid composition containing aromatic dicarboxylic acids and aliphatic dicarboxylic acids, fatty acids, aliphatic or cycloaliphatic diols having 2 to 18 carbon atoms or alkoxylates thereof, and a polyether polyol having a functionality of not less than 2.
Abstract translation: 具有低脆性的刚性聚氨酯泡沫体或刚性聚异氰脲酸酯泡沫体是通过基于通过酯化含有芳族二羧酸和脂族二羧酸的二羧酸组合物获得的芳族二羧酸的多异氰酸酯聚醚酯多元醇，脂肪酸，脂族或脂环族二醇 至18个碳原子或烷氧基，以及官能度不小于2的聚醚多元醇。
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公开(公告)号：US20190153187A1
公开(公告)日：2019-05-23
申请号：US16099897
申请日：2017-05-18
Applicant: BASF SE
Inventor： Gianpaolo Tomasi , Ludwig Windeler , Gunnar Kampf , Ulrich Gaukesbrink
IPC: C08J9/14 , C08G18/42 , C08G18/50 , C08G18/48 , C08G18/40 , C08G18/76 , C08G18/22 , C08G18/18 , C08G18/16 , C08K5/521 , C08J9/00 , F16L59/00
Abstract: Provided herein is a process for preparing a rigid polyisocyanurate foam including reacting a composition (A) including a polyesterol, a blowing agent including formic acid, a catalyst system including at least one trimerization catalyst and at least one polyisocyanate as component (B), wherein composition (A) further includes at least one polyether alcohol prepared by addition of alkylene oxides to toluenediamine. Further provided herein is a rigid polyisocyanurate foam obtained through the process described herein and the use of said rigid polyisocyanurate foam as insulating material.
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公开(公告)号：US20210198412A1
公开(公告)日：2021-07-01
申请号：US17267864
申请日：2019-08-08
Applicant: BASF SE
IPC: C08G18/42 , C08K5/521 , C08J9/14 , C08J9/00 , C08G18/76 , C08G18/66 , C08G18/65 , C08G18/48 , C08G18/40 , C08G18/32 , C08G18/24 , C08G18/18 , C08G18/16
Abstract: Described herein are processes for producing a polyurethane foam by mixing the following: (a) polymeric MDI with less than 40% by weight content of difunctional MDI and an aliphatic halogenated hydrocarbon compound (d1) composed of 2 to 5 carbon atoms and of at least one hydrogen atom and of at least one fluorine and/or chlorine atom, where the compound (d1) includes at least one carbon-carbon double bond, to give an isocyanate component (A), and reacting with a polyol component (b) to give the polyurethane foam. Also described herein is a polyurethane foam obtainable by said process.
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公开(公告)号：US20130324626A1
公开(公告)日：2013-12-05
申请号：US13897690
申请日：2013-05-20
Applicant: BASF SE
Inventor： Roland FABISIAK , Gunnar Kampf , Lars Schoen , Olaf Jacobmeier
IPC: C08J9/00
CPC classification number: C08J9/0038 , C08G18/092 , C08G18/225 , C08G18/4018 , C08G18/4288 , C08G18/7664 , C08G2101/0025 , C08J2375/04
Abstract: The invention relates to a process for producing rigid polyurethane foams by reaction of A) one or more organic polyisocyanates, B) one or more polyester polyols, C) optionally one or more polyether polyols, D) a flame-retardant mixture, E) further auxiliaries or addition agents, F) one or more blowing agents, and also G) catalysts, wherein said flame-retardant mixture D) comprises d1) 10 to 90 wt %, based on the amount of flame-retardant mixture, of a flame retardant having a boiling point of not more than 220° C., and d2) 10 to 90 wt %, based on the amount of flame-retardant mixture, of a phosphorus-containing flame retardant having a boiling point of above 220° C., wherein said components d1) and d2) total 100 wt %.
Abstract translation: 本发明涉及通过A）一种或多种有机多异氰酸酯，B）一种或多种聚酯多元醇，C）任选的一种或多种聚醚多元醇，D）阻燃混合物的反应生产硬质聚氨酯泡沫的方法，E）进一步 助剂或添加剂，F）一种或多种发泡剂，以及G）催化剂，其中所述阻燃混合物D）包含d1）基于阻燃混合物的量的阻燃剂的10至90重量％的阻燃剂 沸点为220℃以下，d2为10〜90重量％，相对于阻燃剂混合物，沸点为220℃以上的含磷阻燃剂为10〜90重量％ 其中所述组分d1）和d2）总共为100重量％。
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Patent Agency Ranking
公开(公告)号：US20130231410A1
公开(公告)日：2013-09-05
申请号：US13780508
申请日：2013-02-28
Applicant: BASF SE
Inventor： Olaf JACOBMEIER , Gunnar Kampf , Christian Koenig
IPC: C08J9/04
CPC classification number: C08J9/04 , C08G18/225 , C08G18/3284 , C08G18/4891 , C08G18/6688 , C08G2101/0025 , C08G2101/005 , C08G2101/0083
Abstract: The invention relates to rigid polyurethane foams obtainable by reaction of A) organic or modified organic polyisocyanates or mixtures thereof, B) compounds having two or more isocyanate-reactive hydrogen atoms in the presence of C) optionally further polyester polyols, D) optionally polyetherol polyols, E) optionally flame retardants, F) one or more blowing agents, G) catalysts, and H) optionally further auxiliaries and/or additives, wherein component B) comprises the reaction product of a1) 15 to 40 wt % of one or more polyols or polyamines having an average functionality of 2.5 to 8, a2) 2 to 30 wt % of one or more fatty acids and/or fatty acid monoesters, a3) 35 to 70 wt % of one or more alkylene oxides of 2 to 4 carbon atoms.
Abstract translation: 本发明涉及通过A）有机或改性有机多异氰酸酯或其混合物的反应获得的硬质聚氨酯泡沫; B）在C）任选的其它聚酯多元醇存在下具有两个或多个异氰酸酯反应性氢原子的化合物，D）任选的聚醚多元醇 ，E）任选的阻燃剂，F）一种或多种发泡剂，G）催化剂，和H）任选的其它助剂和/或添加剂，其中组分B）包含a1）15至40重量％的一种或多种 平均官能度为2.5〜8的多元醇或多胺，a2）2〜30重量％的一种或多种脂肪酸和/或脂肪酸单酯，a3）35〜70重量％的一种或多种2〜4碳的氧化烯 原子
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公开(公告)号：US10472454B2
公开(公告)日：2019-11-12
申请号：US13740732
申请日：2013-01-14
Applicant: BASF SE
Inventor： Gunnar Kampf
Abstract: The present invention relates to a process for preparing rigid polyurethane foams or rigid polyisocyanurate foams by using certain polyetherester polyols B) based on aromatic dicarboxylic acids, optionally further polyester polyols C), which differ from those of component B), and polyether polyols D), wherein the mass ratio of total components B) and optionally C) to component D) is less than 1.6. The present invention also relates to the rigid foams thus obtainable and to their use for producing sandwich elements having rigid or flexible outer layers. The present invention further relates to the underlying polyol components.
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公开(公告)号：US10259906B2
公开(公告)日：2019-04-16
申请号：US15117960
申请日：2015-01-27
Applicant: BASF SE
Inventor： Tobias Kaluschke , Gunnar Kampf
IPC: C08G63/672 , C08G18/48 , C08G18/76 , C08G18/40 , C08G18/42 , C08G63/668 , C08G18/08 , C08G18/18 , C08J9/00 , C08J9/14 , C08G101/00
Abstract: The present invention relates to polyester polyols obtainable or obtained by esterification of 10 to 70 mol % of at least one compound from the group consisting of terephthalic acid (TPA), dimethyl terephthalate (DMT), polyethylene terephthalate (PET), phthalic anhydride (PA), phthalic acid and isophthalic acid, 0.1 to 30 mol % of one or more fatty acids and/or fatty acid derivatives, 10 to 70 mol % of one or more aliphatic or cycloaliphatic diols having 2 to 18 carbon atoms or alkoxylates thereof, 5 to 70 mol % of a polyether polyol prepared by alkoxylating an aromatic starter molecule having a functionality of not less than 2, and of 0 to 70 mol % of a tri- or polyol other than the polyether polyol, all based on the total amount of the components used, wherein the amounts used of the components add up to 100 mol %. The present invention further relates to a process for producing rigid polyurethane or polyisocyanurate foams which comprises reacting an isocyanate component with a polyol component (PK) comprising a polyester polyol of the present invention and further components, to the polyol component as such and also to the rigid polyurethane or polyisocyanurate foams obtainable or obtained by a process of the present invention. The present invention also relates to the method of using a polyester polyol (P1) of the present invention in the manufacture of rigid polyurethane foams or rigid polyisocyanurate foams.
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公开(公告)号：US20170209897A1
公开(公告)日：2017-07-27
申请号：US15500399
申请日：2015-07-14
Applicant: BASF SE
Inventor： Oliver Clamor , Gunnar Kampf , Andrea Eisenhardt , Erhard Gleinig , Sven Moennig , Sarunas Turcinskas , Dirk Weinrich
CPC classification number: B05D1/02 , B05D1/28 , B32B5/18 , B32B5/20 , B32B5/22 , B32B5/24 , B32B5/32 , B32B7/12 , B32B15/08 , B32B15/095 , B32B15/14 , B32B15/16 , B32B27/08 , B32B27/12 , B32B27/18 , B32B27/20 , B32B27/40 , B32B2255/06 , B32B2255/062 , B32B2255/20 , B32B2255/26 , B32B2255/28 , B32B2260/025 , B32B2260/046 , B32B2266/0278 , B32B2307/304 , B32B2307/7246 , B32B2607/00 , E04B1/762 , E04B2001/7691
Abstract: The present invention relates to a process for the production of a composite element. The process includes (i) provision of an outer layer with an uncoated surface and a coated surface coated at least partially with a composition (B) including at least one inorganic material, (ii) treatment of the uncoated surface of the outer layer and (iii) application, to the treated surface of the outer layer, of a composition (Z2) suitable for the production of a polyurethane foam and/or polyisocyanurate foam. The present invention further relates to a composite element obtainable or obtained by a process of the invention, and also to the use of a composite element obtainable or obtained by a process of the invention or of a composite element of the invention as insulation material or in the construction of façades.
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公开(公告)号：US09353234B2
公开(公告)日：2016-05-31
申请号：US13780508
申请日：2013-02-28
Applicant: BASF SE
Inventor： Olaf Jacobmeier , Gunnar Kampf , Christian Koenig
CPC classification number: C08J9/04 , C08G18/225 , C08G18/3284 , C08G18/4891 , C08G18/6688 , C08G2101/0025 , C08G2101/005 , C08G2101/0083
Abstract: The invention relates to rigid polyurethane foams obtainable by reaction of A) organic or modified organic polyisocyanates or mixtures thereof, B) compounds having two or more isocyanate-reactive hydrogen atoms in the presence of C) optionally further polyester polyols, D) optionally polyetherol polyols, E) optionally flame retardants, F) one or more blowing agents, G) catalysts, and H) optionally further auxiliaries and/or additives, wherein component B) comprises the reaction product of a1) 15 to 40 wt % of one or more polyols or polyamines having an average functionality of 2.5 to 8, a2) 2 to 30 wt % of one or more fatty acids and/or fatty acid monoesters, a3) 35 to 70 wt % of one or more alkylene oxides of 2 to 4 carbon atoms.
Abstract translation: 本发明涉及通过A）有机或改性有机多异氰酸酯或其混合物的反应获得的硬质聚氨酯泡沫; B）在C）任选的其它聚酯多元醇存在下具有两个或多个异氰酸酯反应性氢原子的化合物，D）任选的聚醚多元醇 ，E）任选的阻燃剂，F）一种或多种发泡剂，G）催化剂，和H）任选的其它助剂和/或添加剂，其中组分B）包含a1）15至40重量％的一种或多种 平均官能度为2.5〜8的多元醇或多胺，a2）2〜30重量％的一种或多种脂肪酸和/或脂肪酸单酯，a3）35〜70重量％的一种或多种2〜4碳的氧化烯 原子
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