Copper film deposition method
    91.
    发明申请
    Copper film deposition method 有权
    铜膜沉积法

    公开(公告)号:US20070197398A1

    公开(公告)日:2007-08-23

    申请号:US10591476

    申请日:2005-02-25

    IPC分类号: H01L39/24

    摘要: A Cu film is deposited on a substrate by ALD (Atomic Layer Deposition) process, in which: a Cu-carboxyl acid complex or a derivative thereof having a high vapor pressure and wettability to a base is used in a gasified state; H2 is used as a reductive gas; and a step of adsorbing a source material gas to a substrate and a step of forming a Cu film by reducing the adsorbed gas with a reductive gas are repeated alternately. With this method, a conformal Cu film having excellent quality can be formed.

    摘要翻译: 通过ALD(原子层沉积)方法将Cu膜沉积在基板上,其中:在气化状态下使用具有高蒸气压和对碱的润湿性的Cu-羧酸络合物或其衍生物; H 2 2被用作还原气体; 并且将源材料气体吸附到基板的步骤和通过用还原气体还原吸附气体形成Cu膜的步骤交替地重复。 通过这种方法,可以形成具有优良品质的共形Cu膜。

    Processing method
    92.
    发明申请
    Processing method 审中-公开
    加工方法

    公开(公告)号:US20070160757A1

    公开(公告)日:2007-07-12

    申请号:US11717183

    申请日:2007-03-13

    IPC分类号: C23C16/00

    摘要: In a processing apparatus which performs a film deposition by alternately supplying a plurality of source gases, the source gases are prevented from reacting within an exhaust pipe so as to prevent the exhaust pipe from clogging due to a reaction by-product. A gas supply to a processing container is switched between a TiCl4 supply system and a NH3 supply system. Additionally, a gas exhaust from the processing container is switched between a TiCl4 exhaust system and a NH3 exhaust system. The gas exhaust is switched to the TiCl4 exhaust system when the gas supply is switched to the TiCl4 supply system, and the gas exhaust is switched to the NH3 exhaust system when the gas supply is switched to the NH3 supply system. The switching is performed by a stop valve provided to each of the supply system and the exhaust system.

    摘要翻译: 在通过交替供给多个源气体进行膜沉积的处理装置中,防止源气体在排气管内发生反应,以防止排气管因反应副产物而堵塞。 供给到处理容器的气体在TiCl 4供应系统和NH 3供应系统之间切换。 此外,来自处理容器的排气在TiCl 4排气系统和NH 3排气系统之间切换。 当气体供应切换到TiCl 4供应系统时,排气被切换到TiCl 4排气系统,并且排气被切换到NH 3 3气体供应系统切换到NH 3供应系统时。 通过设置在供给系统和排气系统中的每一个的截止阀进行切换。

    Cleaning method of treatment equipment and treatment equipment
    93.
    发明授权
    Cleaning method of treatment equipment and treatment equipment 有权
    处理设备和处理设备的清洁方法

    公开(公告)号:US07172657B2

    公开(公告)日:2007-02-06

    申请号:US09801825

    申请日:2001-03-09

    IPC分类号: B08B3/10 B08B9/00

    CPC分类号: C23C16/4405

    摘要: In a state of the inside of a treatment chamber of treatment equipment being evacuated, therein a cleaning gas containing trifluoroaceticacid (TFA) as a cleaning agent is supplied. Metal such as copper used in the formation of an interconnection or an electrode and stuck on an inner wall surface of the treatment chamber, when coming into contact with the cleaning agent (TFA) in the cleaning gas, without forming an oxide or a metallic salt, is directly complexed. The complex is sublimed due to the evacuation and is exhausted outside the treatment chamber. Accordingly, at less labor and low cost, the cleaning can be efficiently implemented.

    摘要翻译: 在处理设备的处理室的内部被抽真空的状态下,其中提供含有三氟乙酸(TFA)作为清洁剂的清洁气体。 当形成互连或电极并且在与清洁气体中的清洁剂(TFA)接触时粘附在处理室的内壁表面上的金属,例如铜,而不形成氧化物或金属盐 ,直接复合。 复合体由于排空而升华,并在处理室外排出。 因此,以较少的劳动力和低成本,可以有效地实施清洁。

    Processing device and processing method
    96.
    发明申请
    Processing device and processing method 审中-公开
    处理装置及处理方法

    公开(公告)号:US20050211167A1

    公开(公告)日:2005-09-29

    申请号:US10517345

    申请日:2003-06-09

    摘要: The ceiling surface (12b) of a chamber (12) is substantially entirely formed with a gas supply port (19). Further, the gas supply port (19) has shower head (20) fitted therein. The peripheral edge of the ceiling surface (12b) has connected thereto a second side wall (12d) forming an angle greater than 90 degrees with ceiling surface (12b). Further, the side surface of a susceptor (16) is formed such that it forms an angle greater than 90 degrees with a mounting surface for a wafer (W) and is substantially parallel with the second side wall (12d) of the chamber (12). Further, the susceptor (16) is disposed such that the distance (L2) between its side surface and the second side wall (12d) is greater than the distance (L1) between the shower head (20) and the wafer (W).

    摘要翻译: 室(12)的顶表面(12b)基本上完全由气体供给口(19)形成。 此外,气体供给口(19)具有嵌入其中的喷头(20)。 天花板表面(12b)的周缘连接有形成与天花板表面(12b)大于90度的角度的第二侧壁(12d)。 此外,基座(16)的侧表面形成为与晶片(W)的安装表面形成大于90度的角度并且基本上平行于腔室的第二侧壁(12d) 12)。 此外,基座(16)设置成使得其侧表面和第二侧壁(12d)之间的距离(L 2)大于喷头(20)和晶片(20)之间的距离(L 1) W)。

    Urea synthesis process and apparatus therefor
    100.
    发明授权
    Urea synthesis process and apparatus therefor 失效
    尿素合成方法及其设备

    公开(公告)号:US5936122A

    公开(公告)日:1999-08-10

    申请号:US939126

    申请日:1997-09-26

    摘要: A vertical condenser is installed on or above a urea synthesis column to condense the mixed gas from the stripper by bringing it into contact with an absorption medium under cooling. A first down pipe for making the top part of the condenser communicate with the bottom part of the synthesis column is provided to allow the resultant condensate to flow down to the bottom part of the synthesis column by gravity. The condensate is subjected to urea synthesis together with feed ammonia or a part of feed carbon dioxide supplied thereto. The urea synthesis solution thus formed is introduced into the stripper by gravity through a second down pipe having an opening in the top part of the synthesis column. Unreacted ammonia and carbon dioxide are separated as the aforesaid mixed gas by the rest of the feed carbon dioxide and introduced into the bottom part of the aforesaid condenser so as to be condensed. Alternatively, the condensate from the vertical condenser is sucked by means of an ejector using preheated feed liquid ammonia as the driving fluid, so that it is introduced into the bottom part of the urea synthesis column and is subjected to urea synthesis.

    摘要翻译: 立式冷凝器安装在尿素合成塔上或上方,通过使其与冷却下的吸收介质接触而将来自汽提塔的混合气体冷凝。 提供用于使冷凝器的顶部与合成塔的底部连通的第一下管,以使所得的冷凝物通过重力向下流到合成塔的底部。 冷凝物与供给氨或供给二氧化碳的一部分进行尿素合成。 如此形成的尿素合成溶液通过重力通过在合成塔的顶部具有开口的第二下管引入汽提器。 未反应的氨和二氧化碳作为前述混合气体被剩余的进料二氧化碳分离,并被引入上述冷凝器的底部以便冷凝。 或者,来自垂直冷凝器的冷凝物借助于使用预热的进料液氨作为驱动流体的喷射器吸入,从而将其引入到尿素合成塔的底部并进行尿素合成。