Abstract:
A METHOD OF PREPARING A LUBRICATING OIL COMPOSITION OF DETERGENT PROPERTIES CONTAINING A NORMAL CALCIUM ALKYLPHENOLATE COMPRISING CONTACTING IN THE PRESENCE OF ACETIC ACID, ALKYLPHENOL, A CALCIUM MEMBER SELECTED FROM THE GROUP CONSISTING OF CALCIUM OXIDE AND CALCIUM HYDROXIDE AND A HYDROCARBON OIL OF LUBRICATING VISCOSITY.
Abstract:
Antistatic fuel composition comprising a mixture of hydrocarbons in the gasoline, kerosene and/or furnace oil boiling ranges and a minor amount of a reaction product of an aliphatic monoamine having the formula RNH2 in which R is an aliphatic radical having from eight to 20 carbon atoms and either a fluorinated polystyrene having the empirical formula: (C16H3F25)x in which x is an average integer between 3 to 5, or a fluorinated polypropylene having the empirical formula: (C3HF5)x in which x has a value from 20 to 40, and a method for preparing the above-noted aliphatic monoamine derivatives.
Abstract:
Sulfurized and chlorinated alkylene-polyamine reaction product effective as an ashless lubricant additive and a mineral lubricating oil composition containing same.
Abstract:
A reaction product of detergent-dispersant properties in lubricating oil prepared by the sequential method of (1) reacting polyalkene of from 30 to 300 carbons with maleic anhydride to form alkenyl succinic anhydride, (2) contacting the alkenyl succinic anhydride with chlorine or bromine in the absence of hydroxylic and solvent compounds to form halogenated alkenyl succinic anhydride, (3) contacting the halogenated alkenyl succinic anhydride with alkylene polyamine to form crude reaction product of halogenated alkenyl succinic anhydride and alkylene polyamine and (4) preferably contacting the crude reaction product with a strong inorganic base and recovering the purified reaction product. Lubricant compositions containing a detergentdispersant quantity of said halogenated succinic anhydridealkylene polyamine reaction product.
Abstract:
Method of carboxylating an organic compound of the group of RC*CH, RCH2CN, indene or cyclopentadiene where R is hydrocarbyl comprising contacting under anhydrous conditions in an inert atmosphere and in the presence of an inert, aprotic, dipolar, liquid solvent, said compound with a carbonated metal phenoxide, the metal phenoxide of the formula: WHERE X is sodium or potassium, R1 is hydrogen or alkyl, and subsequently acidifying the resultant intermediate product to form the carboxylated product.
Abstract:
Method of carboxylating a compound of the group of R-C CH, RCH2CN, indene, cyclopentadiene or fluorene, where R is hydrocarbyl, comprising contacting said compound with carbon dioxide under substantially anhydrous conditions in the presence of a base of the formula: WHERE X is sodium or potassium, R1 is hydrogen or alkyl and subsequently acidifying the resultant reaction product to form the carboxylated product.
Abstract:
A PROCESS FOR PREPARING ALKANOIC ACIDS FROM VICINAL NITROALKANONES WHICH COMPRISES CONTACTIG THE VICINAL NITROALKANONE UNDER NON-AQUEOUS CONDITION WITH A CATALYST COMPRISING A SULFONIC ACID CATION EXCHANGE RESIN AT TEMPERATURES OF AT LEAST 100*C.