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公开(公告)号：US20090013872A1
公开(公告)日：2009-01-15
申请号：US12171379
申请日：2008-07-11
IPC分类号： B01D53/14
CPC分类号： B01D53/1456 , B01D53/1493 , B01D2257/308 , C10L3/10
摘要： The present invention relates to a method of removing acid gases, notably carbonyl sulfide, contained in gaseous effluents, comprising: an acid gas absorption stage by contacting the gaseous effluent with an aqueous solution comprising 2-[2-amino-1-(aminomethyl)ethoxy]ethanol, and possibly another alkanolamine and an organic compound, and at least one aqueous solution regeneration stage. The method can comprise a second aqueous solution regeneration stage. The regeneration stages are carried out by expansion and/or thermal regeneration.
摘要翻译： 本发明涉及一种除去气态流出物中含有的酸性气体，特别是羰基硫化物的方法，包括：通过使气态流出物与包含2- [2-氨基-1-（氨基甲基） 乙氧基]乙醇和可能的另一种链烷醇胺和有机化合物，以及至少一种水溶液再生阶段。 该方法可以包括第二水溶液再生阶段。 再生阶段通过膨胀和/或热再生进行。
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22.发明授权Method for processing a natural gas with extraction of the solvent contained in the purified natural gas 失效通过提取纯化天然气中所含的溶剂来处理天然气的方法公开(公告)号：US07470829B2
公开(公告)日：2008-12-30
申请号：US11057026
申请日：2005-02-14
IPC分类号： C07C7/10
CPC分类号： C10L3/102 , B01D53/1462 , B01D2257/304 , B01D2257/504 , C10L3/10
摘要： The natural gas arriving through pipe 1 is deacidified by being brought into contact with a solvent in column C2. The solvent charged with acid compounds is regenerated in zone R. The purified gas evacuated by pipe 9 includes some of the solvent. The method enables the solvent contained in the purified gas to be extracted. In zone ZA, the purified gas is brought into contact with a non-aqueous ionic liquid whose general formula is Q+ A−, where Q+ designates an ammonium, phosphonium, and/or sulfonium cation, and A− designates an anion able to form a liquid salt. The solvent-impoverished purified gas is evacuated through pipe 17. The ionic liquid charged with solvent is regenerated by heating in an evaporator DE. The solvents separated from the ionic liquid in evaporator DE are recycled.
摘要翻译： 通过管道1到达的天然气通过与C2中的溶剂接触而脱酸。 带有酸性化合物的溶剂在区域R中再生。由管道9抽出的净化气体包括一些溶剂。 该方法能够提纯纯化气体中所含的溶剂。 在区域ZA中，纯化的气体与通式为Q + A-的非水性离子液体接触，其中Q +表示铵，鏻和/或锍阳离子，A-表示能形成 液体盐 将溶剂贫化的净化气体通过管道17抽真空。通过在蒸发器DE中加热来再生装有溶剂的离子液体。 在蒸发器DE中与离子液体分离的溶剂被再循环。
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23.发明授权公开(公告)号：US07470359B2
公开(公告)日：2008-12-30
申请号：US11056279
申请日：2005-02-14
摘要： The method enables the antihydrate compounds contained in a condensed-hydrocarbon liquid feedstock arriving through pipe 1 to be extracted. The liquid feedstock is brought into contact, in zone ZA, with a non-aqueous ionic liquid having the general formula Q+ A31 , where Q+ designates an ammonium, phosphonium, and/or sulfonium cation, and A31 designates an anion able to form a liquid salt. The antihydrate compounds in the liquid hydrocarbon feedstock evacuated through pipe 2 are eliminated. The ionic liquid charged with antihydrate compounds is evacuated through pipe 3, then introduced into evaporator DE to be heated in order to evaporate the antihydrate compounds. The regenerated ionic liquid is recycled through pipes 8 and 9 to zone ZA. The antihydrates are evacuated through pipe 7a.
摘要翻译： 该方法能够提取通过管1到达的缩合烃液体原料中含有的防水化合物。 液体原料在区域ZA中与具有通式Q + A31的非水离子液体接触，其中Q +表示铵，鏻和/或锍阳离子，A31表示能够形成液体的阴离子 盐。 消除了通过管2排出的液体烃原料中的防水化合物。 装有防水化合物的离子液体通过管3抽真空，然后引入蒸发器DE中进行加热以蒸发掉防水剂。 再生的离子液体通过管道8和9再循环到区域ZA。 通过管7a抽出抗水合物。
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24.发明授权Method of decarbonating a combustion fume with extraction of the solvent contained in the purified fume 失效通过提取净化烟气中所含的溶剂来对燃烧烟进行脱碳的方法公开(公告)号：US07459134B2
公开(公告)日：2008-12-02
申请号：US11336888
申请日：2006-01-23
CPC分类号： B01D53/1493
摘要： The combustion fume flowing in through line 1 is decarbonated by contacting with a solvent in column C2. The solvent laden with carbon dioxide is regenerated in zone R. The purified fume discharged through line 9 comprises part of the solvent. The method allows to extract the solvent contained in the purified fume. The purified fume is contacted in zone ZA with a non-aqueous ionic liquid of general formula Q+ A−; Q+ designates an ammonium, phosphonium and/or sulfonium cation, and A− an anion likely to form a liquid salt. The solvent-depleted purified fume is discharged through line 17. The solvent-laden ionic liquid is regenerated by heating in evaporation device DE. The solvent separated from the ionic liquid in device DE is recycled.
摘要翻译： 通过管线1流入的燃烧烟气通过与C2中的溶剂接触而脱碳。 含有二氧化碳的溶剂在区域R中再生。通过管线9排出的净化烟气包含部分溶剂。 该方法允许提取纯化烟雾中所含的溶剂。 纯化的烟气在ZA区域与通式为Q + A-的非水离子液体接触; Q +表示铵，鏻和/或锍阳离子，A-是可能形成液体盐的阴离子。 通过管线17排出溶剂贫化的净化烟雾。通过在蒸发装置DE中加热来再生含溶剂的离子液体。 从设备DE中的离子液体分离的溶剂被再循环。
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25.发明申请Method for eliminating the carbonyl sulfide contained in a liquid hydrocarbon stream 有权消除液态烃流中所含羰基硫化物的方法公开(公告)号：US20070039854A1
公开(公告)日：2007-02-22
申请号：US11483742
申请日：2006-07-11
申请人： Arnaud Baudot , Renaud Cadours , Raphael Huyghe , Elsa Jolimaitre , Pascal Mougin , Eszter Toth
发明人： Arnaud Baudot , Renaud Cadours , Raphael Huyghe , Elsa Jolimaitre , Pascal Mougin , Eszter Toth
摘要： The liquid hydrocarbon stream including COS is introduced via line 1 into membrane contactor CM to be placed in contact, through membrane M, with the aqueous alkanolamine solution arriving via line 3. The COS contained in the hydrocarbon stream is absorbed by the aqueous alkanolamine solution. The liquid hydrocarbons from which the COS has been removed are evacuated from CM via line 2. The aqueous solution containing COS is sent via line 4 to zone R to be regenerated. The compounds released during regeneration, particularly COS and COS-derived products, are evacuated from zone R via line 5. The regenerated aqueous alkanolamine solution is recycled via line 3 into membrane contactor CM.
摘要翻译： 包括COS的液态烃流通过管线1引入膜接触器CM中，通过膜M与烷基胺胺水溶液经由管线3到达接触。 包含在烃流中的COS被链烷醇胺水溶液吸收。 已经从其中除去COS的液体烃通过管线2从CM排出。 含有COS的水溶液通过管线4送至区R以再生。 在再生期间释放的化合物，特别是COS和COS衍生产物，经由管线5从区域R排出。 再生的链烷醇胺水溶液通过管线3再循环到膜接触器CM中。
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公开(公告)号：US07811538B2
公开(公告)日：2010-10-12
申请号：US12057407
申请日：2008-03-28
申请人： Renaud Cadours , Eric Lemaire , Julia Magne-Drisch
发明人： Renaud Cadours , Eric Lemaire , Julia Magne-Drisch
IPC分类号： B01D53/48
CPC分类号： C10L3/10 , B01D53/86 , B01D53/8606 , B01D2257/306 , C10L3/102
摘要： The method allows to remove mercaptans contained in a gaseous feed comprising hydrocarbons by carrying out the following stages: a) contacting, in a reactor R1, gaseous feed 1 with a liquid stream 13 comprising olefins, in the presence of a first acid catalyst so that the mercaptans react with the olefins so as to form sulfides, b) discharging an effluent 3 from reactor R1 and separating the effluent into a gas phase and a liquid phase so as to obtain a mercaptan-depleted treated gas 4 and a sulfide-laden liquid, c) separating the sulfide-laden liquid into a first fraction 6 and a second fraction 5, the volume flow rate of first fraction 6 being at least three times higher than the volume flow rate of second fraction 5, d) recycling first fraction 6 to stage a) as a first portion of said liquid stream to be fed into said reactor R1, e) regenerating second fraction 5 by cracking so as to obtain a sulfide-depleted second fraction 2 that is recycled to stage a) as a second portion of said liquid stream.
摘要翻译： 该方法允许通过进行以下步骤来除去包含在包含烃的气态进料中的硫醇：a）在反应器R1中将气态进料1与包含烯烃的液体流13在第一酸催化剂存在下接触使得 硫醇与烯烃反应以形成硫化物，b）从反应器R1排出流出物3，并将流出物分离成气相和液相，以获得硫醇贫化处理气体4和含硫化物的液体 ，c）将含硫化物的液体分离成第一馏分6和第二馏分5，第一馏分6的体积流量比第二馏分5的体积流速高至少三倍，d）回收第一馏分6 将a）作为待进料到所述反应器R1中的所述液体物流的第一部分，e）通过裂化再生第二馏分5，以获得被再循环至a）段的硫化物贫乏的第二馏分2作为第二部分 的说 液体流。
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27.发明授权Acetonitrile removal from the olefinic feed of ether production processes using ionic liquids 失效使用离子液体从醚生产过程的烯烃进料中除去乙腈公开(公告)号：US07759528B2
公开(公告)日：2010-07-20
申请号：US11954108
申请日：2007-12-11
CPC分类号： C07B63/00 , B01D11/0426 , B01D11/0488 , B01D11/0492 , B01J2219/00006 , C07C41/06 , Y02P20/542 , C07C43/046
摘要： An enhanced ether production process from an olefinic cut containing at least one iso-olefin and from an alcohol comprises a stage of removal of the acetonitrile present in the hydrocarbon feed by liquid-liquid extraction, the extraction solvent being a non-aqueous ionic liquid of general formula Q+A−, wherein Q+ is an ammonium, phosphonium and/or sulfonium cation, and A− an anion likely to form a liquid salt with said cation. Advantageously, the method according to the invention generally allows the amount of water at the etherification reactor inlet to be divided by at least two and thus the purity of the ether produced to be improved.
摘要翻译： 含有至少一种异烯烃和醇的烯烃切割剂的增强的乙醚生产方法包括通过液 - 液萃取除去存在于烃进料中的乙腈的一个阶段，萃取溶剂是一种非水离子液体 通式Q + A-，其中Q +是铵，鏻和/或锍阳离子，A-是可能与所述阳离子形成液体盐的阴离子。 有利地，根据本发明的方法通常允许将醚化反应器入口处的水量除以至少两个，从而提高生产的醚的纯度。
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28.发明授权公开(公告)号：US07635424B2
公开(公告)日：2009-12-22
申请号：US11625935
申请日：2007-01-23
申请人： Patrick Briot , Renaud Cadours , Sophie Drozdz , Fabrice Lecomte
发明人： Patrick Briot , Renaud Cadours , Sophie Drozdz , Fabrice Lecomte
IPC分类号： C10G45/04
CPC分类号： B01D53/8603 , B01D53/04 , B01D2253/108 , B01D2257/306 , B01D2258/06 , B01D2259/40086 , C10L3/10 , C10L3/102
摘要： The mercaptan-laden natural gas is contacted with a mercaptan-adsorbing sieve T1. The mercaptan-rich gaseous effluent obtained upon regeneration of sieve T2 is then contacted with an olefin-containing liquid feed in the presence of an acid catalyst. Under suitable conditions, the mercaptans are absorbed in the liquid feed and they react with the olefins so as to form solvent-soluble sulfides. A solvent regeneration stage allows the capture agent to be recycled.
摘要翻译： 载有硫醇的天然气与硫醇吸附筛T1接触。 然后，在酸性催化剂存在下，将通过再生筛子T2获得的富含硫醇的气态流体与含烯烃的液体进料接触。 在合适的条件下，硫醇被吸收在液体进料中，它们与烯烃反应，形成溶剂可溶的硫化物。 溶剂再生阶段允许捕获剂再循环。
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29.发明授权Method for processing a natural gas with extraction of the solvent contained in the acid gases 失效通过萃取酸性气体中所含的溶剂来处理天然气的方法公开(公告)号：US07459011B2
公开(公告)日：2008-12-02
申请号：US11057011
申请日：2005-02-14
IPC分类号： B01D53/14
CPC分类号： C10L3/10
摘要： The natural gas arriving through pipe 1 is deacidified by being brought into contact with a solvent in zone C. The solvent charged with acid compounds is regenerated in zone R. The acid gases, released into pipe 5 upon regeneration, include a quantity of solvent. The method enables the solvent contained in the acid gases to be extracted. In zone ZA, the acid gases are brought into contact with a non-aqueous ionic liquid whose general formula is Q+ A−, where Q+ designates an ammonium, phosphonium, and/or sulfonium cation, and A− designates an anion able to form a liquid salt. The solvent is removed from the acid gases evacuated through pipe 6. The ionic liquid charged with solvent is regenerated by heating in an evaporator DE. The ionic liquid regenerated is recycled through pipes 8 and 9 to zone ZA. The solvent is evacuated through pipe 13.
摘要翻译： 通过管道1到达的天然气通过与区域C中的溶剂接触而脱酸。在酸性化合物中加入的溶剂在区域R中再生。再生时释放到管道5中的酸性气体包括一定量的溶剂。 该方法能够提取酸性气体中所含的溶剂。 在区域ZA中，酸性气体与通式为Q + A-的非水性离子液体接触，其中Q +表示铵，鏻和/或锍阳离子，A-表示能形成 液体盐 从通过管道6排出的酸性气体中除去溶剂。加入溶剂的离子液体通过在蒸发器DE中加热而再生。 再生的离子液体通过管道8和9循环到区域ZA。 溶剂通过管13排出。
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公开(公告)号：US07192565B2
公开(公告)日：2007-03-20
申请号：US11194557
申请日：2005-08-02
申请人： Patrick Briot , Renaud Cadours , Sophie Drozdz , Fabrice Lecomte
发明人： Patrick Briot , Renaud Cadours , Sophie Drozdz , Fabrice Lecomte
CPC分类号： C10L3/10
摘要： The gaseous feed flowing in through line 1 is contacted in contacting zone ZA with a liquid solvent flowing in through line 2. The solvent comprises between 0.001% and 100% by weight of a liquid olefin. Contacting in zone ZA is carried out in the presence of an acid catalyst. The purified gaseous feed is discharged from zone ZA through line 3. The sulfide-laden solvent is discharged through line 4, then regenerated in unit RE. The regenerated solvent is recycled through lines 7 and 2 to zone ZA.
摘要翻译： 通过管线1流动的气态进料在接触区ZA中与通过管线2流动的液体溶剂接触。溶剂包含0.001至100重量％的液体烯烃。 ZA区在酸催化剂存在下进行接触。 纯化的气体进料通过管线3从区域ZA排出。含硫化物的溶剂通过管线4排出，然后在单元RE中再生。 再生的溶剂通过管线7和2再循环到区域ZA。
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