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公开(公告)号：US5200238A
公开(公告)日：1993-04-06
申请号：US766492
申请日：1991-09-25
IPC分类号： G02F1/1337 , G02F1/139
CPC分类号： G02F1/133711 , G02F1/1397 , G02F2001/133746 , Y10T428/1005 , Y10T428/1014 , Y10T428/31663
摘要： A method of forming liquid crystal alignment layers of high tilt angle, said method comprising preparing a polymeric film of a monomer of the formula IV: ##STR1## wherein X and Y are strong electron withdrawing groups, optionally substituted with or containing Si or Ti, and A is --H or --CH.dbd.CH.sub.2 or, provided that X and Y are both --CN, A may be --R.sup.2 or --CH.dbd.CHR.sup.2 wherein R.sup.2 is hydrocarbyl, aryl or alkaryl; exposing said polymeric film to ultraviolet radiation for sufficient period of time to photochemically modify the polymer and, thereafter, subjecting the modified polymer to a heat treatment in the range of 100.degree.-400.degree. C. for at least 5 seconds.
摘要翻译： 一种形成高倾斜角的液晶取向层的方法，所述方法包括制备式IV单体的聚合物膜：其中X和Y是强吸电子基团，任选被Si或Ti取代 并且A是-H或-CH = CH 2，或者X和Y都是-CN，A可以是-R2或-CH = CHR2，其中R2是烃基，芳基或烷芳基; 将所述聚合物膜暴露于紫外线辐射足够的时间以光聚合改性聚合物，然后将改性聚合物在100-400℃范围内进行热处理至少5秒。
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22.发明授权
公开(公告)号：US5386047A
公开(公告)日：1995-01-31
申请号：US209785
申请日：1994-03-11
申请人： Steven T. Nakos , John G. Woods
发明人： Steven T. Nakos , John G. Woods
IPC分类号： C07F7/08 , C08F136/20 , C09J4/00 , C07F7/10 , C08F30/08
CPC分类号： C08F136/20 , C07F7/0854 , C09J4/00
摘要： Anionically polymerizable di-.alpha.-cyanopentadienoate disiloxane compounds of the formula:[CH.sub.2 .dbd.CH--CH.dbd.C(CN)--C(.dbd.O)--O--CH.sub.2 --R--Si(R").sub.2 ].sub.2 --Owhere R is --CH.dbd.CH-- or --C(.dbd.CH.sub.2)-- and the R" groups are the same or different hydrocarbon or halo substituted hydrocarbon groups are prepared by hydrolysis of a cyanoacetoxypropenylsilane having a hydrolyzable group attached to the silicon atom and then condensing the resulting disiloxane compound with acrolein. The di-.alpha.-cyanopentadienoate disiloxane compounds are useful as instant adhesives and as co-monomers in cyanoacrylate or cyanopentadienoate instant adhesives, providing the adhesive polymers or copolymers with improved thermal resistance.
摘要翻译： 具有下式的阴离子可聚合二 - 氰基戊二酸二硅氧烷化合物：[CH 2 = CH-CH = C（CN）-C（= O）-O-CH 2 -R-Si（R“）2] 是-CH = CH-或-C（= CH 2） - ，并且R“基团是相同或不同的烃基或卤素取代的烃基，其通过水解具有连接到硅原子的可水解基团的氰基乙酰氧基丙烯基硅烷然后冷凝 所得的二甲氧基化合物与丙烯醛。 二 - 氰基戊二酸二异氰酸酯二硅氧烷化合物可用作速溶胶粘剂，也可用作氰基丙烯酸酯或氰基戊二酸酯速溶胶粘剂中的共聚单体，为粘合剂聚合物或共聚物提供改善的耐热性。
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公开(公告)号：US20100105795A1
公开(公告)日：2010-04-29
申请号：US11814536
申请日：2005-11-11
申请人： Eerik Maandi , Edwin Perez , John G. Woods , Joel D. Schall , Seamus Grant
发明人： Eerik Maandi , Edwin Perez , John G. Woods , Joel D. Schall , Seamus Grant
CPC分类号： C08F222/1006
摘要： The present invention relates to liquid stable thiol-acrylate and thiol-vinyl ether compositions. More particularly, in accordance with some embodiments, the compositions may include a (meth)acrylate, a thiol component, an organic acid stabilizer, and a curing initiator. In other embodiments, the compositions may include a curable component selected from a (meth)acrylate, vinyl ether and/or alkenyl ether, a reactive diluent having vinyl ether and acrylate functionality, a thiol component and a stabilizer selected from an organic acid, a hemiacetal ester derivative of an organic acid and/or a phenol acetal.
摘要翻译： 本发明涉及液体稳定的硫醇 - 丙烯酸酯和硫醇 - 乙烯基醚组合物。 更具体地，根据一些实施方案，组合物可以包括（甲基）丙烯酸酯，硫醇组分，有机酸稳定剂和固化引发剂。 在其它实施方案中，组合物可以包括选自（甲基）丙烯酸酯，乙烯基醚和/或烯基醚的可固化组分，具有乙烯基醚和丙烯酸酯官能团的反应性稀释剂，硫醇组分和选自有机酸， 有机酸的半缩醛酯衍生物和/或酚缩醛。
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24.发明授权Thiol-ene cured oil-resistant polyacrylate sealants for in-place gasketing applications 有权硫辛烯固化耐油聚丙烯酸酯密封胶，适用于就地垫片应用公开(公告)号：US09243083B2
公开(公告)日：2016-01-26
申请号：US12062090
申请日：2008-04-03
CPC分类号： C08F8/02 , C08F8/14 , C08F8/32 , C08F8/34 , C08K5/0025 , C08K5/372 , C09J133/14 , G02F2202/023 , G02F2202/28 , C08F220/28 , C08F220/18 , C08F20/18
摘要： The present invention relates to thiol-ene curing compositions, which cure upon exposure to ultraviolet (UV) light and/or heat. The compositions include components having alkenyl (or “ene”) functionality and components having thiol functionality, which undergo thiol-ene curing. The compositions also include a cure system. More specifically, in some embodiments, the curable compositions include a vinyl polymer bearing alkenyl or thiol terminal functional group(s) and a cross-linking agent having the opposing functionality, i.e., thiol cross-linking agents with alkenyl-terminated vinyl polymers and vinyl cross-linking agents with thiol-terminated vinyl polymers. Also provided are methods of making and using the compositions, such as for sealants for in-place gasketing applications.
摘要翻译： 本发明涉及硫醇烯固化组合物，其在暴露于紫外线（UV）光和/或热时固化。 组合物包括具有烯基（或“烯”）官能团的组分和具有硫醇官能团的组分，其经历硫醇烯固化。 组合物还包括固化体系。 更具体地，在一些实施方案中，可固化组合物包括带有烯基或硫醇末端官能团的乙烯基聚合物和具有相反官能团的交联剂，即具有链烯基封端的乙烯基聚合物和乙烯基的硫醇交联剂 交联剂与硫醇封端的乙烯基聚合物。 还提供了制备和使用组合物的方法，例如用于就地垫片应用的密封剂。
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公开(公告)号：US20100212824A1
公开(公告)日：2010-08-26
申请号：US11993110
申请日：2006-06-19
CPC分类号： B29C48/15 , B29C35/08 , B32B7/12 , B32B27/308 , C08F120/18 , C08L2312/06 , C09D133/08 , Y10T428/31935
摘要： The present invention relates to photocurable elastomer compositions and methods of preparation and use of such compositions for cure-in-place applications such as gaskets. The curable compositions generally include an elastomer component, a monofunctional and/or multifunctional reactant and a photoinitiator that in various aspects may be a visible and/or UV curing initiator. The various components may be present in different amounts, depending on the combination of components and composition desired.
摘要翻译： 本发明涉及光固化弹性体组合物以及这种组合物的制备和使用方法，用于就地固化应用如垫片。 可固化组合物通常包括弹性体组分，单官能和/或多官能反应物和光引发剂，其在各个方面可以是可见和/或UV固化引发剂。 各种组分可以以不同的量存在，这取决于组分和组合物的组合。
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26.发明申请THIOL-ENE CURED OIL-RESISTANT POLYACRYLATE SEALANTS FOR IN-PLACE GASKETING APPLICATIONS 有权THIOL-ENE固化耐油聚丙烯酸酯密封剂，用于内部气体应用公开(公告)号：US20140216649A1
公开(公告)日：2014-08-07
申请号：US12062090
申请日：2008-04-03
CPC分类号： C08F8/02 , C08F8/14 , C08F8/32 , C08F8/34 , C08K5/0025 , C08K5/372 , C09J133/14 , G02F2202/023 , G02F2202/28 , C08F220/28 , C08F220/18 , C08F20/18
摘要： The present invention relates to thiol-ene curing compositions, which cure upon exposure to ultraviolet (UV) light and/or heat. The compositions include components having alkenyl (or “ene”) functionality and components having thiol functionality, which undergo thiol-ene curing. The compositions also include a cure system. More specifically, in some embodiments, the curable compositions include a vinyl polymer bearing alkenyl or thiol terminal functional group(s) and a cross-linking agent having the opposing functionality, i.e., thiol cross-linking agents with alkenyl-terminated vinyl polymers and vinyl cross-linking agents with thiol-terminated vinyl polymers. Also provided are methods of making and using the compositions, such as for sealants for in-place gasketing applications.
摘要翻译： 本发明涉及硫醇烯固化组合物，其在暴露于紫外线（UV）光和/或热时固化。 组合物包括具有烯基（或“烯”）官能团的组分和具有硫醇官能团的组分，其经历硫醇烯固化。 组合物还包括固化体系。 更具体地，在一些实施方案中，可固化组合物包括带有烯基或硫醇末端官能团的乙烯基聚合物和具有相反官能团的交联剂，即具有链烯基封端的乙烯基聚合物和乙烯基的硫醇交联剂 交联剂与硫醇封端的乙烯基聚合物。 还提供了制备和使用组合物的方法，例如用于就地垫片应用的密封剂。
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27.发明授权Adhesive of substituted oxirane or oxetane compound with silver-based, lead-free solder 有权取代环氧乙烷或氧杂环丁烷化合物与银基，无铅焊料的粘合剂公开(公告)号：US07671114B2
公开(公告)日：2010-03-02
申请号：US12176729
申请日：2008-07-21
CPC分类号： H01L21/563 , C08G59/1455 , C08G59/1494 , C08K5/5435 , C09J163/00 , H01L23/293 , H01L2224/73203 , H01L2924/01004 , H01L2924/01077 , H01L2924/01079
摘要： In accordance with the present invention, it has now been found that glycidyl epoxy resins containing substitution on the epoxide ring can be used with conventional epoxy curing agents and fluxing agents to produce underfill adhesives that are suitable for use with silver-based alloys. Owing to the structural similarity of the new materials to conventional epoxy resins, physical and material properties of the invention formulations are altered little, if at all, relative to products currently in use, and so are highly compatible with existing processes.
摘要翻译： 根据本发明，已经发现在环氧化物环上含有取代基的缩水甘油基环氧树脂可以与常规的环氧固化剂和助熔剂一起使用，以生产适用于银基合金的底部填充粘合剂。 由于新材料与常规环氧树脂的结构相似性，本发明制剂的物理和材料性能相对于目前使用的产品而言几乎没有改变，因此与现有方法高度兼容。
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公开(公告)号：US20090018239A1
公开(公告)日：2009-01-15
申请号：US12176729
申请日：2008-07-21
IPC分类号： C08K5/00
CPC分类号： H01L21/563 , C08G59/1455 , C08G59/1494 , C08K5/5435 , C09J163/00 , H01L23/293 , H01L2224/73203 , H01L2924/01004 , H01L2924/01077 , H01L2924/01079
摘要： In accordance with the present invention, it has now been found that glycidyl epoxy resins containing substitution on the epoxide ring can be used with conventional epoxy curing agents and fluxing agents to produce underfill adhesives that are suitable for use with silver-based alloys. Owing to the structural similarity of the new materials to conventional epoxy resins, physical and material properties of the invention formulations are altered little, if at all, relative to products currently in use, and so are highly compatible with existing processes.
摘要翻译： 根据本发明，已经发现在环氧化物环上含有取代基的缩水甘油基环氧树脂可以与常规的环氧固化剂和助熔剂一起使用，以生产适用于银基合金的底部填充粘合剂。 由于新材料与常规环氧树脂的结构相似性，本发明制剂的物理和材料性能相对于目前使用的产品而言几乎没有改变，因此与现有方法高度兼容。
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公开(公告)号：US07193016B1
公开(公告)日：2007-03-20
申请号：US10692935
申请日：2003-10-27
申请人： John G. Woods , Mark M. Konarski , Kyra M. Kozak , Yuhshi Luh
发明人： John G. Woods , Mark M. Konarski , Kyra M. Kozak , Yuhshi Luh
CPC分类号： C09J163/00 , C08F8/14 , C08F2810/40 , C08F20/16
摘要： In accordance with the present invention, there are provided toughening agents which are useful for improving the performance properties of epoxy-based adhesive formulations. For example, epoxidized polybutylacrylates have been found to be useful toughening agents of component level underfill adhesive compositions. Invention materials are generally liquid rubbers which provided improved fracture toughness while maintaining satisfactory capillary flow properties. Invention materials can be synthesized in neat (solventless) reactions from readily available low-cost raw materials and isolated in high yields. They have a branched telechelic structure with terminal epoxide functional groups. The polyacrylate is typically obtained as a mixture of epoxidized polymer, chain extended polyoligomer and unreacted monomer. Invention materials are compatible with common epoxy formulations and may be used without purification. At low levels of incorporation, they provide adhesives that meet the minimum fracture toughness (Gq>2.0 lb/in) and capillary flow specifications (flow time
摘要翻译： 根据本发明，提供了可用于改善环氧基粘合剂制剂的性能的增韧剂。 例如，已经发现环氧化的聚丁基丙烯酸酯是组分级底部填充粘合剂组合物的有用的增韧剂。 发明材料通常是液体橡胶，其提供改善的断裂韧性同时保持令人满意的毛细管流动性能 本发明材料可以从易于获得的低成本原料的纯（无溶剂）反应中合成并以高收率分离。 它们具有末端环氧官能团的分子遥爪结构。 聚丙烯酸酯通常以环氧化聚合物，链延长多元寡聚物和未反应单体的混合物形式获得。 本发明材料与普通的环氧配方相容，可以不经纯化地使用。 在低掺量下，它们提供了许多商业底层填充应用的粘合剂，其满足最小断裂韧性（Gq> 2.0lb / in）和毛细管流动规格（流动时间<180秒）。 根据本发明的另一个实施方案，提供了包含本发明化合物的粘合剂组合物及其使用方法。 在本发明的另外的实施方案中，提供了制备本发明增韧剂的方法，用于将装置粘附到基底上的方法以及包括附着到第二制品上的第一制品的组件。
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公开(公告)号：US06740193B2
公开(公告)日：2004-05-25
申请号：US10032128
申请日：2001-12-21
申请人： John G. Woods , Jianzhao Wang , Jean M. J. Fréchet
发明人： John G. Woods , Jianzhao Wang , Jean M. J. Fréchet
IPC分类号： C09J16300
CPC分类号： C07D303/12 , Y10T156/1111 , Y10T428/31511
摘要： In accordance with the present invention, there are provided gem-diesters and epoxidized derivatives thereof. When cured, thermosets comprising invention gem-diesters and epoxidized derivatives thereof have thermally and/or chemically labile gem-diester groups interspersed throughout the crosslinked network. Thus, thermosets based on invention gem-diesters and epoxidized derivatives thereof can be easily reworked thermally or chemically by treatment with dilute acidic or basic solutions. Further provided by the present invention are adhesive compositions comprising invention gem-diesters and epoxidized derivatives thereof.
摘要翻译： 根据本发明，提供了偕二酯及其环氧化衍生物。 当固化时，包含本发明偕二酯和环氧化衍生物的热固性材料具有散布在整个交联网络中的热和/或化学不稳定的偕二酯基团。 因此，基于本发明的偕二酯和其环氧化衍生物的热固性材料可以通过用稀酸或碱性溶液处理而易于热或化学地再加工。 本发明进一步提供的是含有本发明的偕二酯及其环氧化衍生物的粘合剂组合物。
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