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21.发明申请公开(公告)号：US20160167013A1
公开(公告)日：2016-06-16
申请号：US14945516
申请日：2015-11-19
申请人： Jean W. Beeckman , Ivy D. Johnson , Natalie A. Fassbender , Tilman W. Beutel , Nadya A. Hrycenko , Randolph J. Smiley , Peter I. Ravikovitch
发明人： Jean W. Beeckman , Ivy D. Johnson , Natalie A. Fassbender , Tilman W. Beutel , Nadya A. Hrycenko , Randolph J. Smiley , Peter I. Ravikovitch
CPC分类号： B01J20/18 , B01D53/02 , B01D2253/116 , B01D2256/245 , B01D2257/102 , B01D2257/304 , B01D2257/40 , B01D2257/504 , C01B39/026 , C01B39/48 , Y02C10/08 , Y02P20/152
摘要： A composition is described comprising a molecular sieve having pores defined by channels formed by one or more 8-membered rings of tetrahedrally coordinated atoms, such as a DDR-type molecular sieve, and an amorphous deposit of a boron compound on the molecular sieve.
摘要翻译： 描述了一种组合物，其包含具有由一个或多个四面体配位原子的8元环（例如DDR型分子筛）和硼化合物在分子筛上的无定形沉积物形成的通道限定的孔的分子筛。
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22.发明申请SYNTHESIS OF ZSM-58 CRYSTALS WITH IMPROVED DIFFUSIVITY FOR USE IN GAS SEPARATIONS 有权ZSM-58晶体的合成与气体分离中使用的改善差异公开(公告)号：US20150182947A1
公开(公告)日：2015-07-02
申请号：US14573177
申请日：2014-12-17
申请人： Ivy D. Johnson , Tilman W. Beutel , Peter I. Ravikovitch , Harry W. Deckman , Jack W. Johnson , Jean W. Beeckman , Natalie A. Fassbender , Nadya A. Hrycenko , Randy J. Smiley
发明人： Ivy D. Johnson , Tilman W. Beutel , Peter I. Ravikovitch , Harry W. Deckman , Jack W. Johnson , Jean W. Beeckman , Natalie A. Fassbender , Nadya A. Hrycenko , Randy J. Smiley
IPC分类号： B01J20/30 , B01J20/18 , B01J20/282 , C01B39/04
CPC分类号： B01J20/3078 , B01D53/02 , B01D2253/108 , B01D2256/245 , B01D2257/304 , B01D2257/504 , B01J20/18 , B01J20/186 , B01J20/282 , B01J20/30 , B01J20/3085 , B01J29/035 , B01J29/70 , B01J2220/80 , B01J2229/36 , B01J2229/40 , C01B37/02 , C01B39/026 , C01B39/04 , C01B39/48 , Y02C10/08 , Y02P20/152
摘要： Methods are provided for synthesizing ZSM-58 crystals with an improved morphology and/or an improved size distribution. By controlling the conditions during synthesis of the ZSM-58 crystals, crystals of a useful size with a narrow size distribution can be generated. Additionally, by controlling the ratio of water content to silica content in the synthesis mixture, it has unexpectedly been found that ZSM-58 crystals can be formed with an improved morphology. The improved morphology can result in ZSM-58 crystals with a more uniform size across the various dimensions of the crystal, which allows for more uniform diffusion within the crystal. This is in contrast to conventionally synthesized crystals, where the size of the crystal can vary along different axes of the crystals.
摘要翻译： 提供了用于合成具有改进的形态和/或改进的尺寸分布的ZSM-58晶体的方法。 通过控制合成ZSM-58晶体的条件，可以产生具有窄尺寸分布的有用尺寸的晶体。 另外，通过控制合成混合物中水含量与二氧化硅含量的比例，意外地发现可以形成具有改进的形态的ZSM-58晶体。 改进的形态可以导致在晶体的各种尺寸上具有更均匀尺寸的ZSM-58晶体，这允许在晶体内更均匀的扩散。 这与常规合成的晶体形成对比，其中晶体的尺寸可以沿晶体的不同轴线变化。
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23.发明授权Catalyst composition, the method of manufacturing and the process of use thereof in aromatics alkylation 有权催化剂组合物，其制备方法及其在芳烃烷基化中的应用方法公开(公告)号：US07919421B2
公开(公告)日：2011-04-05
申请号：US11643530
申请日：2006-12-21
IPC分类号： B01J29/06
CPC分类号： B01J29/7038 , B01J29/70 , B01J29/7007 , B01J29/80 , B01J35/10 , B01J37/0009 , B01J2229/42 , C07C2/66 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/65 , C07C2529/70 , C07C2529/80 , Y02P20/52 , C07C15/085
摘要： A catalyst composition comprises a crystalline MCM-22 family molecular sieve and a binder, wherein the catalyst composition is characterized by an extra-molecular sieve porosity greater than or equal to 0.122 ml/g for pores having a pore diameter ranging from about 2 nm to about 8 nm, wherein the porosity is measured by N2 porosimetry. The catalyst composition may be used for the process of alkylation or transalkylation of an alkylatable aromatic compound with an alkylating agent. The molecular sieve may have a Constraint Index of less than 12, e.g., less than 2. Examples of molecular sieve useful for this disclosure are a MCM-22 family molecular sieve, zeolite Y, and zeolite Beta.
摘要翻译： 一种催化剂组合物包括结晶MCM-22族分子筛和粘合剂，其中该催化剂组合物的特征在于具有大于或等于0.122ml / g的分子量以上孔隙，孔隙范围为约2nm至 约8nm，其中通过N 2孔隙率法测量孔隙度。 催化剂组合物可用于烷基化芳族化合物与烷基化剂的烷基化或烷基转移过程。 分子筛可以具有小于12，例如小于2的约束指数。可用于本公开的分子筛的实例是MCM-22族分子筛，沸石Y和沸石β。
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24.发明申请Catalyst Composition, The Method of Manufacturing, and the Process of Use Thereof in Aromatics Alkylation 有权催化剂组合物，制备方法及其在芳烃烷基化中的应用过程公开(公告)号：US20110028772A1
公开(公告)日：2011-02-03
申请号：US12906393
申请日：2010-10-18
IPC分类号： C07C2/66
CPC分类号： B01J29/7038 , B01J29/70 , B01J29/7007 , B01J29/80 , B01J35/10 , B01J37/0009 , B01J2229/42 , C07C2/66 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/65 , C07C2529/70 , C07C2529/80 , Y02P20/52 , C07C15/085
摘要： A catalyst composition comprises a crystalline MCM-22 family molecular sieve and a binder, wherein the catalyst composition is characterized by an extra-molecular sieve porosity greater than or equal to 0.122 ml/g for pores having a pore diameter ranging from about 2 nm to about 8 nm, wherein the porosity is measured by N2 porosimetry. The catalyst composition may be used for the process of alkylation or transalkylation of an alkylatable aromatic compound with an alkylating agent. The molecular sieve may have a Constraint Index of less than 12, e.g., less than 2. Examples of molecular sieve useful for this disclosure are a MCM-22 family molecular sieve, zeolite Y, and zeolite Beta
摘要翻译： 一种催化剂组合物包括结晶MCM-22族分子筛和粘合剂，其中该催化剂组合物的特征在于具有大于或等于0.122ml / g的分子量以上孔隙，孔隙范围为约2nm至 约8nm，其中通过N 2孔隙率法测量孔隙度。 催化剂组合物可用于烷基化芳族化合物与烷基化剂的烷基化或烷基转移过程。 分子筛可以具有小于12，例如小于2的约束指数。可用于本公开的分子筛的实例是MCM-22族分子筛，沸石Y和沸石β
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25.发明授权Selectivation of molecular sieve catalysts and use therof in hydrocarbon conversion 有权选择分子筛催化剂，并在烃转化中使用公开(公告)号：US07326818B2
公开(公告)日：2008-02-05
申请号：US10641604
申请日：2003-08-15
申请人： Jean W. Beeckman , William G. Borghard , Arthur W. Chester , Robert A. Crane , Owen C. Feeley , John C. Fried , Dominick N. Mazzone , Glenn R. Sweeten
发明人： Jean W. Beeckman , William G. Borghard , Arthur W. Chester , Robert A. Crane , Owen C. Feeley , John C. Fried , Dominick N. Mazzone , Glenn R. Sweeten
IPC分类号： C07C5/00
CPC分类号： B01J29/40 , B01J2229/12 , B01J2229/18 , B01J2229/40 , B01J2229/42 , C07C6/123 , C07C2521/08 , C07C2529/40 , Y02P20/52 , Y10S585/906 , C07C15/08
摘要： In a process for preparing a selectivated catalyst composition useful in the disproportionation of toluene, a catalyst comprising an acidic molecular sieve is contacted with a boron compound at a temperature in excess of 500° C.; and the resultant catalyst is then contacted with a medium containing hydrogen ions to at least partially restore the acid activity of the molecular sieve.
摘要翻译： 在制备可用于甲苯歧化的选择性催化剂组合物的方法中，包含酸性分子筛的催化剂在硼氢化合物与超过500℃的温度下接触; 然后使得到的催化剂与含有氢离子的介质接触，至少部分地恢复分子筛的酸活性。
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公开(公告)号：US5585082A
公开(公告)日：1996-12-17
申请号：US410244
申请日：1995-03-24
摘要： An alumina sorbent capable of adsorbing NOx and SOx from waste gases and being regenerated by heating above 650.degree. C. is made by incorporating an alumina stabilizing agent into the sorbent. A preferred method is to add the stabilizer when the alumina is precipitated. The precipitated powder is formed subsequently into a slurry, milled and spray dried to form the stabilized spheroidal alumina particles having a particle size of less than 500 microns. These particles are impregnated with an alkali metal or alkaline earth metal to form the stabilized sorbent. Alumina stabilizers include one or more of silica, lanthana, other rare earths, titania, zirconia and alkaline earths.
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公开(公告)号：US5427995A
公开(公告)日：1995-06-27
申请号：US21709
申请日：1993-02-24
摘要： An alumina sorbent capable of adsorbing NOx and SOx from waste gases and being regenerated by heating above 650.degree. C. is made by incorporating an alumina stabilizing agent into the sorbent. A preferred method is to add the stabilizer when the alumina is precipitated. The precipitated powder is formed subsequently into a slurry, milled and spray dried to form the stabilized spheroidal alumina particles having a particle size of less than 500 microns. These particles are impregnated with an alkali metal or alkaline earth metal to form the stabilized sorbent. Alumina stabilizers include one or more of silica, lanthana, other rare earths, titania, zirconia and alkaline earths.
摘要翻译： 能够从废气中吸附NOx和SOx并通过加热高于650℃再生的氧化铝吸附剂是通过将氧化铝稳定剂掺入吸附剂而制成的。 优选的方法是在氧化铝沉淀时加入稳定剂。 沉淀的粉末随后形成浆料，研磨并喷雾干燥以形成粒度小于500微米的稳定的球形氧化铝颗粒。 这些颗粒用碱金属或碱土金属浸渍以形成稳定的吸附剂。 氧化铝稳定剂包括二氧化硅，氧化镧，其它稀土，二氧化钛，氧化锆和碱土金属中的一种或多种。
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公开(公告)号：US5413771A
公开(公告)日：1995-05-09
申请号：US955771
申请日：1992-11-06
IPC分类号： B01D53/60 , B01D53/00 , B01D53/02 , B01D53/74 , B01J20/08 , B01J20/30 , C01B21/00 , C01B17/00
CPC分类号： B01J20/08 , B01D53/02 , B01D2257/30
摘要： An alumina sorbent capable of adsorbing NOx and SOx from waste gases and being regenerated by heating above 600.degree. C. is made by incorporating an alumina stabilizing agent into the sorbent. A preferred method is to add the stabilizer when the alumina is precipitated. The precipitated powder is formed subsequently into a slurry, milled and dripped to form the stabilized spheroidal alumina particles. These particles are impregnated with an alkali metal or alkaline earth metal to form the stabilized sorbent. Alumina stabilizers include one or more of silica, lanthana, other rare earths, titania, zirconia and alkaline earths.
摘要翻译： 通过将氧化铝稳定剂并入吸附剂中，可以从废气中吸附NOx和SOx并通过加热高于600℃再生的氧化铝吸附剂。 优选的方法是在氧化铝沉淀时加入稳定剂。 沉淀的粉末随后形成浆料，研磨并滴下以形成稳定的球状氧化铝颗粒。 这些颗粒用碱金属或碱土金属浸渍以形成稳定的吸附剂。 氧化铝稳定剂包括二氧化硅，氧化镧，其它稀土，二氧化钛，氧化锆和碱土金属中的一种或多种。
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公开(公告)号：US10307751B2
公开(公告)日：2019-06-04
申请号：US15013035
申请日：2016-02-02
申请人： Jean W. Beeckman , Natalie A. Fassbender , Theodore E. Datz , Chuansheng Bai , Adrienne J. Thornburg , Tilman W. Beutel
发明人： Jean W. Beeckman , Natalie A. Fassbender , Theodore E. Datz , Chuansheng Bai , Adrienne J. Thornburg , Tilman W. Beutel
摘要： Disclosed herein are an apparatus and a method for mixing and/or mulling a sample, the apparatus comprising at least one container made of a flexible material and containing a sample, means for holding the container, and means for impacting the container, wherein the means for holding and the means for impacting are movable relative to each other, and wherein the means for holding, the means for impacting, and the container are arranged such that the means for impacting and the container can repeatedly collide, whereby an energy of collision can be imparted to the sample, thereby mixing and/or mulling the sample. Also disclosed is an assembly for performing high throughput experiments including the apparatus for mixing and/or mulling a sample and an extruder configured to receive a sample weighing less than 100 grams.
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公开(公告)号：US09597655B2
公开(公告)日：2017-03-21
申请号：US14945516
申请日：2015-11-19
申请人： Jean W. Beeckman , Ivy D. Johnson , Natalie A. Fassbender , Tilman W. Beutel , Nadya A. Hrycenko , Randolph J. Smiley , Peter I. Ravikovitch
发明人： Jean W. Beeckman , Ivy D. Johnson , Natalie A. Fassbender , Tilman W. Beutel , Nadya A. Hrycenko , Randolph J. Smiley , Peter I. Ravikovitch
CPC分类号： B01J20/18 , B01D53/02 , B01D2253/116 , B01D2256/245 , B01D2257/102 , B01D2257/304 , B01D2257/40 , B01D2257/504 , C01B39/026 , C01B39/48 , Y02C10/08 , Y02P20/152
摘要： A composition is described comprising a molecular sieve having pores defined by channels formed by one or more 8-membered rings of tetrahedrally coordinated atoms, such as a DDR-type molecular sieve, and an amorphous deposit of a boron compound on the molecular sieve.
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