公开(公告)号：US20180141033A1

公开(公告)日：2018-05-24

申请号：US15013035

申请日：2016-02-02

申请人： Jean W. Beeckman ,  Natalie A. Fassbender ,  Theodore E. Datz ,  Chuansheng Bai ,  Adrienne J. Thornburg ,  Tilman W. Beutel

发明人： Jean W. Beeckman ,  Natalie A. Fassbender ,  Theodore E. Datz ,  Chuansheng Bai ,  Adrienne J. Thornburg ,  Tilman W. Beutel

IPC分类号： B01J37/04 ,  B01J37/00 ,  B01J35/02 ,  B01J21/04 ,  B01J35/10

CPC分类号： B01J37/04 ,  B01J21/04 ,  B01J35/023 ,  B01J35/1004 ,  B01J35/1033 ,  B01J37/0009 ,  B01J37/0036 ,  B01J37/0063 ,  B01J2229/42 ,  C01B33/2807 ,  C07C2521/04

摘要： Disclosed herein are an apparatus and a method for mixing and/or mulling a sample, the apparatus comprising at least one container made of a flexible material and containing a sample, means for holding the container, and means for impacting the container, wherein the means for holding and the means for impacting are movable relative to each other, and wherein the means for holding, the means for impacting, and the container are arranged such that the means for impacting and the container can repeatedly collide, whereby an energy of collision can be imparted to the sample, thereby mixing and/or mulling the sample. Also disclosed is an assembly for performing high throughput experiments including the apparatus for mixing and/or mulling a sample and an extruder configured to receive a sample weighing less than 100 grams.

公开(公告)号：US10307751B2

公开(公告)日：2019-06-04

申请号：US15013035

申请日：2016-02-02

申请人： Jean W. Beeckman ,  Natalie A. Fassbender ,  Theodore E. Datz ,  Chuansheng Bai ,  Adrienne J. Thornburg ,  Tilman W. Beutel

发明人： Jean W. Beeckman ,  Natalie A. Fassbender ,  Theodore E. Datz ,  Chuansheng Bai ,  Adrienne J. Thornburg ,  Tilman W. Beutel

IPC分类号： B01J37/04 ,  B01J37/00 ,  B01J35/02 ,  B01J21/04 ,  B01J35/10 ,  C01B33/26

摘要： Disclosed herein are an apparatus and a method for mixing and/or mulling a sample, the apparatus comprising at least one container made of a flexible material and containing a sample, means for holding the container, and means for impacting the container, wherein the means for holding and the means for impacting are movable relative to each other, and wherein the means for holding, the means for impacting, and the container are arranged such that the means for impacting and the container can repeatedly collide, whereby an energy of collision can be imparted to the sample, thereby mixing and/or mulling the sample. Also disclosed is an assembly for performing high throughput experiments including the apparatus for mixing and/or mulling a sample and an extruder configured to receive a sample weighing less than 100 grams.

公开(公告)号：US20090216056A1

公开(公告)日：2009-08-27

申请号：US12070861

申请日：2008-02-21

申请人： Jean W. Beeckman ,  Theodore E. Datz ,  Glenn R. Sweeten ,  Jason Wu

发明人： Jean W. Beeckman ,  Theodore E. Datz ,  Glenn R. Sweeten ,  Jason Wu

IPC分类号： B29C47/00 ,  B01J21/00 ,  C07C2/00

CPC分类号： B01J37/0009 ,  B01J21/08 ,  B01J23/04 ,  B01J29/06 ,  B01J29/40 ,  B01J35/002 ,  B01J35/023 ,  B01J35/026 ,  B01J2229/42 ,  C04B35/14 ,  C04B35/16 ,  C04B35/6263 ,  C04B35/62695 ,  C04B2235/3201 ,  C04B2235/6021

摘要： In a method of forming a shaped body, a mixture is formed comprising a particulate silica-rich material, water and a potassium base or basic salt, wherein the total solids content of the mixture is from about 20 to about 90 weight percent. The mixture is extruded into extrudates and the extrudates are dried and heated to a temperature of from about 300° C. to about 800° C. to form the shaped body.

摘要翻译： 在形成成形体的方法中，形成包含颗粒二氧化硅的材料，水和钾碱或碱式盐的混合物，其中混合物的总固体含量为约20至约90重量％。 将混合物挤出成挤出物，并将挤出物干燥并加热至约300℃至约800℃的温度以形成成形体。

公开(公告)号：US08343335B2

公开(公告)日：2013-01-01

申请号：US12070861

申请日：2008-02-21

申请人： Jean W. Beeckman ,  Theodore E. Datz ,  Glenn R. Sweeten ,  Jason Wu

发明人： Jean W. Beeckman ,  Theodore E. Datz ,  Glenn R. Sweeten ,  Jason Wu

IPC分类号： C10G11/00

CPC分类号： B01J37/0009 ,  B01J21/08 ,  B01J23/04 ,  B01J29/06 ,  B01J29/40 ,  B01J35/002 ,  B01J35/023 ,  B01J35/026 ,  B01J2229/42 ,  C04B35/14 ,  C04B35/16 ,  C04B35/6263 ,  C04B35/62695 ,  C04B2235/3201 ,  C04B2235/6021

摘要： In a method of forming a shaped body, a mixture is formed comprising a particulate silica-rich material, water and a potassium base or basic salt, wherein the total solids content of the mixture is from about 20 to about 90 weight percent. The mixture is extruded into extrudates and the extrudates are dried and heated to a temperature of from about 300° C. to about 800° C. to form the shaped body.

公开(公告)号：US08207082B2

公开(公告)日：2012-06-26

申请号：US12087981

申请日：2007-01-12

申请人： Jason Wu ,  Theodore E. Datz ,  Ralph Dehaas ,  Jean W. Beeckman

发明人： Jason Wu ,  Theodore E. Datz ,  Ralph Dehaas ,  Jean W. Beeckman

IPC分类号： B01J21/08 ,  B01J31/06

CPC分类号： B01J37/0009 ,  B01J21/08 ,  B01J23/882 ,  B01J29/0308 ,  B01J35/1014 ,  B01J35/1019 ,  B01J35/1042 ,  B01J35/1047 ,  B01J35/1061 ,  B01J35/1066 ,  B01J37/0018 ,  B01J37/0203 ,  B01J37/10 ,  B01J37/20 ,  C10G49/08 ,  C10G2300/1044 ,  C10G2300/202 ,  C10G2400/02

摘要： This invention relates to a method for making shaped bodies having a silica content of at least 85 wt %, to shaped bodies made by such method, to catalyst compositions comprising shaped bodies made by such methods and to catalytic conversion processes using catalyst compositions comprising shaped bodies made by such methods. The method of making the shaped bodies comprises the steps of a) forming shaped bodies from a mixture obtained from at least one amorphous silica powder, at least one silica sol having a pH below 7, and at least one polymeric organic extrusion aid, optionally supplemental liquid medium and optionally crystallites of a zeolite or zeolite-type material; b) drying the shaped bodies obtained in step a); and c) heating the shaped bodies to a temperature ranging from about 500° C. to about 800° C.

摘要翻译： 本发明涉及一种制备具有至少85重量％的二氧化硅含量的成型体，通过这种方法制成的成形体，包括由这种方法制成的成型体的催化剂组合物，以及使用包含成形体的催化剂组合物的催化转化方法 通过这种方法制成。 制造成形体的方法包括以下步骤：a）从由至少一种无定形二氧化硅粉末，至少一种pH值低于7的硅溶胶和至少一种聚合有机挤出助剂获得的混合物形成成型体，任选地补充 液体介质和任选的沸石或沸石型材料的微晶; b）干燥步骤a）中获得的成形体; 和c）将成形体加热至约500℃至约800℃的温度。

公开(公告)号：US20100206775A1

公开(公告)日：2010-08-19

申请号：US12087981

申请日：2007-01-12

申请人： Jean W. Beeckman ,  Jason Wu ,  Theodore E. Datz ,  Ralph Dehaas

发明人： Jean W. Beeckman ,  Jason Wu ,  Theodore E. Datz ,  Ralph Dehaas

IPC分类号： C10G35/06 ,  B01J21/08 ,  B01J29/06 ,  B01J31/06 ,  B01J31/02 ,  B01J23/28 ,  B01J23/75

CPC分类号： B01J37/0009 ,  B01J21/08 ,  B01J23/882 ,  B01J29/0308 ,  B01J35/1014 ,  B01J35/1019 ,  B01J35/1042 ,  B01J35/1047 ,  B01J35/1061 ,  B01J35/1066 ,  B01J37/0018 ,  B01J37/0203 ,  B01J37/10 ,  B01J37/20 ,  C10G49/08 ,  C10G2300/1044 ,  C10G2300/202 ,  C10G2400/02

摘要： This invention relates to a method for making shaped bodies having a silica content of at least 85 wt %, to shaped bodies made by such method, to catalyst compositions comprising shaped bodies made by such methods and to catalytic conversion processes using catalyst compositions comprising shaped bodies made by such methods. The method of making the shaped bodies comprises the steps of a) forming shaped bodies from a mixture obtained from at least one amorphous silica powder, at least one silica sol having a pH below 7, and at least one polymeric organic extrusion aid, optionally supplemental liquid medium and optionally crystallites of a zeolite or zeolite-type material; b) drying the shaped bodies obtained in step a); and c) heating the shaped bodies to a temperature ranging from about 500° C. to about 800° C.

摘要翻译： 本发明涉及一种制备具有至少85重量％的二氧化硅含量的成型体，通过这种方法制成的成形体，包括由这种方法制成的成型体的催化剂组合物，以及使用包含成形体的催化剂组合物的催化转化方法 通过这种方法制成。 制造成形体的方法包括以下步骤：a）从由至少一种无定形二氧化硅粉末，至少一种pH低于7的二氧化硅溶胶和至少一种聚合有机挤出助剂获得的混合物形成成型体，任选地补充 液体介质和任选的沸石或沸石型材料的微晶; b）干燥步骤a）中获得的成形体; 和c）将成形体加热至约500℃至约800℃的温度。

公开(公告)号：US20110152062A1

公开(公告)日：2011-06-23

申请号：US12957817

申请日：2010-12-01

申请人： William A. Wachter ,  Brenda A. Raich ,  Theodore E. Datz ,  David O. Marler ,  Nicholas Rollman ,  Jeffrey T. Elks ,  Gordon F. Stuntz

发明人： William A. Wachter ,  Brenda A. Raich ,  Theodore E. Datz ,  David O. Marler ,  Nicholas Rollman ,  Jeffrey T. Elks ,  Gordon F. Stuntz

IPC分类号： B01J37/08 ,  B01J37/10 ,  B01J35/10 ,  B01J31/06 ,  B01J29/04

CPC分类号： B01J29/06 ,  B01J29/70 ,  B01J37/0018 ,  B01J37/0072 ,  B01J37/0236 ,  B01J37/08 ,  B01J2229/36 ,  B01J2229/42 ,  C10G11/05

摘要： Catalysts for experimentation are produced having a controlled matrix pore structure. The manufacturing process utilizes tape casting in the drying procedure in which a catalyst slurry is cast on a substrate and dried at a temperature of between about 50° C. to 200° C. for a period of time of about 0.1 to 1.0 hour. The dried catalyst particles can be removed from the substrate by several techniques, including scraping, burning, and deforming the substrate material, The resulting catalytic particles can be produced in an amount of about ca. 3 g to 300 g from slurries with volumes between 5 cc to 500 cc, which are suitable for small scale FCC reactors and for high throughput experimentation.

摘要翻译： 生产具有受控矩阵孔结构的用于实验的催化剂。 制造方法在干燥过程中使用带铸造，其中将催化剂浆料浇铸在基材上并在约50℃至200℃的温度下干燥约0.1至1.0小时的时间。 干燥的催化剂颗粒可以通过几种技术从基材中除去，包括刮擦，燃烧和使基材变形。所得到的催化剂颗粒可以以约约 3克至300克，体积在5毫升至500毫升之间的浆料，适用于小规模的FCC反应器和高通量实验。

公开(公告)号：US07867937B2

公开(公告)日：2011-01-11

申请号：US12001361

申请日：2007-12-11

申请人： William A. Wachter ,  Jeffrey T. Elks ,  Brenda A. Raich ,  Theodore E. Datz ,  Mary T. Van Nostrand ,  Gordon F. Stuntz ,  David O. Marler ,  Nicholas Rollman

发明人： William A. Wachter ,  Jeffrey T. Elks ,  Brenda A. Raich ,  Theodore E. Datz ,  Mary T. Van Nostrand ,  Gordon F. Stuntz ,  David O. Marler ,  Nicholas Rollman

IPC分类号： B01J35/02

CPC分类号： B01J29/06 ,  B01J29/70 ,  B01J37/0018 ,  B01J37/0072 ,  B01J37/0236 ,  B01J37/08 ,  B01J2229/36 ,  B01J2229/42 ,  C10G11/05

摘要： Catalysts for experimentation are produced having a controlled matrix pore structure. The manufacturing process utilizes tape casting in the drying procedure in which a catalyst slurry is cast on a substrate and dried at a temperature of between about 50° C. to 200° C. for a period of time of about 0.1 to 1.0 hour. The dried catalyst particles can be removed from the substrate by several techniques, including scraping, burning, and deforming the substrate material. The resulting catalytic particles can be produced in an amount of about ca. 3 g to 300 g from slurries with volumes between 5 cc to 500 cc, which are suitable for small scale FCC reactors and for high throughput experimentation.

摘要翻译： 生产具有受控矩阵孔结构的用于实验的催化剂。 制造方法在干燥过程中使用带铸造，其中将催化剂浆料浇铸在基材上并在约50℃至200℃的温度下干燥约0.1至1.0小时的时间。 干燥的催化剂颗粒可以通过几种技术从基材中除去，包括刮擦，燃烧和使基材变形。 所得到的催化剂颗粒可以以约约 3克至300克，体积在5毫升至500毫升之间的浆料，适用于小规模的FCC反应器和高通量实验。

公开(公告)号：US20080146435A1

公开(公告)日：2008-06-19

申请号：US12001361

申请日：2007-12-11

申请人： William A. Wachter ,  Jeffrey T. Elks ,  Brenda A. Raich ,  Theodore E. Datz ,  Mary T. Van Nostrand ,  Gordon F. Stuntz ,  David O. Marler ,  Nicholas Rollman

发明人： William A. Wachter ,  Jeffrey T. Elks ,  Brenda A. Raich ,  Theodore E. Datz ,  Mary T. Van Nostrand ,  Gordon F. Stuntz ,  David O. Marler ,  Nicholas Rollman

IPC分类号： B01J35/02 ,  B01J29/04 ,  B29B9/00

CPC分类号： B01J29/06 ,  B01J29/70 ,  B01J37/0018 ,  B01J37/0072 ,  B01J37/0236 ,  B01J37/08 ,  B01J2229/36 ,  B01J2229/42 ,  C10G11/05

摘要： Catalysts for experimentation are produced having a controlled matrix pore structure. The manufacturing process utilizes tape casting in the drying procedure in which a catalyst slurry is cast on a substrate and dried at a temperature of between about 50° C. to 200° C. for a period of time of about 0.1 to 1.0 hour. The dried catalyst particles can be removed from the substrate by several techniques, including scraping, burning, and deforming the substrate material. The resulting catalytic particles can be produced in an amount of about ca. 3g to 300g from slurries with volumes between 5 cc to 500 cc, which are suitable for small scale FCC reactors and for high throughput experimentation.

摘要翻译： 生产具有受控矩阵孔结构的用于实验的催化剂。 制造方法在干燥过程中使用带铸造，其中将催化剂浆料浇铸在基材上并在约50℃至200℃的温度下干燥约0.1至1.0小时的时间。 干燥的催化剂颗粒可以通过几种技术从基材中除去，包括刮擦，燃烧和使基材变形。 所得到的催化剂颗粒可以以约约 3g至300g，体积在5 cc至500 cc之间的浆料，适用于小型FCC反应器和高通量实验。