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    Process for making nitriles
    21.
    发明授权
    Process for making nitriles 有权
    制造腈的方法

    公开(公告)号：US09040734B2

    公开(公告)日：2015-05-26

    申请号：US13808760

    申请日：2011-06-16

    Applicant: Larry E. Moerbe ,  Tseng H. Chao

    Inventor： Larry E. Moerbe ,  Tseng H. Chao

    IPC: C07C253/10

    CPC classification number: C07C253/10 ,  Y02P20/584 ,  C07C255/04

    Abstract: Adiponitrile is made by reacting 3-pentenenitrile with hydrogen cyanide. The 3-pentenenitrile is made by reacting 1,3-butadiene with hydrogen cyanide and by isomerizing 2-methyl-3-butenenitrile. The reaction of 1,3-butadiene with hydrogen cyanide to produce 3-pentenenitrile also produces small amounts of dinitrile compounds, including adiponitrile (ADN) and methylglutaronitrile (MGN). Methylglutaronitrile is removed to provide an adiponitrile-enriched stream, which is used in a catalyst purification step.

    Abstract translation: 己腈通过3-戊烯腈与氰化氢反应制得。 3-戊烯腈通过使1,3-丁二烯与氰化氢反应并通过异构化2-甲基-3-丁烯腈制备。 1,3-丁二烯与氰化氢反应生成3-戊烯腈也会产生少量的二腈化合物，包括己二腈（ADN）和甲基戊二腈（MGN）。 除去甲基戊二腈以提供富含己二腈的物流，其用于催化剂纯化步骤中。

    Hydrogenation and esterification to form diesters
    26.
    发明授权
    Hydrogenation and esterification to form diesters 失效
    氢化和酯化形成二酯

    公开(公告)号：US08338636B2

    公开(公告)日：2012-12-25

    申请号：US12851296

    申请日：2010-08-05

    Applicant: Yanhui Sun ,  Richard P. Beatty

    Inventor： Yanhui Sun ,  Richard P. Beatty

    IPC: C07C67/08 ,  C07C69/347

    CPC classification number: C07C67/08 ,  C07C67/303 ,  C07C69/40 ,  C07C69/60

    Abstract: A process is disclosed which employs hydrogenation and esterification to form alkyl diesters. The process subjects an unrefined or otherwise not purified composition comprising maleic anhydride production residue to the processes of hydrogenation and esterification and forming diesters at high conversion efficiency.

    Abstract translation: 公开了一种采用氢化和酯化形成烷基二酯的方法。 该方法将包含马来酸酐生产残余物的未精制或未纯化的组合物以高转化率处理氢化和酯化和形成二酯的方法。

    HYDROCYANATION OF 2-PENTENENITRILE
    27.
    发明申请
    HYDROCYANATION OF 2-PENTENENITRILE 有权
    2-苯并噻唑的水解

    公开(公告)号：US20120035387A1

    公开(公告)日：2012-02-09

    申请号：US13022208

    申请日：2011-02-07

    Applicant: James Michael Garner ,  Christian P. Lenges ,  Ronald J. McKinney ,  Wilson Tam

    Inventor： James Michael Garner ,  Christian P. Lenges ,  Ronald J. McKinney ,  Wilson Tam

    IPC: C07C253/10

    CPC classification number: C07C253/10 ,  B01J31/185 ,  B01J2231/32 ,  B01J2531/847 ,  C07C255/04

    Abstract: The invention provides a process for hydrocyanation, comprising: contacting 2-pentenenitrile with hydrogen cyanide at a temperature in the range of about 0° C. to about 150° C. in the presence of at least one Lewis acid promoter and a catalyst precursor composition, wherein the catalyst precursor composition comprises a zero-valent nickel and at least one bidentate phosphite ligand selected from a member of the group represented by Formula I and Formula II, in which all like reference characters have the same meaning, except as further explicitly limited: wherein R1 and R5 are independently selected from the group consisting of C1 to C5 hydrocarbyl; and R2, R3, R4, R6, R7 and R8 are independently selected from the group consisting of H and C1 to C4 hydrocarbyl.

    Abstract translation: 本发明提供一种氢氰化方法，其包括：在至少一种路易斯酸促进剂和催化剂前体组合物的存在下，在约0℃至约150℃的温度范围内使2-戊烯与氰化氢接触 其中所述催化剂前体组合物包含零价镍和至少一种选自由式I和式II表示的基团的成员的二齿亚磷酸酯配体，其中所有相似的附图标记具有相同的含义，除了进一步明确限制 ：其中R 1和R 5独立地选自C 1至C 5烃基; 并且R 2，R 3，R 4，R 6，R 7和R 8独立地选自H和C 1至C 4烃基。

    Hydrocyanation of pentenenitriles
    28.
    发明授权
    Hydrocyanation of pentenenitriles 有权
    戊烯腈的氢氰化

    公开(公告)号：US08088943B2

    公开(公告)日：2012-01-03

    申请号：US12353584

    申请日：2009-01-14

    Applicant: Thomas Foo ,  James Michael Garner ,  Ron Ozer ,  Paul S. Pearlman

    Inventor： Thomas Foo ,  James Michael Garner ,  Ron Ozer ,  Paul S. Pearlman

    IPC: C07C253/00

    CPC classification number: C07C253/10 ,  C07C255/04

    Abstract: The invention provides a hydrocyanation process to produce adiponitrile and other dinitriles having six carbon atoms, in the presence of catalyst composition comprising a zero-valent nickel and at least one bidentate phosphorus-containing ligand wherein the bidentate phosphorus-containing ligand gives acceptable results according to at least one protocol of the 2-Pentenenitrile Hydrocyanation Test Method.

    Abstract translation: 在含有零价镍和至少一种二齿含磷配体的催化剂组合物的存在下，本发明提供了一种氢氰化方法来生产具有六个碳原子的己二腈和其它二腈，其中二齿含磷配体根据 至少一种2-戊烯腈氢氰化测试方法。

    HIGH LOAD BEARING CAPACITY NYLON STAPLE FIBER AND NYLON BLENDED YARNS AND FABRICS MADE THEREFROM
    29.
    发明申请
    HIGH LOAD BEARING CAPACITY NYLON STAPLE FIBER AND NYLON BLENDED YARNS AND FABRICS MADE THEREFROM 审中-公开
    高负载能力尼龙胶带和尼龙混纺纱和织物制成

    公开(公告)号：US20110177738A1

    公开(公告)日：2011-07-21

    申请号：US13120687

    申请日：2009-10-12

    Applicant: Douglas A. Bloom

    Inventor： Douglas A. Bloom

    IPC: D03D15/00 ,  D02G3/00 ,  D01D5/08

    CPC classification number: D03D15/00 ,  D01D5/16 ,  D01D5/26 ,  D01F6/60 ,  D02G3/04 ,  D02G3/442 ,  D03D1/0041 ,  D03D15/12 ,  D10B2201/02 ,  D10B2201/24 ,  D10B2211/02 ,  D10B2321/041 ,  D10B2321/101 ,  D10B2331/02 ,  D10B2331/021 ,  D10B2401/063 ,  D10B2401/16 ,  Y10T428/2913 ,  Y10T428/298 ,  Y10T442/30 ,  Y10T442/313

    Abstract: Disclosed is the preparation of improved high strength nylon staple fibers having a denier per filament of 1.0 to 3.0, a tenacity T at break of at least about 6.0, and a load-bearing capacity, T7, of greater than 3.2. Such nylon staple fibers are produced by preparing tows of relatively uniformly spun and quenched nylon filaments, drawing and annealing such tows via a two-stage drawing and annealing operation using relatively high draw ratios and then cutting or otherwise converting the drawn and annealed tows into the desired high strength nylon staple fibers. The nylon staple fibers so prepared can be blended with other fibers such as cotton staple fibers to produce nylon/cotton (NYCO) yarns which are also of desirably high strength.

    Abstract translation: 公开了改进的高强度尼龙短纤维的制备，每根长丝的旦尼尔为1.0-3.0，断裂强度为至少约6.0，承载能力T7大于3.2。 这种尼龙短纤维通过制备相对均匀的纺丝和淬火尼龙丝的丝束，通过使用相对高的拉伸比的两阶段拉伸和退火操作拉伸和退火这种丝束，然后切割或以其它方式将拉伸和退火的丝束转变成 所需的高强度尼龙短纤维。 如此制备的尼龙短纤维可以与其他纤维如棉短纤维混合，以生产也具有理想的高强度的尼龙/棉（NYCO）纱线。

    Process for making and refining 3-pentenenitrile, and for refining 2-methyl-3-butenenitrile
    30.
    发明授权
    Process for making and refining 3-pentenenitrile, and for refining 2-methyl-3-butenenitrile 有权
    制备和精制3-戊烯腈的方法，以及用于精制2-甲基-3-丁烯腈的方法

    公开(公告)号：US07977502B2

    公开(公告)日：2011-07-12

    申请号：US12353410

    申请日：2009-01-14

    Applicant: Thomas Foo ,  Sigridur S. Kristjansdottir ,  Ronald J. McKinney ,  Ron Ozer ,  Paul S. Pearlman

    Inventor： Thomas Foo ,  Sigridur S. Kristjansdottir ,  Ronald J. McKinney ,  Ron Ozer ,  Paul S. Pearlman

    IPC: C07C253/10

    CPC classification number: C07C253/10 ,  B01J31/185 ,  B01J2231/32 ,  B01J2531/0238 ,  B01J2531/847 ,  C07C255/04 ,  C07C255/07

    Abstract: The invention provides an integrated, continuous process for the production of 3-pentenenitrile, the refining of 3-pentenenitrile, and the refining of 2-methyl-3-butenenitrile, the process comprising: (a) contacting, in a reaction zone, a hydrogen cyanide-containing feed, a butadiene-containing feed, and a catalyst composition, wherein the catalyst composition comprises a zero-valent nickel and at least one bidentate phosphorus-containing ligand selected from the group consisting of a phosphite, a phosphonite, a phosphinite, a phosphine, a mixed phosphorus-containing ligand, and combination thereof; (b) maintaining a residence time in the reaction zone sufficient to convert about 95% or more of the hydrogen cyanide and to produce a reaction mixture comprising 3-pentenenitrile and 2-methyl-3-butenenitrile, wherein the 2-methyl-3-butenenitrile concentration is maintained below about 15 weight percent of the total mass of the reaction mixture; (c) distilling the reaction mixture to obtain a first stream comprising 1,3-butadiene, a second stream comprising 3-pentenenitrile, 2-methyl-3-butenenitrile, (Z)-2-methyl-2-butenenitrile, and optionally 1,3-butadiene, and a third stream comprising the catalyst composition; (d) distilling the second stream to obtain a fourth stream comprising 1,3-butadiene, a fifth stream comprising 2-methyl-3-butenenitrile, (Z)-2-methyl-2-butenenitrile, and optionally 1,3-butadiene, and a sixth stream comprising 3-pentenenitrile; and (e) distilling the fifth stream to obtain a seventh stream comprising 1,3-butadiene, an eighth stream comprising (Z)-2-methyl-2-butenenitrile, and a ninth stream comprising 2-methyl-3-butenenitrile.

    Abstract translation: 本发明提供了一种用于生产3-戊烯腈的整合的连续方法，3-戊烯腈的精制和2-甲基-3-丁烯腈的精制，该方法包括：（a）在反应区中将 含有氰化氢的进料，含丁二烯的进料和催化剂组合物，其中催化剂组合物包含零价镍和至少一种选自亚磷酸酯，亚膦酸酯，亚磷酸盐的二齿含磷配位体 膦，混合含磷配体及其组合; （b）保持反应区中的停留时间足以转化约95％或更多的氰化氢并产生包含3-戊烯腈和2-甲基-3-丁烯腈的反应混合物，其中2-甲基-3- 丁烯腈浓度保持在反应混合物总质量的约15重量％以下; （c）蒸馏反应混合物以获得包含1,3-丁二烯的第一料流，包含3-戊烯腈，2-甲基-3-丁烯腈，（Z）-2-甲基-2-丁烯腈和任选的1 1,3-丁二烯和包含该催化剂组合物的第三料流; （d）蒸馏第二物流以获得包含1,3-丁二烯的第四料流，包含2-甲基-3-丁烯腈，（Z）-2-甲基-2-丁烯腈和任选的1,3-丁二烯的第五料流 ，和包含3-戊烯腈的第六料流; 和（e）蒸馏第五料流以获得包含1,3-丁二烯的第七料流，包含（Z）-2-甲基-2-丁烯腈的第八料流和包含2-甲基-3-丁烯腈的第九料流。

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