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    Photocurable resin composition for the preparation of a printed wiring board and process for the preparation of photocurable resin
    22.
    发明授权
    Photocurable resin composition for the preparation of a printed wiring board and process for the preparation of photocurable resin 失效
    用于制备印刷线路板的光固化树脂组合物和用于制备光固化树脂的方法

    公开(公告)号：US5523383A

    公开(公告)日：1996-06-04

    申请号：US240906

    申请日：1994-05-11

    Applicant: Nobuo Ikeda ,  Teruhisa Kuroki ,  Tatsuo Yamaguchi ,  Hiroyoshi Oomiya

    Inventor： Nobuo Ikeda ,  Teruhisa Kuroki ,  Tatsuo Yamaguchi ,  Hiroyoshi Oomiya

    IPC: C08C19/28 ,  C08C19/36 ,  C08F290/12 ,  C08L19/00 ,  G03F7/038 ,  C08G61/06 ,  C08G73/10

    CPC classification number: C08L19/006 ,  C08C19/28 ,  C08C19/36 ,  C08F290/12 ,  C08F290/128 ,  G03F7/0388

    Abstract: A process for the preparation of a photocurable resin which comprises the steps of(I) (a) imidating 20 to 80 mole % of the acid arthydride groups present in an adduct prepared by the addition reaction of an .alpha.,.beta.-unsaturated dicarboxylic acid arthydride to a conjugated diene polymer or copolymer with a primary amine to produce water and an amide,(b) reacting the thus formed water as a by-product with at least a part of the remaining acid arthydride groups in said adduct to produce the succinic acid groups by opening the ring of said acid arthydride groups,(II) dehydrating the thus produced succinic acid groups by heating to cause ring closure again thereby forming acid anhydride groups and(III) reacting at least a part, preferably at least 50 mole %, of the acid anhydride rings present in the polymer with an .alpha.,.beta.-unsaturated monocarboxylic acid ester having an alcoholic hydroxyl group to conduct a half-esterification by opening the ring of said acid arthydride groups.

    Abstract translation: 一种制备可光固化树脂的方法，其包括以下步骤：（a）（a）酰胺化20-80％（摩尔）存在于通过α，β-不饱和二羧酸亚硫酸酯加成反应制备的加合物中的酸性亚硫酸酯基 与伯胺反应生成水和酰胺的共轭二烯聚合物或共聚物，（b）将如此形成的水作为副产物与所述加合物中剩余的酸亚硫酸酯基团的至少一部分反应，生成琥珀酸 通过打开所述酸性亚硫酸酯基团的环，（II）通过加热使由此产生的琥珀酸基团脱水以再次引起闭环，从而形成酸酐基团，和（III）使至少一部分，优选至少50摩尔％ 的存在于聚合物中的酸酐环与具有醇羟基的α，β-不饱和一元羧酸酯进行半酯化，通过打开所述酸亚硫酸氢盐环的环 ps。

    Poly(benxoic acid), method for the preparation thereof and method for the preparation of poly(p-phenylene) from poly(benzoic acid)
    23.
    发明授权
    Poly(benxoic acid), method for the preparation thereof and method for the preparation of poly(p-phenylene) from poly(benzoic acid) 失效
    聚（苯甲酸），其制备方法和由聚（苯甲酸）制备聚（对亚苯基）的方法

    公开(公告)号：US5312874A

    公开(公告)日：1994-05-17

    申请号：US116702

    申请日：1993-09-07

    Applicant: Susumu Tanaka ,  Kyoji Kaeriyama

    Inventor： Susumu Tanaka ,  Kyoji Kaeriyama

    IPC: C08G61/00 ,  C08G61/06 ,  C08G61/10 ,  C08G83/00

    CPC classification number: C08G61/10

    Abstract: Disclosed is a novel polymeric compound poly(benzoic acid) which is a linear polymer consisting of the 1,4-phenylene linkages, each phenylene group having a carboxyl group. Poly(benzoic acid) can be prepared by hydrolyzing a poly(alkyl benzoate) in the presence of an acid or alkali. The thus obtained poly(benzoic acid) can be converted into a poly(p-phenylene) by the decarbonation reaction thereof in an organic solvent such as quinoline in the presence of metallic copper dust or a copper (II) compound such as copper (II) oxide and copper (II) carbonate hydroxide.

    Abstract translation: 公开了一种新型聚合化合物聚（苯甲酸），它是由1,4-亚苯基键组成的线性聚合物，各亚苯基具有羧基。 聚（苯甲酸）可以通过在酸或碱的存在下水解聚（烷基苯甲酸酯）来制备。 由此得到的聚（苯甲酸）可以在有机溶剂如喹啉中，在金属铜粉或铜（II）化合物如铜（II）的存在下通过其脱碳反应转化成聚（对亚苯基） ）氧化物和碳酸氢铜（II）。

    Metathesis polymerization catalyst and method of polymerizing cyclic olefins therewith
    24.
    发明授权
    Metathesis polymerization catalyst and method of polymerizing cyclic olefins therewith 失效
    复分解聚合催化剂及其与环烯烃聚合的方法

    公开(公告)号：US5266665A

    公开(公告)日：1993-11-30

    申请号：US531663

    申请日：1990-06-01

    Applicant: Christopher J. Hardiman

    Inventor： Christopher J. Hardiman

    IPC: C08F4/26 ,  C08G61/06 ,  C08G61/08 ,  B32B33/00 ,  C08F32/04

    CPC classification number: C08G61/08 ,  Y10S526/902 ,  Y10T428/2991

    Abstract: Cyclic olefin metathesis polymerization catalyst comprising metal compounds wherein said metals consist essentially of a minor amount of a transition metal which Will initiate ring-opening metathesis polymerization of a cyclic olefin and a major amount of at least one second metal which will propagate the polymerization, wherein said catalyst is essentially devoid of pyrophoric metal compounds, e.g. metal alkyls, and preformed metal carbenes. A preferred transition metal is ruthenium. Said second metal can comprise aluminum, copper, hafnium, iron (III), iridium, manganese, molybdenum, nickel, niobium, rhenium, rhodium, tantalum, titanium, tungsten, yttrium, a Lanthanide, zinc or zirconium or a mixture thereof. Using such catalyst cyclic olefin, e.g. norbornene derivatives, can be polymerized, e.g. in an extruder, even in the presence of water.

    Abstract translation: 包含金属化合物的环状烯烃易位聚合催化剂，其中所述金属基本上由少量的过渡金属组成，其将引发环烯烃的开环易位聚合和主要量的至少一种将使聚合反应的第二金属，其中 所述催化剂基本上没有自燃金属化合物，例如 金属烷基和预制金属卡宾。 优选的过渡金属是钌。 所述第二金属可以包括铝，铜，铪，铁（III），铱，锰，钼，镍，铌，铼，铑，钽，钛，钨，钇，镧系元素，锌或锆或它们的混合物。 使用这种催化剂环烯烃，例如 降冰片烯衍生物可以聚合，例如 在挤出机中，甚至在水的存在下。

    Polymerizable compositions containing olefin metathesis catalysts and cocatalysts, and methods of use therefor
    25.
    发明授权
    Polymerizable compositions containing olefin metathesis catalysts and cocatalysts, and methods of use therefor 失效
    含有烯烃复分解催化剂和助催化剂的可聚合组合物及其使用方法

    公开(公告)号：US5198511A

    公开(公告)日：1993-03-30

    申请号：US811785

    申请日：1991-12-20

    Applicant: Katherine A. Brown-Wensley ,  Michael C. Palazzotto ,  William M. Lamanna ,  Larry D. Boardman ,  John E. Gozum ,  Fred B. McCormick

    Inventor： Katherine A. Brown-Wensley ,  Michael C. Palazzotto ,  William M. Lamanna ,  Larry D. Boardman ,  John E. Gozum ,  Fred B. McCormick

    IPC: C08F4/06 ,  C08F4/42 ,  C08F4/80 ,  C08G61/06 ,  C08G61/08 ,  C08L61/08

    CPC classification number: C08G61/08 ,  Y10S526/943

    Abstract: Polymerization of ring-strained cyclic olefins takes place in the presence of a one-part or two-part catalyst which is air and moisture stable and which comprises a transition metal-containing compound.The one-part transition metal-containing catalyst is selected from the group consisting of(a) compounds of the formula(L.sup.1) (L.sup.2)Q whereinQ represents Mo or W;L.sup.1 represents one to six CO (carbonyl) ligands;L.sup.2 represents none to 5 ligands, each of which is a non-ionic compound or unit of a polymer which can be the same or different, each contributes two, four, or six electrons to the metal and is different from L.sup.1 ;wherein the sum of the valence electrons of Q and the electrons contributed by the ligands L.sup.1 and L.sup.2 is 18,(b) at least one of cationic ruthenium and osmium-containing organometallic salts having at least one polyene ligand, and(c) [Ir(RO.sub.2 CHC=CHCO.sub.2 R).sub.2 Cl].sub.2 wherein each R independently is hydrogen or lower alkyl (C.sub.1 to C.sub.4), provided that the oxidation state of the metal is in the range of +3 to 0, and that cocatalysts containing C-halogen bonds are not present.The two-part catalyst comprises(a) a transition metal-containing catalyst, provided that the oxidation state of the transition metal is in the range of +3 to 0, and(b) a cocatalyst selected from the group consisting of(i) terminal or silyl alkynes,(ii) organosilanes containing at least ##STR1## (iii) oxidative salts or oxidative compounds containing an oxygen atom to non-oxygen atom double bond, and(iv) heteroatom-containing alkenes.The polymerized composition is useful to provide molded articles, elastomers, dielectric supports, ionophoric or biologically active materials, composite materials, and the like.

    Abstract translation: 环应变环烯烃的聚合在空气和水分稳定的含有过渡金属的化合物的一部分或两部分催化剂存在下进行。 一部分过渡金属的催化剂选自（a）式（L1）（L2）Q化合物，其中Q表示Mo或W; L1代表一至六个CO（羰基）配体; L2代表无5个配体，它们各自是可以相同或不同的非离子化合物或聚合物单元，每个赋予金属二，四或六个电子，并且不同于L1; 其中Q和由配体L1和L2贡献的电子的价数之和为18，（b）至少一种具有至少一个多烯配体的阳离子钌和含锇的有机金属盐，和（c）[Ir （RO2CHC = CHCO2R）2Cl] 2，其中每个R独立地为氢或低级烷基（C1-C4），条件是金属的氧化态在+3至0的范围内，并且含有C-卤键的助催化剂为 不存在。 两部分催化剂包含（a）含过渡金属的催化剂，条件是过渡金属的氧化态在+3至0的范围内，和（b）选自（i）的助催化剂， （ii）至少含有（iii）氧化盐或含有氧原子的氧化化合物与非氧原子双键的有机硅烷，（iv）含杂原子的烯烃的有机硅烷。 聚合的组合物可用于提供模塑制品，弹性体，电介质载体，离子或生物活性材料，复合材料等。

    Method of making an electrical interconnection device
    26.
    发明授权
    Method of making an electrical interconnection device 失效
    制造电气互连装置的方法

    公开(公告)号：US5196103A

    公开(公告)日：1993-03-23

    申请号：US729525

    申请日：1991-07-12

    Applicant: James C. Tou ,  Paul H. Townsend, III

    Inventor： James C. Tou ,  Paul H. Townsend, III

    IPC: C08G61/06 ,  C23C14/02 ,  C23C14/20 ,  H01L23/498

    CPC classification number: C23C14/20 ,  C08G61/06 ,  C23C14/022 ,  H01L23/49894 ,  H01L2924/0002

    Abstract: The present invention refers to an electrical interconnection device having conductive metal layers separated by a dielectric cyclobutarene polymer layer. The adhesion of the conductive metal layer to the dielectric cyclobutarene polymer layer is promoted by a carbide-forming metal interface layer. Further disclosed is a method of making such electrical interconnection device by ion sputtering the dielectric cyclobutarene polymer surface, vapor depositing a carbide-forming metal interface layer onto the sputtered polymer surface, and then vapor depositing the superior conductive metal layer onto the carbide-forming metal interface layer.

    Abstract translation: 本发明涉及一种具有由介电环丁烯聚合物层分离的导电金属层的电互连装置。 通过碳化物形成金属界面层促进导电金属层与电介质环丁烯聚合物层的粘附。 进一步公开的是通过离子溅射介电环丁烯聚合物表面，将碳化物形成金属界面层气相沉积到溅射的聚合物表面上，然后将上导电金属层气相沉积到碳化物形成金属上的方法 界面层

    Polymerization process employing mixture of Diels-Alder adducts of 4-vinylcyclohexene and cyclopentadiene
    29.
    发明授权
    Polymerization process employing mixture of Diels-Alder adducts of 4-vinylcyclohexene and cyclopentadiene 失效
    使用4-乙烯基环己烯和环戊二烯的狄尔斯 - 阿尔德加合物的混合物的聚合方法

    公开(公告)号：US5095082A

    公开(公告)日：1992-03-10

    申请号：US712296

    申请日：1991-06-10

    Applicant: Donald R. Kelsey

    Inventor： Donald R. Kelsey

    IPC: C08G61/06 ,  C08G61/08

    CPC classification number: C08G61/08

    Abstract: A hard, infusible, crosslinked polymeric product free from detectable cyclopentadiene odor is obtained by contacting, under polymerization conditions, a mixture of Diels-Alder adducts of 4-vinylcyclohexene and cyclopentadiene and Diels-Alder oligomers of cyclopentadiene of at least 3 cyclopentadiene units with an olefin methathesis catalyst.

    Abstract translation: 通过在聚合条件下将4-乙烯基环己烯和环戊二烯的狄尔斯 - 阿尔德加合物和至少3个环戊二烯单元的狄尔斯 - 阿尔德环戊二烯低聚物的混合物与具有至少3个环戊二烯单元的环戊二烯的混合物与 烯烃异构催化剂。

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