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    Stabilized polyethylene material
    31.
    发明授权
    Stabilized polyethylene material 有权
    稳定的聚乙烯材料

    公开(公告)号：US07744972B2

    公开(公告)日：2010-06-29

    申请号：US10579360

    申请日：2004-12-03

    申请人： Thoi H. Ho ,  Detlef Schramm ,  Pak-Meng Cham ,  Kalyan Sehanobish

    发明人： Thoi H. Ho ,  Detlef Schramm ,  Pak-Meng Cham ,  Kalyan Sehanobish

    IPC分类号： F16L9/12

    CPC分类号： F16L11/06 ,  C08K5/13 ,  C08K5/49 ,  C08K2201/014 ,  C08L23/04 ,  Y10T428/139

    摘要： Stabilized polyethylene materials which offer an advantageously balanced combination of thermal, mechanical and processing properties, and which maintain their physical properties in chlorinated water environments are disclosed. The materials include an antioxidant system with components to provide extraction resistance in hot water environments and additionally provides oxidation resistance to both chlorine in the water interior of the pipe and oxygen in contact with the pipe's exterior.

    摘要翻译： 公开了稳定的聚乙烯材料，其提供热，机械和加工性能的有利平衡组合，并且在氯化水环境中保持其物理性能。 这些材料包括具有在热水环境中提供提取阻力的组分的抗氧化系统，并且还对管道的水内部的氯和与管道外部接触的氧进行氧化抗性。

    POLYETHYLENE COMPOSITIONS, METHODS OF MAKING THE SAME, AND ARTICLES PREPARED THEREFROM
    32.
    发明申请
    POLYETHYLENE COMPOSITIONS, METHODS OF MAKING THE SAME, AND ARTICLES PREPARED THEREFROM 有权
    聚乙烯组合物，其制备方法和制备的制品

    公开(公告)号：US20100003439A1

    公开(公告)日：2010-01-07

    申请号：US12446652

    申请日：2007-10-19

    申请人： William J. Michie, JR. ,  Dane Chang ,  Lonnie G. Hazlitt ,  Stephanie M. Whited ,  Michael A. Kinnan ,  Anthony C. Neubauer ,  Thoi H. Ho

    发明人： William J. Michie, JR. ,  Dane Chang ,  Lonnie G. Hazlitt ,  Stephanie M. Whited ,  Michael A. Kinnan ,  Anthony C. Neubauer ,  Thoi H. Ho

    IPC分类号： B32B1/08 ,  C08L23/08 ,  C08K5/17 ,  C08K5/13 ,  C08K5/53 ,  C08K5/09

    CPC分类号： C08L23/26 ,  C08L23/0815 ,  C08L2205/02 ,  C08L2666/06

    摘要： The invention is related to compositions suitable for the fabrication of pipes, and other articles, with excellent performance properties. The invention provides a composition, comprising a blend, wherein said blend comprises a high molecular weight ethylene-based interpolymer and a low molecular weight ethylene-based interpolymer, and the high molecular weight ethylene-based interpolymer is a heterogeneously branched linear or a homogeneously branched linear ethylene-based interpolymer, and has a density from 0.922 g/cc to 0.929 g/cc, and a high load melt index (I21) from 0.2 g/10 min to 1.0 g/10 min, and the low molecular weight ethylene-based interpolymer is heterogeneously branched linear or a homogeneously branched linear ethylene-based interpolymer, and has a density from 0.940 g/cc to 0.955 g/cc, and a melt index (I2) from 6 g/10 min to 50 g/10 min. The blend has a single peak in an ATREF profile eluting above 30° C., and has a coefficient of viscosity average molecular weight (CM?) less than −0.0032 in the log(calculated Mv) versus elution temperature, said CMv calculated in the range of elution temperatures from 70° C. to 90° C. The Mv is the viscosity average molecular weight.

    摘要翻译： 本发明涉及适于制造具有优异性能的管道和其它制品的组合物。 本发明提供一种包含共混物的组合物，其中所述共混物包含高分子量乙烯基互聚物和低分子量乙烯基互聚物，并且高分子量乙烯基互聚物是非均匀支化的线性或均匀分支的 线性乙烯类互聚物，密度为0.922g / cc〜0.929g / cc，高负荷熔融指数（I21）为0.2g / 10min〜1.0g / 10min，低分子量乙烯 - 基于异构支化的线型或均匀支化的线性乙烯基互聚物，其密度为0.940g / cc至0.955g / cc，熔体指数（I 2）为6g / 10min至50g / 10min 。 共混物在30℃以上洗脱的ATREF谱中具有单峰，并且在对数（计算的Mv）相对于洗脱温度具有小于-0.0032的粘均分子量（CM 3）系数，所述CMv计算为 洗脱温度范围为70℃至90℃.Mv为粘均分子量。

    Process for preparing thermoplastic vulcanizates
    34.
    发明授权
    Process for preparing thermoplastic vulcanizates 失效
    制备热塑性硫化胶的方法

    公开(公告)号：US06277916B1

    公开(公告)日：2001-08-21

    申请号：US09257771

    申请日：1999-02-25

    申请人： Robert H. Terbrueggen ,  Ray E. Drumright ,  Thoi H. Ho

    发明人： Robert H. Terbrueggen ,  Ray E. Drumright ,  Thoi H. Ho

    IPC分类号： C08L5300

    CPC分类号： C08K5/43 ,  C08F8/34 ,  C08F2800/20 ,  C08F2810/20 ,  C08F210/02 ,  C08F212/08 ,  C08F297/04 ,  C08F297/046 ,  C08F8/04 ,  C08F210/18

    摘要： This invention includes a process for forming a thermoplastic vulcanizate comprising: (a) admixing a C—H insertion curing agent with at least one elastomeric phase polymer to form a first admixture; (b) admixing at least one non-elastomeric polyolefin with the first admixture to form a second admixture; and (c) heating the second admixture to a temperature at least the decomposition temperature of the curing agent to crosslink the elastomeric phase while mixing the admixture to an extent sufficient to result in the formation of a thermoplastic material, hereinafter referred to as a thermoplastic vulcanizate, and optionally including an additional step (d) of shaping the resulting thermoplastic vulcanizate, especially by heating and foaming or molding the TPV. The C—H insertion curing agent is preferably selected from alkyl and aryl azides (R—N3), acyl azides (R—C(O)N3), azidoformates (R—O—C(O)—N3), sulfonyl azides (R—SO2—N3), phosphoryl azides ((RO)2—(PO)—N3), phosphinic azides (R2—P(O)—N3) and silyl azides (R3—Si—N3), with poly(sulfonyl azide) most preferred. Additionally, the invention includes a thermoplastic vulcanizate comprising a blend of: (1) an elastomeric phase crosslinked using a C—H insertion curing agent dispersed in; (2) at least one non-elastomeric thermoplastic polyolefin. The invention also includes a foamable composition comprising (1) an elastomeric phase crosslinked using a C—H insertion curing agent dispersed in; (2) at least one non-elastomeric thermoplastic polyolefin; and (3) from about 0.1 to about 25 percent by weight based on the combined weight of components (1) and (2) of at least one foaming agent as well as a fabricated part, cable jacket, cable insulation, or foam comprising the thermoplastic vulcanizate or the invention or resulting from the process of the invention.

    摘要翻译： 本发明包括形成热塑性硫化橡胶的方法，其包括：（a）将C-H嵌入固化剂与至少一种弹性体相聚合物混合以形成第一混合物; （b）将至少一种非弹性体聚烯烃与第一混合物混合以形成第二混合物; 和（c）将第二混合物加热到至少固化剂的分解温度的温度以交联弹性体相，同时将该混合物混合到足以导致形成热塑性材料的程度，以下称为热塑性硫化橡胶 并且任选地包括使得到的热塑性硫化橡胶成型的附加步骤（d），特别是通过加热和发泡或模制TPV。 CH插入固化剂优选选自烷基和芳基叠氮化物（R-N 3），酰基叠氮化物（RC（O）N 3），叠氮基甲酸酯（ROC（O）-N 3），磺酰基叠氮化物（R-SO 2 -N 3） 叠氮化物（（RO）2-（PO）-N3），次膦酸叠氮化物（R2-P（O）-N3）和甲硅烷基叠氮化物（R3-Si-N3），最优选为聚（磺酰基叠氮化物）。 另外，本发明包括热塑性硫化橡胶，其包含以下共混物：（1）使用分散在其中的C-H嵌入固化剂交联的弹性体相; （2）至少一种非弹性体热塑性聚烯烃。 本发明还包括可发泡组合物，其包含（1）使用分散在其中的C-H插入固化剂交联的弹性体相; （2）至少一种非弹性热塑性聚烯烃; 和（3）约0.1至约25重量％，基于至少一种发泡剂的组分（1）和（2）的组合重量，以及制造的部件，电缆护套，电缆绝缘或泡沫，其包含 热塑性硫化橡胶或本发明，或由本发明的方法得到。

    ETHYLENE-BASED COMPOSITIONS
    37.
    发明申请
    ETHYLENE-BASED COMPOSITIONS 审中-公开
    乙烯基组合物

    公开(公告)号：US20140004287A1

    公开(公告)日：2014-01-02

    申请号：US14004860

    申请日：2012-03-14

    申请人： Carl F. Baker ,  Thoi H. Ho

    发明人： Carl F. Baker ,  Thoi H. Ho

    IPC分类号： C08K5/00

    CPC分类号： C08K5/00 ,  C08K5/0008 ,  C08K5/005 ,  C08K5/13 ,  C08K5/1345 ,  C08K5/25 ,  C08K5/526 ,  Y10T428/139 ,  C08L23/0815

    摘要： The invention provides a composition comprising the following: A) an ethylene-based polymer; B) a compound selected from Formula 1, as shown herein, wherein R1 and R2 are each independently selected from a C1-C20 alkyl group; X is selected from Cl, Br, I, F, OH, NH2, NHR′ or NR′R″, where R′ and R″ are each independently a C1-C6 alkyl; n is from 1 to 10; and m is from 10 to 30; and wherein this compound is present in an amount greater than, or equal to, 500 ppm, based on the total weight of the composition; C) a compound selected from Formula 2, as shown herein, wherein R1, R2 and R3 are each independently selected N from a C1-C20 alkyl group; R4, R5, R6, R7, R8 and R9 are each independently selected from a C1-C20 alkyl group; X1, X2 and X3 are each independently selected from Cl, Br, I, F, OH, NH2, NHR′ or NR′R″, where R′ and R″ are each independently a C1-C6 alkyl; n is from 1 to 6; m is from 1 to 6; and o is from 1 to 6; and wherein the weight ratio of Component C to Component B (C/B) is greater than 1.

    摘要翻译： 本发明提供了包含以下物质的组合物：A）乙烯类聚合物; B）选自式1的化合物，如本文所示，其中R 1和R 2各自独立地选自C 1 -C 20烷基; X选自Cl，Br，I，F，OH，NH 2，NHR'或NR'R“，其中R'和R”各自独立地为C 1 -C 6烷基; n为1至10; m为10〜30; 并且其中该化合物以基于组合物的总重量大于或等于500ppm的量存在; C）选自式2的化合物，如本文所示，其中R 1，R 2和R 3各自独立地选自C 1 -C 20烷基; R 4，R 5，R 6，R 7，R 8和R 9各自独立地选自C 1 -C 20烷基; X1，X2和X3各自独立地选自Cl，Br，I，F，OH，NH2，NHR'或NR'R“，其中R'和R”各自独立地为C1-C6烷基; n为1至6; m为1〜6; o为1〜6; 并且其中组分C与组分B的重量比（C / B）大于1。

    Stabilized polyethylene material
    38.
    发明授权
    Stabilized polyethylene material 有权
    稳定的聚乙烯材料

    公开(公告)号：US08163226B2

    公开(公告)日：2012-04-24

    申请号：US12787695

    申请日：2010-05-26

    申请人： Thoi H. Ho ,  Detlef Schramm ,  Pak-Meng Cham ,  Kalyan Sehanobish

    发明人： Thoi H. Ho ,  Detlef Schramm ,  Pak-Meng Cham ,  Kalyan Sehanobish

    IPC分类号： B29D23/00 ,  B32B1/08

    CPC分类号： F16L11/06 ,  C08K5/13 ,  C08K5/49 ,  C08K2201/014 ,  C08L23/04 ,  Y10T428/139

    摘要： Stabilized polyethylene materials which offer an advantageously balanced combination of thermal, mechanical and processing properties, and which maintain their physical properties in chlorinated water environments are disclosed. The materials include an antioxidant system with components to provide extraction resistance in hot water environments and additionally provides oxidation resistance to both chlorine in the water interior of the pipe and oxygen in contact with the pipe's exterior.

    摘要翻译： 公开了稳定的聚乙烯材料，其提供热，机械和加工性能的有利平衡组合，并且在氯化水环境中保持其物理性能。 这些材料包括具有在热水环境中提供提取阻力的组分的抗氧化系统，并且还对管道的水内部的氯和与管道外部接触的氧气另外提供抗氧化性。