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    METHOD FOR PRODUCING NITROUS ACID ESTER, AND METHOD FOR PRODUCING DIALKYL OXALATE AND DIALKYL CARBONATE
    35.
    发明申请
    METHOD FOR PRODUCING NITROUS ACID ESTER, AND METHOD FOR PRODUCING DIALKYL OXALATE AND DIALKYL CARBONATE 有权
    生产硝酸酯的方法，以及生产二烷基氧化铝和碳酸二乙酯的方法

    公开(公告)号：US20150065742A1

    公开(公告)日：2015-03-05

    申请号：US14389583

    申请日：2013-02-27

    Applicant: UBE INDUSTRIES, LTD

    Inventor： Syuji Tanaka ,  Hirofumi Ii ,  Akira Hino ,  Yuya Fukui ,  Satoshi Ueda

    IPC: C07C201/04 ,  C07C68/00 ,  C07C67/36

    CPC classification number: C07C201/04 ,  C07C67/36 ,  C07C68/00 ,  C07C69/96 ,  C07C69/36 ,  C07C203/00

    Abstract: A method for producing nitrous acid ester in which nitric oxide, oxygen, and an alcohol are reacted, thereby generating nitrous acid ester includes a step of generating nitrous acid ester by supplying a bottom liquid from a bottom part of the reaction column, and nitric oxide and/or carbon monoxide, a step of supplying nitrous acid ester to the reaction column; a step of supplying a reaction liquid containing water, nitric acid, and the alcohol to a nitric acid condensing column from the reactor; and a step of separating a low-boiling point component by distillation from the reaction liquid under control of a concentration of the alcohol in a condensed liquid being generated at a bottom part of the nitric acid condensing column to be less than 4.0% by weight so as to introduce the condensed liquid into the reactor from the nitric acid condensing column.

    Abstract translation: 一氧化氮，氧和醇反应生成亚硝酸酯的方法，从而产生亚硝酸酯包括通过从反应塔的底部供应底部液体和一氧化氮产生亚硝酸酯的步骤 和/或一氧化碳，向反应塔供应亚硝酸酯的步骤; 将含有水，硝酸和醇的反应液体从反应器供给到硝酸冷凝塔的步骤; 在硝酸浓缩塔的底部产生的冷凝液中，醇的浓度控制下，通过蒸馏将反应液中的低沸点成分分离成低于4.0重量％的步骤，从而 将浓缩的液体从硝酸冷凝塔引入反应器。

    Method for the manufacture of therapeutic compounds and compositions, compounds and compositions produced therewith, and their use
    37.
    发明授权
    Method for the manufacture of therapeutic compounds and compositions, compounds and compositions produced therewith, and their use 有权
    用于制备治疗化合物和组合物，由其制备的化合物和组合物的方法及其用途

    公开(公告)号：US08030511B2

    公开(公告)日：2011-10-04

    申请号：US12282878

    申请日：2007-03-14

    Applicant: Lars E. Gustafsson ,  Dag Linnarsson ,  Kristofer Nilsson

    Inventor： Lars E. Gustafsson ,  Dag Linnarsson ,  Kristofer Nilsson

    IPC: C07C203/04

    CPC classification number: C07C201/04 ,  C07B43/02 ,  C07C203/00

    Abstract: Organic nitrites can be produced from a compound which is a mono/polyhydric alcohol or an aldehyde- or ketone-derivate thereof after de-aeration of the same, using NO gas, and stored in an environment saturated with gaseous NO. Organic nitrites produced according to the invention exhibit less impurities and improved storage stability compared to conventionally produced nitrites. The organic nitrites of the invention can easily be formulated into pharmaceutical compositions and have utility for the treatment of various conditions.

    Abstract translation: 有机亚硝酸盐可以通过使用NO气体在其通气之后从作为单/多元醇或其醛衍生物或酮衍生物的化合物生产，并储存在饱和有NO的环境中。 根据本发明生产的有机亚硝酸盐与常规生产的亚硝酸盐相比表现出较少的杂质和改善的储存稳定性。 本发明的有机亚硝酸盐可以容易地配制成药物组合物，并具有治疗各种病症的效用。

    Process for producing alkyl nitrite
    39.
    发明授权
    Process for producing alkyl nitrite 有权
    亚硝酸烷基酯的制备方法

    公开(公告)号：US06191302B1

    公开(公告)日：2001-02-20

    申请号：US09176372

    申请日：1998-10-21

    Applicant: Keigo Nishihira ,  Shuji Tanaka ,  Shinichi Yoshida

    Inventor： Keigo Nishihira ,  Shuji Tanaka ,  Shinichi Yoshida

    IPC: C07C20302

    CPC classification number: C07C201/04 ,  C07C203/00

    Abstract: An alkyl nitrite can be produced on an industrial scale with a high efficiency and with a low yield of by-products by the process wherein nitrogen oxide-containing feed gas is brought into an alkyl alcohol liquid in a distillation column reactor while circulating a liquid fraction, produced in the reactor and containing the alkyl alcohol, through a circulation path including a lower section of the reactor and a cooler to remove the reaction heat vigorously generated in the reactor, and while controlling the weight ratio of the circulating liquid fraction to the total alkyl alcohol fed into the reactor to 50:1 to 200:1, the molar ratio of the total alkyl alcohol fed to the reactor and contained in the circulating liquid fraction to nitrogen oxide in the feed gas to 20:1 to 150:1, and the content of the alkyl alcohol in the liquid fraction to 15 to 60% by weight; and the resultant gas fraction containing the target alkyl nitrite is collected from the reactor.

    Abstract translation: 亚硝酸烷基酯可以在工业规模上以高效率和低产率的副产物生产，其中将含氮氧化物的进料气体在蒸馏塔反应器中进入烷基醇液体，同时使液体馏分 在反应器中生产并含有烷基醇，通过包括反应器的下部的循环路径和冷却器，以除去在反应器中剧烈产生的反应热，同时控制循环液体馏分与总的重量比 将进料到反应器中的烷基醇的摩尔比为50:1至200:1，进料到反应器中并且包含在循环液体馏分中的总烷基醇与进料气体中的氮氧化物的摩尔比为20:1-150:1， 并且液体馏分中的烷基醇的含量为15〜60重量％ 从反应器收集含有目标亚硝酸烷基酯的所得气体馏分。

    Nitration of organic compounds and organic nitrogen compounds produced
    40.
    发明授权
    Nitration of organic compounds and organic nitrogen compounds produced 失效
    生成有机化合物和有机氮化合物的硝化

    公开(公告)号：US4496783A

    公开(公告)日：1985-01-29

    申请号：US489467

    申请日：1983-04-28

    Applicant: Ian M. Campbell ,  Donald L. Baulch ,  Gary J. Audley

    Inventor： Ian M. Campbell ,  Donald L. Baulch ,  Gary J. Audley

    IPC: C07B43/00 ,  C07B31/00 ,  C07C67/00 ,  C07C201/00 ,  C07C201/02 ,  C07C201/04 ,  C07C201/08 ,  C07C203/00 ,  C07C203/02 ,  C07C205/02 ,  C07C79/02

    CPC classification number: C07C201/08 ,  C07C201/02 ,  C07C201/04

    Abstract: Nitration of organic compounds and organic nitrogen compounds produced.Organic nitrogen compounds are formed in the vapor phase by organic radical formation by reaction of an organic compound with hydroxyl radicals derived from the reaction between hydrogen peroxide and nitrogen dioxide and the nitration of the organic radicals, suitably with nitrogen dioxide. The process may be conducted as a single stage process using an excess of nitrogen dioxide over that required for hydroxyl radical formation. The production of hydroxyl radicals is maximized by the use of a catalytic solid surface such as a solid acid or an acidic oxide or mixed oxide. The product may be a mixture of some or all of the nitrite, nitrate and nitro-derivative which may be used as such, e.g. as a fuel additive, as a source of the individual compounds or as a feedstock for a further synthesis.

    Abstract translation: 生成有机化合物和有机氮化合物的硝化。 通过有机化合物与过氧化氢和二氧化氮之间的反应衍生的羟基自由基反应形成有机氮化合物，并适当地用二氧化氮硝化有机氮化合物。 该方法可以作为使用过量二氧化氮超过羟基自由基形成所需的二氧化氮的单阶段方法进行。 通过使用催化固体表面如固体酸或酸性氧化物或混合氧化物，使羟基自由基的产生最大化。 产物可以是一些或全部亚硝酸根，硝酸根和硝基衍生物的混合物，可以如此使用。 作为燃料添加剂，作为单独化合物的来源或作为进一步合成的原料。

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