Boron filled hybrid nanotubes
    32.
    发明授权

    公开(公告)号:US10453583B2

    公开(公告)日:2019-10-22

    申请号:US15249349

    申请日:2016-08-27

    摘要: A boron filled hybrid nanotube and a method for producing and rendering boron filled hybrid nanotubes suitable for applications are provided. A mixture of a boron containing nanowire producing compound and catalysts is prepared and ground for a predetermined time period. The ground mixture is subjected to a vapor deposition process including passing an inert gas over the ground mixture after adding a nanotube producing compound to the ground mixture or after passing a reactant gas on the ground mixture in a reactor at a configurable reaction temperature and a configurable reaction pressure for a configurable reaction time to produce the boron filled hybrid nanotubes with enhanced mechanical, thermal and electrical properties. Each boron filled hybrid nanotube includes one or more boron based nanowires embedded within one or more single walled or multi-walled nanotubes. The boron filled hybrid nanotubes are further purified and functionalized using acids, and/or bases, and/or surfactants.

    Toughened and corrosion- and wear-resistant composite structures and fabrication methods thereof
    35.
    发明授权
    Toughened and corrosion- and wear-resistant composite structures and fabrication methods thereof 有权
    增韧耐腐蚀和耐磨复合结构及其制造方法

    公开(公告)号:US08691343B2

    公开(公告)日:2014-04-08

    申请号:US12122024

    申请日:2008-05-16

    摘要: Composite structures having a reinforced material interjoined with a substrate and methods of creating a composite material interjoined with a substrate. In some embodiments the composite structure may be a line or a spot or formed by reinforced material interjoined with the substrate. The methods typically include disposing a precursor material comprising titanium diboride and/or titanium monoboride on at least a portion of the substrate and heating the precursor material and the at least a portion of the substrate in the presence of an oxidation preventative until at least a portion of the precursor material forms reinforced material interjoined with the substrate. The precursor material may be disposed on the substrate as a sheet or a tape or a slurry or a paste. Localized surface heating may be used to heat the precursor material. The reinforced material typically comprises a titanium boron compound, such as titanium monoboride, and preferably comprises β-titanium. The substrate is typically titanium-bearing, iron-bearing, or aluminum-bearing. A welding rod is provided as an embodiment. The welding rod includes a metal electrode and a precursor material is disposed adjacent at least a portion of the metal electrode. A material for use in forming a composite structure is provided. The material typically includes a precursor material that includes one or more materials selected from the following group: titanium diboride and titanium monoboride. The material also typically includes a flux.

    摘要翻译: 具有与衬底相连的增强材料的复合结构和产生与衬底相连的复合材料的方法。 在一些实施例中,复合结构可以是线或点,或者由与衬底相连的增强材料形成。 所述方法通常包括将包含二硼化钛和/或单硼酸钛的前体材料设置在所述基材的至少一部分上,并且在氧化防止剂存在下加热所述前体材料和所述基材的至少一部分直至至少部分 的前体材料形成与衬底相互连接的增强材料。 前体材料可以作为片材或带或浆料或糊料设置在基底上。 局部表面加热可用于加热前体材料。 增强材料通常包含钛硼化合物,例如单硼酸钛,并且优选包含钛。 基底通常是含钛,含铁或含铝的。 作为实施例提供焊条。 焊条包括金属电极,并且前体材料邻近金属电极的至少一部分设置。 提供了用于形成复合结构的材料。 材料通常包括前体材料,其包括选自以下组的一种或多种材料:二硼化钛和单硼酸钛。 该材料通常还包括助焊剂。

    Combustion synthesis method and boron-containing materials produced therefrom
    36.
    发明授权
    Combustion synthesis method and boron-containing materials produced therefrom 有权
    燃烧合成方法和由其制备的含硼材料

    公开(公告)号:US08557208B2

    公开(公告)日:2013-10-15

    申请号:US12472050

    申请日:2009-05-26

    IPC分类号: C01B35/00 C01B35/02 C01B35/04

    CPC分类号: C01B35/04

    摘要: One embodiment of the present disclosure provides a method of making a ceramic material that contains boron and a metal. A metal source, an oxidizer, a boron source, and a fuel source are combined. These reactants are then heated at, or to, a temperature sufficient to initiate a combustion reaction. The combustion reaction produces a ceramic material that includes boron and the metal. The present disclosure also provides materials formed by the disclosed method, as well as methods and systems using such materials.

    摘要翻译: 本公开的一个实施方案提供了制备含有硼和金属的陶瓷材料的方法。 金属源,氧化剂,硼源和燃料源组合。 然后将这些反应物加热至足以引发燃烧反应的温度。 燃烧反应产生包括硼和金属的陶瓷材料。 本公开还提供了通过所公开的方法形成的材料,以及使用这种材料的方法和系统。

    METHOD FOR CYCLICALLY PREPARING MONOMER BORON AND COPRODUCING POTASSIUM CRYOLITE USING POTASSIUM FLUOBORATE AS INTERMEDIATE MATERIAL
    37.
    发明申请
    METHOD FOR CYCLICALLY PREPARING MONOMER BORON AND COPRODUCING POTASSIUM CRYOLITE USING POTASSIUM FLUOBORATE AS INTERMEDIATE MATERIAL 失效
    使用氟化钾作为中间材料循环制备单体硼和共混磷酸钙的方法

    公开(公告)号:US20130095023A1

    公开(公告)日:2013-04-18

    申请号:US13708959

    申请日:2012-12-08

    IPC分类号: C01B35/02

    摘要: A method for cyclically preparing monomer boron and coproducing potassium cryolite using potassium fluoborate as an intermediate material, which includes following steps: A) adding hydrofluoric acid to boric acid or boron oxide to enable a reaction to form fluoboric acid; B) adding a potassium sulphate aqueous solution to the fluoboric acid to enable a reaction to form the potassium fluoborate; C) putting the potassium fluoborate into a reactor, adding aluminium to react with the potassium fluoborate to form the monomer boron and potassium cryolite; D) extracting the potassium cryolite, sending the potassium cryolite to a rotary reaction kettle together with concentrated sulphuric acid to enable a reaction to form hydrogen fluoride gas and aluminium potassium sulphate, potassium sulphate, collecting the hydrogen fluoride gas and dissolving it into water to obtain the hydrofluoric acid; E) recycling the obtained hydrofluoric acid to Step A to leach the boric acid or boron oxide.

    摘要翻译: 使用氟硼酸钾作为中间体循环制备单体硼并共同生产钾冰晶石的方法,其包括以下步骤:A)向硼酸或氧化硼中加入氢氟酸以使反应形成氟硼酸; B)向氟硼酸中加入硫酸钾水溶液以使其形成氟硼酸钾; C)将氟硼酸钾放入反应器中,加入铝与氟硼酸钾反应形成单体硼和钾冰晶石; D)提取钾冰晶石,将钾冰晶石与浓硫酸一起送入旋转反应釜,使反应生成氟化氢气体和硫酸铝钾,硫酸钾,收集氟化氢气体并将其溶于水中,得到 氢氟酸; E)将获得的氢氟酸循环到步骤A以浸出硼酸或氧化硼。

    METHOD FOR REMOVING CONTAMINANTS FROM BORON POWDER
    38.
    发明申请
    METHOD FOR REMOVING CONTAMINANTS FROM BORON POWDER 有权
    从BORON粉中去除污染物的方法

    公开(公告)号:US20130052114A1

    公开(公告)日:2013-02-28

    申请号:US13220053

    申请日:2011-08-29

    IPC分类号: C01B35/02

    CPC分类号: C01B35/023

    摘要: Methods for removing an organic contaminant from contaminated boron powder are provided. One method includes providing a contaminated boron powder, the boron powder being comingled with an organic contaminant. The method also includes placing the contaminated boron powder and the organic contaminant comingled therewith onto an inert container. The method includes placing the inert container, the contaminated boron powder, and the organic contaminant comingled therewith, into an enclosed space. A heat source is provided in the enclosed space. The method also includes heating the contaminated boron powder and the organic contaminant comingled therewith to an elevated temperature. The method includes altering the organic contaminant so as to reduce the amount of the organic contaminant comingled with the boron powder. Another method includes reducing the amount of the organic contaminant comingled with the boron powder to not more than about 0.1 weight percent of soluble residue.

    摘要翻译: 提供了从污染的硼粉中除去有机污染物的方法。 一种方法包括提供污染的硼粉末,硼粉末与有机污染物一起流出。 该方法还包括将污染的硼粉末和与其接触的有机污染物放置在惰性容器上。 该方法包括将惰性容器,被污染的硼粉末和与其接触的有机污染物放置在封闭空间中。 在封闭空间设有热源。 该方法还包括将被污染的硼粉和与其接触的有机污染物加热到升高的温度。 该方法包括改变有机污染物,以便减少与硼粉混合的有机污染物的量。 另一种方法包括将硼粉末的有机污染物的量减少到不超过约0.1重量%的可溶性残余物。