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公开(公告)号：US20100076238A1
公开(公告)日：2010-03-25
申请号：US12624999
申请日：2009-11-24
CPC分类号： C10L1/08 , C10G3/46 , C10G3/50 , C10G45/58 , C10G47/00 , C10G2300/1014 , C10G2300/1018 , C10G2300/1022 , C10G2300/1037 , C10G2300/4081 , C10G2300/80 , C10G2400/02 , C10G2400/04 , C10G2400/08 , C10G2400/28 , C10L1/06 , Y02E50/13 , Y02P30/20 , Y02T50/678
摘要： A process for producing a fuel or fuel blending component from co-processing at least two different classes of renewable feedstocks, is presented. One feedstock comprises glycerides and free fatty acids in feedstocks such as plant and animal oils while the other feedstock comprises biomass derived pyrolysis oil. The source of the animal or plant oil and the biomass may be the same renewable source.
摘要翻译： 提出了一种从共同处理至少两种不同类别的可再生原料生产燃料或燃料调和组分的方法。 一种原料在原料如植物油和动物油中包含甘油酯和游离脂肪酸，而另一种原料包括生物质衍生的热解油。 动物或植物油和生物质的来源可能是相同的可再生能源。
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公开(公告)号：US20090287029A1
公开(公告)日：2009-11-19
申请号：US12402873
申请日：2009-03-12
IPC分类号： C10G3/00
CPC分类号： C10G45/58 , C01B2203/0233 , C01B2203/0244 , C01B2203/062 , C10G3/42 , C10G3/50 , C10G3/52 , C10G45/64 , C10G45/72 , C10G47/00 , C10G47/36 , C10G65/12 , C10G2300/1014 , C10G2300/1018 , C10G2300/1022 , C10G2300/1037 , C10G2300/4081 , C10G2300/80 , C10G2400/04 , C10G2400/08 , C10L1/08 , Y02E50/13 , Y02P30/20 , Y02T50/678
摘要： A process for controlling the concurrent production of both diesel range hydrocarbons and aviation range hydrocarbons from renewable feedstocks such as plant oils and animal oils. The process involves determining the required specification of the desired products and the desired relative yields of the product that still meet the required specifications. The necessary isomerization and selective hydrocracking zone conditions are determined in order to create a mixture of paraffins which meet the required product specifications and yields. The necessary fractionation zone conditions are determined to separate the desired products. A renewable feedstock is treated by hydrogenating and deoxygenating to provide an effluent comprising paraffins, isomerizing and selectively hydrogenating at least a portion of the paraffins at the predetermined conditions, and separating by fractionation at the predetermined fractionation conditions to generate a diesel range hydrocarbon product and an aviation range hydrocarbon product.
摘要翻译： 控制从可再生原料如植物油和动物油同时生产柴油范围碳氢化合物和航空范围烃的过程。 该过程包括确定所需产品的所需规格以及仍符合要求规格的产品所需的相对产量。 确定所需的异构化和选择性加氢裂化区条件以产生满足所需产物规格和产率的石蜡混合物。 确定所需的分馏区条件以分离所需的产物。 通过氢化和脱氧来处理可再生原料以提供包含链烷烃的流出物，在预定条件下异构化和选择性氢化至少一部分链烷烃，并通过在预定分馏条件下分级分离以产生柴油范围烃产物和 航空范围烃产品。
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公开(公告)号：US20090283442A1
公开(公告)日：2009-11-19
申请号：US12402078
申请日：2009-03-11
申请人： Michael J. McCall , Joseph A. Kocal , Alakananda Bhattacharyya , Tom N. Kalnes , Timothy A. Brandvold
发明人： Michael J. McCall , Joseph A. Kocal , Alakananda Bhattacharyya , Tom N. Kalnes , Timothy A. Brandvold
CPC分类号： C10G3/47 , C10G3/46 , C10G3/49 , C10G3/52 , C10G45/02 , C10G45/58 , C10G47/00 , C10G2300/1014 , C10G2300/1018 , C10G2300/1022 , C10G2300/1037 , C10G2300/4081 , C10G2300/80 , C10G2400/08 , Y02P30/20
摘要： A hydrocarbon product stream having hydrocarbons with boiling points in the aviation fuel range is produced from renewable feedstocks such as plant and animal oils. The process involves treating a renewable feedstock by hydrogenating, deoxygenating, isomerization, and selectively hydrocracking the feedstock to produce paraffinic hydrocarbons having from about 9 to about 16 carbon atoms and a high iso/normal ratio in a single reaction zone containing a multifunctional catalyst, or set of catalysts, having hydrogenation, deoxygenation, isomerization and selective hydrocracking functions.
摘要翻译： 在航空燃料范围内具有沸点的烃的烃产物流由可再生原料如植物油和动物油生产。 该方法包括通过氢化，脱氧，异构化和选择性加氢裂解原料来处理可再生原料，以在含有多官能催化剂的单个反应区中产生具有约9至约16个碳原子的链烷烃和高异/正常比例，或 具有氢化，脱氧，异构化和选择性加氢裂化功能的催化剂组。
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公开(公告)号：US20080249198A1
公开(公告)日：2008-10-09
申请号：US11697780
申请日：2007-04-09
IPC分类号： C07C27/06
CPC分类号： C07C29/095 , C07C67/035 , C12C11/02 , C07C31/04 , C07C69/63
摘要： A process for the oxidation of methane to methanol has been developed. The process involves contacting a gas stream, comprising methane, a solvent and an oxidizing agent with a bimetallic catalyst at oxidation conditions to produce a methyl ester. Finally, the methyl ester is hydrolyzed to yield a methanol product stream. The bimetallic catalyst comprises at least two transition metal components. One example of the catalytic component is a combination of cobalt and manganese.
摘要翻译： 已经开发了将甲烷氧化成甲醇的方法。 该方法包括在氧化条件下使包含甲烷，溶剂和氧化剂的气流与双金属催化剂接触以产生甲酯。 最后，将甲酯水解，得到甲醇产物流。 双金属催化剂包含至少两种过渡金属组分。 催化组分的一个实例是钴和锰的组合。
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公开(公告)号：US06368495B1
公开(公告)日：2002-04-09
申请号：US09689550
申请日：2000-10-12
IPC分类号： C10G2922
CPC分类号： C10G27/04
摘要： A novel process effective for the removal of organic sulfur compounds from liquid hydrocarbons is disclosed. The process more specifically addresses the removal of thiophenes and thiophene derivatives from a number of petroleum fractions, including gasoline, diesel fuel, and kerosene. In the first step of the process, the liquid hydrocarbon is subjected to oxidation conditions in order to oxidize at least some of the thiophene compounds to sulfones. Then, these sulfones can be catalytically decomposed to hydrocarbons (e.g. hydroxybiphenyl) and volatile sulfur compounds (e.g. sulfur dioxide). The hydrocarbon decomposition products remain in the treated liquid as valuable blending components, while the volatile sulfur compounds are easily separable from the treated liquid using well-known techniques such as flash vaporization or distillation.
摘要翻译： 公开了一种有效从液态烃中除去有机硫化合物的新方法。 该方法更具体地涉及从许多石油馏分（包括汽油，柴油燃料和煤油）中除去噻吩和噻吩衍生物。 在该方法的第一步中，液态烃经受氧化条件以使至少一些噻吩化合物氧化成砜。 然后，这些砜可以催化分解成烃类（如羟基联苯）和挥发性硫化合物（如二氧化硫）。 烃分解产物保留在经处理的液体中作为有价值的共混组分，而使用众所周知的技术，例如闪蒸或蒸馏，挥发性硫化合物容易与处理液体分离。
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46.发明授权
公开(公告)号：US5888927A
公开(公告)日：1999-03-30
申请号：US889809
申请日：1997-07-08
申请人： Beth McCulloch , Timothy A. Brandvold , Peter K. Nickl , Jennifer S. Holmgren , Joseph J. Alcaraz
发明人： Beth McCulloch , Timothy A. Brandvold , Peter K. Nickl , Jennifer S. Holmgren , Joseph J. Alcaraz
CPC分类号： B01J20/103 , B01D15/3833 , B01J20/28057 , B01J20/2809 , B01J20/286 , B01J20/29 , B01J20/3204 , Y10S502/507 , Y10T428/2991 , Y10T428/2998
摘要： Chiral stationary phases perform well when the underlying support for the chiral organic material is coated onto a silica pore widened by a hydrothermal treatment. The resulting silica is amorphous with a unimodal distribution of large pores. A variety of chiral stationary phases perform well and are distinguished, inter alia, by the treatment, if any, prior to coating the chiral organic material.
摘要翻译： 当将手性有机材料的底层载体涂覆到通过水热处理加宽的二氧化硅孔上时，手性固定相表现良好。 所得的二氧化硅是具有单峰分布的大孔的无定形的。 各种手性固定相表现良好，特别是通过在涂覆手性有机材料之前的处理（如果有的话）来区分。
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47.发明授权Acid functionalized organically-bridged polysilsesquioxanes as catalysts for acid catalyzed reactions 失效酸官能化有机桥连聚倍半硅氧烷作为酸催化反应的催化剂
公开(公告)号：US5475162A
公开(公告)日：1995-12-12
申请号：US277554
申请日：1994-07-19
IPC分类号： C08G77/52 , C07C29/04 , C07C41/06 , C07C45/45 , C07C49/203
CPC分类号： C08G77/52
摘要： A process of effecting an acid catalyzed reaction wherein a reactant capable of undergoing an acid catalyzed reaction is contacted with an acid functionalized organically-bridged polysilsesquioxane catalyst where all of the acid functionality is covalently bonded to the organic portion of an organically-bridged polysilsesquioxane framework has been developed. The acid functionalized organically-bridged polysilsesquioxane is formed by polymerizing a monomer through sol-gel processing to form an organically-bridged polysilsesquioxane, reacting an acid group onto the organic portion of the organically-bridged polysilsesquioxane, and recovering the acid functionalized product. An embodiment of the invention is where the acid catalyzed reaction is the hydration of olefins, alkylation, acylation, isomerization, or aldol condensation/elimination. A specific embodiment of the invention is effecting the aldol condensation/elimination reaction of acetone with itself to form mesityl oxide by contacting the acetone with an effective amount of sulfonated phenylene-bridged polysilsesquioxane.
摘要翻译： 实现酸催化反应的方法，其中能够进行酸催化反应的反应物与酸官能化的有机桥连聚倍半硅氧烷催化剂接触，其中所有的酸官能团共价键合到有机桥连的聚倍半硅氧烷骨架的有机部分， 已经开发 酸官能化有机桥连聚倍半硅氧烷是通过溶胶 - 凝胶加工聚合单体形成有机桥连聚倍半硅氧烷，使酸基与有机桥连聚倍半硅氧烷的有机部分反应，并回收酸官能化产物形成的。 本发明的一个实施方案是酸催化反应是烯烃的水合，烷基化，酰化，异构化或醛醇缩合/消除。 本发明的一个具体实施方案是通过使丙酮与有效量的磺化亚苯基桥连聚倍半硅氧烷接触来实现丙酮与其自身的醛醇缩合/消除反应以形成三甲氧基。
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48.发明授权Processes for washing a spent ion exchange bed and for treating biomass-derived pyrolysis oil, and apparatuses for treating biomass-derived pyrolysis oil 有权用于洗涤废离子交换床和处理生物质衍生的热解油的方法，以及用于处理生物质衍生的热解油的装置公开(公告)号：US09192931B2
公开(公告)日：2015-11-24
申请号：US13436648
申请日：2012-03-30
CPC分类号： B01J39/043 , B01J39/05 , B01J39/20 , B01J49/06 , B01J49/53 , B01J49/60 , C10B53/02 , C10G1/002 , C10G3/50 , C10G25/05 , C10G25/12 , Y02E50/14 , Y02P20/145 , Y02P30/20
摘要： Processes and apparatuses for washing a spent ion exchange bed and for treating biomass-derived pyrolysis oil are provided herein. An exemplary process for washing a spent ion exchange bed employed in purification of biomass-derived pyrolysis oil includes the step of providing a ion-depleted pyrolysis oil stream having an original oxygen content. The ion-depleted pyrolysis oil stream is partially hydrotreated to reduce the oxygen content thereof, thereby producing a partially hydrotreated pyrolysis oil stream having a residual oxygen content that is less than the original oxygen content. At least a portion of the partially hydrotreated pyrolysis oil stream is passed through the spent ion exchange bed. Water is passed through the spent ion exchange bed after passing at least the portion of the partially hydrotreated pyrolysis oil stream therethrough.
摘要翻译： 本文提供了用于洗涤废离子交换床和处理生物质衍生的热解油的方法和设备。 用于净化生物质衍生的热解油所用的废离子交换床的示例性方法包括提供具有原始氧含量的离子贫化裂解油流的步骤。 部分加氢处理离子贫化热解油料流以降低其氧含量，由此产生部分加氢处理的裂解油料流，其残余氧含量小于原始氧含量。 部分加氢处理的热解油流中的至少一部分通过废离子交换床。 在通过部分加氢处理的热解油流的至少一部分之后，水通过废离子交换床。
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49.发明授权公开(公告)号：US09163181B2
公开(公告)日：2015-10-20
申请号：US13528475
申请日：2012-06-20
CPC分类号： C10G3/42 , C10G3/40 , C10G3/50 , C10G3/52 , C10G45/02 , C10G69/06 , C10G2300/1011 , Y02P30/20
摘要： Embodiments of methods and apparatuses for deoxygenating a biomass-derived pyrolysis oil are provided. In one example, a method comprises the steps of separating a low-oxygen biomass-derived pyrolysis oil effluent into a low-oxygen-pyoil organic phase stream and an aqueous phase stream. Phenolic compounds are removed from the aqueous phase stream to form a phenolic-rich diluent recycle stream. A biomass-derived pyrolysis oil stream is diluted and heated with the phenolic-rich diluent recycle stream to form a heated diluted pyoil feed stream. The heated diluted pyoil feed stream is contacted with a deoxygenating catalyst in the presence of hydrogen to deoxygenate the heated diluted pyoil feed stream.
摘要翻译： 提供了用于脱氧生物质衍生的裂解油的方法和装置的实施方案。 在一个实例中，方法包括以下步骤：将低氧生物质衍生的热解油流出物分离成低氧 - 有机相物流和水相物流。 从水相流中除去酚类化合物以形成富含酚的稀释剂再循环流。 将生物质衍生的热解油流稀释并用富含酚的稀释剂再循环流加热以形成加热的稀释的原料流。 将加热的稀释的原料流与脱氧催化剂在氢存在下接触以对加热的稀释的原料流进行脱氧。
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公开(公告)号：US09080109B2
公开(公告)日：2015-07-14
申请号：US13326059
申请日：2011-12-14
申请人： Timothy A. Brandvold
发明人： Timothy A. Brandvold
CPC分类号： C10G3/42 , C10G3/45 , C10G3/50 , C10G2300/1011 , C10G2300/44 , C10G2300/802 , Y02E50/14 , Y02P30/20
摘要： Methods for deoxygenating a biomass-derived pyrolysis oil are provided. A method comprising the steps of diluting the biomass-derived pyrolysis oil with a phenolic-containing diluent to form a diluted pyoil-phenolic feed is provided. The diluted pyoil-phenolic feed is contacted with a deoxygenating catalyst in the presence of hydrogen at hydroprocessing conditions effective to form a low-oxygen biomass-derived pyrolysis oil effluent.
摘要翻译： 提供了用于脱氧生物质的热解油的方法。 提供了一种方法，其包括用含酚的稀释剂稀释生物质衍生的热解油以形成稀释的酚 - 酚进料的步骤。 在有效形成低氧生物质衍生的裂解油流出物的加氢处理条件下，将稀释的酚 - 酚进料与脱氧催化剂在氢的存在下接触。
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