Continuous countercurrent extraction process for removing water-soluble
impurities from water immiscible polymer solutions
    42.
    发明授权
    Continuous countercurrent extraction process for removing water-soluble impurities from water immiscible polymer solutions 失效
    连续逆流提取方法,用于从水不混溶的聚合物溶液中除去水溶性杂质

    公开(公告)号:US4360662A

    公开(公告)日:1982-11-23

    申请号:US208201

    申请日:1980-11-19

    CPC classification number: C08G63/90

    Abstract: There is disclosed a continuous countercurrent extraction process for removing tertiary amine hydrochloride impurities which are soluble in water from a water immiscible polymer solution of a halogenated aromatic polyester which has a viscosity of at least about 10 poise and a density greater than about 1.0 gm/cc. This process comprises (a) introducing the polymer solution at the top of an extraction column and introducing water at the bottom of the column to form a two phase mixture, and (b) mechanically agitating the mixture in a particularly defined manner in order to extract the water-soluble impurities from the polymer solution and economically recover the tertiary amine hydrochloride.

    Abstract translation: 公开了一种连续逆流提取方法,用于从卤代芳族聚酯的水不混溶性聚合物溶液中除去可溶于水的叔胺盐酸盐杂质,其具有至少约10泊的粘度和大于约1.0gm / cc的密度 。 该方法包括(a)将聚合物溶液引入萃取塔的顶部并在塔底引入水以形成两相混合物,和(b)以特别限定的方式机械搅拌该混合物以提取 来自聚合物溶液的水溶性杂质经济地回收盐酸叔胺。

    Process for recovery of polyol fatty acid polyesters
    43.
    发明授权
    Process for recovery of polyol fatty acid polyesters 失效
    多元醇脂肪酸聚酯的回收方法

    公开(公告)号:US4334061A

    公开(公告)日:1982-06-08

    申请号:US89145

    申请日:1979-10-29

    CPC classification number: C07H13/06 C08G63/90

    Abstract: A process for recovering polyol fatty acid polyesters from the crude reaction product in which it is produced by contacting with an aqueous washing medium in the presence of an emulsion decreasing organic solvent so that the alkali metal fatty acid soaps and the color-forming bodies are taken into the aqueous phase, and upon settling the phases are separated from each other.

    Abstract translation: 从粗反应产物中回收多元醇脂肪酸聚酯的方法,其中通过在降低有机溶剂的乳液存在下与含水洗涤介质接触来制备多元醇脂肪酸聚酯,从而使碱金属脂肪酸皂和成色体被带走 进入水相,并且在沉降时,相分离。

    Method for producing acid-decomposable polymer

    公开(公告)号:US11725078B2

    公开(公告)日:2023-08-15

    申请号:US16893577

    申请日:2020-06-05

    CPC classification number: C08G63/90 B01J39/05 C08G63/66 G03F7/0045 G03F7/0392

    Abstract: [Problem to be Solved]
    To Provide a method for producing an acid-decomposable polymer having a reduced metal ion content, which suppresses decomposition and deprotection of the acid-decomposable polymer.
    [Means to Solve the Problem]
    The method for producing an acid-decomposable polymer according to the present invention comprises the steps of:



    preparing a polymer solution comprising an acid-decomposable polymer;
    washing an acidic cation exchanger with an organic solvent until the water content in the organic solvent discharged from the acidic cation exchanger falls to 400 ppm or less; and
    passing the polymer solution through the washed acidic cation exchanger to reduce the metal ion content of the polymer.

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