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    Polymerizable compositions with acylgermanium compounds
    51.
    发明授权
    Polymerizable compositions with acylgermanium compounds 有权
    具有酰基锗化合物的可聚合组合物

    公开(公告)号：US07605190B2

    公开(公告)日：2009-10-20

    申请号：US11902865

    申请日：2007-09-26

    Applicant: Norbert Moszner ,  Ulrich Salz ,  Urs Karl Fischer ,  Robert Liska ,  Heinrich Gruber ,  Beate Ganster

    Inventor： Norbert Moszner ,  Ulrich Salz ,  Urs Karl Fischer ,  Robert Liska ,  Heinrich Gruber ,  Beate Ganster

    IPC: A61C13/00 ,  A61C13/225 ,  A61K6/00 ,  C08F2/50 ,  C08J3/28

    CPC classification number: C08F2/50 ,  A61K6/083 ,  C08F4/72 ,  Y10S522/908 ,  C08L33/00

    Abstract: Composition with at least one polymerizable binder and at least one polymerization initiator, which contains at least one acylgermanium compound according to general Formula (I), in which R0 is a substituted or unsubstituted C1-18-alkyl radical or an acyl group; R1 and R2 are H, an acyl group or have one of the meanings given for R3; R3 is a branched or linear C1-18-alkyl radical which can be unsubstituted or substituted one or more times by —O—, —NH—, —NR—, —S— or interrupted by other groups, trimethylsilyl, hal-(CH3)2Si—[OSi(CH3)2]r−, (CH3)3Si—[OSi(CH3)2]r—, —COOH, —COO—R10, —CO—NR11R12, —CO-vinyl, —CO-phenyl, phenyl-C1-4-alkyl, phenyl, naphthyl or biphenyl, C5-12 cycloalkyl, a 5 or 6-membered O, S or N-containing heterocyclic ring, halogen, OH, an aromatic C6-30 radical which can be substituted or unsubstituted and/or interrupted by O, S or —NR—, or a branched, cyclic or linear C1-20 alkyl, -alkenyl, -alkoxy or -alkenoxy radical; m is 1, 2 or 3; n is 0 or 1 and p is 0 or 1; wherein in each case two of the radicals R0, R1, R2 or R3 can be connected to each other accompanied by the formulation of a 5 to 8 member ring; and the use of acylegermanium compounds of Formula (I), for example, as initiator for radical polymerization.

    Abstract translation: 含有至少一种可聚合粘合剂和至少一种聚合引发剂的组合物，其含有至少一种根据通式（I）的酰基锗化合物，其中R 0是取代或未取代的C 1-18 - 烷基或酰基; R 1和R 2是H，酰基或具有R 3给出的含义之一; R3是支链或直链的C1-18 - 烷基，其可以是未取代的或被-O - ， - NH - ， - NR - ， - S-取代或被其它基团间隔的一个或多个，三甲基甲硅烷基，hal-（CH 3 ）2Si- [OSi（CH 3）2] r - ，（CH 3）3 Si- [OSi（CH 3）2] r - ，-COOH，-COO-R 10，-CO-NR 11 R 12，-CO-乙烯基， 苯基，C 1-4 - 烷基，苯基，萘基或联苯基，C 5-12环烷基，5或6元O，S或N的杂环，卤素，OH，可被取代的芳族C 6-30基团 或未取代和/或被O，S或-NR-或支链，环状或直链的C 1-20烷基， - 烯基， - 烷氧基或 - m为1,2或3; n为0或1，p为0或1; 其中在每种情况下，基团R 0，R 1，R 2或R 3中的两个可以相互连接，伴随着5-8元环的配制; 以及使用式（I）的乙烯基锗化合物，例如作为自由基聚合的引发剂。

    Dental materials with unusual fluorine distribution
    52.
    发明授权
    Dental materials with unusual fluorine distribution 有权
    具有不寻常氟分布的牙科材料

    公开(公告)号：US07595354B2

    公开(公告)日：2009-09-29

    申请号：US11338034

    申请日：2006-01-24

    Applicant: Norbert Moszner ,  Urs Karl Fischer ,  Volker M Rheinberger ,  Giancarlo Galli ,  Marina Ragnoli ,  Emo Chiellini

    Inventor： Norbert Moszner ,  Urs Karl Fischer ,  Volker M Rheinberger ,  Giancarlo Galli ,  Marina Ragnoli ,  Emo Chiellini

    IPC: A61C5/04 ,  A61K6/083 ,  C08F12/20 ,  C08F232/04

    CPC classification number: A61K6/083 ,  A61K6/0017 ,  A61K6/0023 ,  C08L33/00 ,  C08L25/00

    Abstract: A composition comprising (A) at least one fluorinated vinylcyclopropane according to Formula (I) wherein R1 is H or —CO—O—(CH2CH2)p—R7; R2 is H or forms together with R6 a —CH2—C(R9)(R10)—CH2— residue; R3 is H; R4 is H or forms together with R5—CH2—C(R9)(R10)—CH2— residue; R5 is H, —CO—O—R8, —CO—O—(CH2CH2)p—R7 or forms together with R4—CH2—C(R9)(R10)—CH2— residue; R6 is H, —CO—O—R8, —CO—O—(CH2CH2)p—R7 or forms together with R2 a —CH2—C(R9)(R10)—CH2— residue; R7 is perfluorinated C2-C20 aliphatic or alicyclic group; R8 is H, phenyl, benzyl, or a linear or branched C1-C12 aliphatic or alicyclic group; R9 is a H, benzoyl, acetyl or a C1-C5-alkyl group; R10H or a —CO—O—R8; p is 1, 2, 3, or 4, provided that the compound of Formula (I) comprises at least one —CO—O—(CH2CH2)p—R7 residue; (B) at least one non-fluorinated vinylcyclopropane derivative; (C) a bisphenol-A-ether di(meth)acrylate according to Formula (II) wherein R18 is H or CH3, R19 is CH3 or CF3, Y is a C2-C5-alkylen residue which can be substituted by an OH group or is preferably unsubstituted.

    Abstract translation: 一种组合物，其包含（A）至少一种根据式（I）的氟化乙烯基环丙烷，其中R 1是H或-CO-O-（CH 2 CH 2）p -R 7; R2是H或与R6一起形成-CH 2 -C（R 9）（R 10）-CH 2 - 残基; R3为H; R4是H或与R5-CH2-C（R9）（R10）-CH2-残基一起形成; R5是H，-CO-O-R8，-CO-O-（CH2CH2）p-R7或与R4-CH2-C（R9）（R10）-CH2-残基一起形成; R6是H，-CO-O-R8，-CO-O-（CH2CH2）p-R7或与R2一起形成-CH2-C（R9）（R10）-CH2-残基; R7是全氟化C 2 -C 20脂族或脂环基; R8是H，苯基，苄基或直链或支链C 1 -C 12脂族或脂环基; R9是H，苯甲酰基，乙酰基或C1-C5-烷基; R10H或-CO-O-R8; p为1,2,3或4，条件是式（I）化合物包含至少一个-CO-O-（CH 2 CH 2）p-R 7残基; （B）至少一种非氟化乙烯基环丙烷衍生物; （C）式（II）的双酚A - 醚二（甲基）丙烯酸酯，其中R18为H或CH3，R19为CH3或CF3，Y为可被OH基取代的C2-C5-亚烷基基团 或优选未被取代。

    DENTAL MATERIALS WITH SURFACE-FUNCTIONALIZED FILLERS
    53.
    发明申请
    DENTAL MATERIALS WITH SURFACE-FUNCTIONALIZED FILLERS 审中-公开
    具有表面官能化填料的牙科材料

    公开(公告)号：US20090186960A1

    公开(公告)日：2009-07-23

    申请号：US12275700

    申请日：2008-11-21

    Applicant: Norbert MOSZNER ,  Jorg ANGERMANN ,  Simone KLAPDOHR

    Inventor： Norbert MOSZNER ,  Jorg ANGERMANN ,  Simone KLAPDOHR

    IPC: A61K6/093 ,  C08G77/14 ,  C07F5/06 ,  C07F7/18 ,  C07F5/00

    CPC classification number: A61K6/0008 ,  A61K6/0017 ,  A61K6/0023 ,  A61K6/0088 ,  A61K6/093 ,  C08L83/10

    Abstract: The invention relates to a polymerizable composition which is characterized in that it contains at least one filler that is surface-functionalized with groups of formula (I), wherein groups of formula (I) (A)a-Z-Y—R2—SiR13−m—(O—)m   (I), are bonded to the filler via at least one oxygen atom that is bound to the silicon atom of the group of formula (I). The invention also relates to a process for the preparation of the composition according to the invention and its use in particular as a dental material.

    Abstract translation: 本发明涉及一种可聚合组合物，其特征在于其含有至少一种用式（I）的基团表面官能化的填料，其中式（I）的基团<？在线公式描述=“In- （A）aZY-R2-SiR13-m-（O-）m（I），<？在线公式描述=“在线公式”end =“tail” α'通过与式（I）的基团的硅原子结合的至少一个氧原子键合到填料上。 本发明还涉及制备根据本发明的组合物及其用途，特别是牙科材料的方法。

    Dental materials based on multicyclic allyl sulphides
    54.
    发明授权
    Dental materials based on multicyclic allyl sulphides 有权
    基于多环烯丙基硫化物的牙科材料

    公开(公告)号：US07501457B2

    公开(公告)日：2009-03-10

    申请号：US11482164

    申请日：2006-07-07

    Applicant: Jörg Angermann ,  Peter Burtscher ,  Urs Karl Fischer ,  Norbert Moszner ,  Volker M. Rheinberger

    Inventor： Jörg Angermann ,  Peter Burtscher ,  Urs Karl Fischer ,  Norbert Moszner ,  Volker M. Rheinberger

    IPC: A61K6/083 ,  C08F28/06

    CPC classification number: A61K6/083 ,  A61K6/0017 ,  A61K6/0023 ,  C08L33/00

    Abstract: Dental materials and associated methods are described based on multicyclic allyl sulphides with general Formula (I): in which R1 is H or a C1-C10 alkyl radical; R2 is H or a C1-C10 alkyl radical; R3 is absent or is a C1-C20 alkylene radical which can be interrupted by O or S, a cycloaliphatic C4-C12 radical, a bicyclic C6-C12 radical, a C6-C14 arylene or C7-C20 alkylene arylene radical; R4 is an n-times substituted aliphatic C2 to C20 hydrocarbon radical which can be interrupted by O or S, a cycloaliphatic C4-C12 radical, an aromatic C6-C14 radical, an aliphatic-aromatic C7-C20 radical or a heterocyclic radical which can contain 4 to 20 carbon atoms and 1 to 6 heteroatoms which are selected from N, O, P and/or S atoms, or which is formed exclusively by these heteroatoms; R5 is absent or is a C1-C10 alkylene radical; X is absent or is O, S, —O—CO— or —O—CO—NH—; Y is absent or is O, S, —O—CO— or —O—CO—NH—; m is 0 or 1 and n is an integer from 3 to 6.

    Abstract translation: 基于具有通式（I）的多环烯丙基硫化物描述牙科材料和相关方法：其中R1是H或C1-C10烷基; R2是H或C1-C10烷基; R3不存在或是可被O或S间隔的C 1 -C 20亚烷基，脂环族C 4 -C 12基，双环C 6 -C 12基，C 6 -C 14亚芳基或C 7 -C 20亚烷基亚芳基; R4是可被O或S间隔的n次取代的脂族C 2 -C 20烃基，脂环族C 4 -C 12基团，芳族C 6 -C 14基团，脂族 - 芳族C 7 -C 20基团或杂环基团，其可以 含有4至20个碳原子和1至6个选自N，O，P和/或S原子的杂原子，或仅由这些杂原子形成的杂原子; R5不存在或是C1-C10亚烷基; X不存在或为O，S，-O-CO-或-O-CO-NH-; Y不存在或为O，S，-O-CO-或-O-CO-NH-; m为0或1，n为3至6的整数。

    Dental Materials Containing Hydrophobic Nanoparticulate Silicic Acid Co-Condensates and Use Thereof
    55.
    发明申请
    Dental Materials Containing Hydrophobic Nanoparticulate Silicic Acid Co-Condensates and Use Thereof 有权
    含疏水性纳米微粒硅酸共冷凝物及其用途的牙科材料

    公开(公告)号：US20090043004A1

    公开(公告)日：2009-02-12

    申请号：US12226129

    申请日：2007-03-27

    Applicant: Norbert Moszner ,  Volker Rheinberger ,  Simone Klapdohr ,  Urs Karl Fischer

    Inventor： Norbert Moszner ,  Volker Rheinberger ,  Simone Klapdohr ,  Urs Karl Fischer

    IPC: A61K8/72 ,  C08F230/08 ,  C08F283/12

    CPC classification number: A61K6/0005 ,  A61K6/0017 ,  A61K6/083 ,  C08G77/12 ,  C08G77/20 ,  C08L51/085

    Abstract: The present invention relates to dental materials comprising liquid, nanoparticulate functionalized hydrophobic co-condensates of tetraalkyl silicates with functionalized trialkoxysilanes of the formula I P—(CH2)n—Si(OR)3 where P, R and n independently of one another have the following meanings: P=a polymerizable CH2═CH—, CH2═CH—O—, styryl, (meth)acrylic or (meth)acrylamide group or an SH group capable of polyaddition, R=methyl, ethyl or propyl and n=from 3 to 15, which can be prepared by co-condensation of tetraalkyl silicates with alkyltrialkoxysilanes functionalized in the ω position and subsequent end group functionalization with trimethylsilyl groups; The invention further relates to the use of the dental materials for filling composites, fixing cements or materials for coatings.

    Abstract translation: 本发明涉及牙科材料，其包括液体，纳米颗粒官能化的四烷基硅酸盐的疏水性共缩合物与式I的官能化三烷氧基硅烷<？in-line-formula description =“In-line formula”end =“lead”→> P- （CH2）n-Si（OR）3 <？in-line-formula description =“In-line Formulas”end =“tail”？>其中P，R和n彼此独立地具有以下含义：P = a 可聚合的CH 2 -CH-，CH 2 -CH-O-，苯乙烯基，（甲基）丙烯酸或（甲基）丙烯酰胺基团或能够加成的SH基团，R =甲基，乙基或丙基，n = 3至15， 通过硅烷四烷基酯与在ω位置官能化的烷基三烷氧基硅烷的共缩合制备，随后用三甲基甲硅烷基进行末端官能化; 本发明还涉及牙科材料用于填充复合材料，固定水泥或涂层材料的用途。

    Dental materials based on multicyclic allyl sulphides
    56.
    发明申请
    Dental materials based on multicyclic allyl sulphides 有权
    基于多环烯丙基硫化物的牙科材料

    公开(公告)号：US20070203256A1

    公开(公告)日：2007-08-30

    申请号：US11482164

    申请日：2006-07-07

    Applicant: Jorg Angermann ,  Peter Burtscher ,  Urs Karl Fischer ,  Norbert Moszner ,  Volker M. Rheinberger

    Inventor： Jorg Angermann ,  Peter Burtscher ,  Urs Karl Fischer ,  Norbert Moszner ,  Volker M. Rheinberger

    IPC: A61K6/08

    CPC classification number: A61K6/083 ,  A61K6/0017 ,  A61K6/0023 ,  C08L33/00

    Abstract: Dental materials and associated methods are described based on multicyclic allyl sulphides with general Formula (I): in which R1 is H or a C1-C10 alkyl radical; R2 is H or a C1-C10 alkyl radical; R3 is absent or is a C1-C20 alkylene radical which can be interrupted by O or S, a cycloaliphatic C4-C12 radical, a bicyclic C6-C12 radical, a C6-C14 arylene or C7-C20 alkylene arylene radical; R4 is an n-times substituted aliphatic C2 to C20 hydrocarbon radical which can be interrupted by O or S, a cycloaliphatic C4-C12 radical, an aromatic C6-C14 radical, an aliphatic-aromatic C7-C20 radical or a heterocyclic radical which can contain 4 to 20 carbon atoms and 1 to 6 heteroatoms which are selected from N, O, P and/or S atoms, or which is formed exclusively by these heteroatoms; R5 is absent or is a C1-C10 alkylene radical; X is absent or is O, S, —O—CO— or —O—CO—NH—; Y is absent or is O, S, —O—CO— or —O—CO—NH—; m is 0 or 1 and n is an integer from 3 to 6.

    Abstract translation: 牙科材料和相关方法基于通式（I）的多环烯丙基硫化物来描述：其中R 1是H或C 1 -C 10烷基， 烷基; R 2是H或C 1 -C 10烷基; R 3不存在或是可以被O或S中断的C 1 -C 20亚烷基，脂环族C 1 -C 20烷基， 4个-C 12 - 基团，双环C 6 -C 12 - 基团，C 6 - -C 14亚芳基或C 7 -C 20亚烷基亚芳基; R 4是可以被O或S间隔的n 20取代的C 20烃基C 2〜C 20烃基， 芳族C 6 -C 14 - 基团，脂族 - 芳族C 1 -C 12烷基，芳基C 6 -C 14 - 或者可以含有4至20个碳原子和1至6个选自N，O，P和/或S原子的杂原子的杂环基团，或其中 完全由这些杂原子形成; R 5不存在或者是C 1 -C 10亚烷基; X不存在或为O，S，-O-CO-或-O-CO-NH-; Y不存在或为O，S，-O-CO-或-O-CO-NH-; m为0或1，n为3至6的整数。

    Dental material based on polymerizable waxes
    60.
    发明授权
    Dental material based on polymerizable waxes 失效
    基于可聚合蜡的牙科材料

    公开(公告)号：US06057383A

    公开(公告)日：2000-05-02

    申请号：US878050

    申请日：1997-06-18

    Applicant: Thomas Volkel ,  Gerhard Zanghellini ,  Karl Fischer ,  Norbert Moszner ,  Volker Rheinberger

    Inventor： Thomas Volkel ,  Gerhard Zanghellini ,  Karl Fischer ,  Norbert Moszner ,  Volker Rheinberger

    IPC: A61K6/083 ,  A61K6/00 ,  C08L33/06

    CPC classification number: A61K6/083

    Abstract: The invention relates to dental materials based on wax-like polymerizable substances. The dental materials contain (a) 0 to 70 wt. % of at least one polymerizable monomer and/or oligomer; (b) 0.1 to 5 wt. % of at least one polymerization initiator; (c) 0 to 60 wt. % of one or more fillers, (d) at least 20 wt. % of the wax-like polymerizable substance. They can be kneaded at room temperature and can be modelled in non-polymerized state without additional heating, like conventional waxes. On polymerization, the wax component is covalently incorporated into the polymer. The dental materials are suitable for producing temporary and permanent dental prostheses.

    Abstract translation: 本发明涉及基于蜡状聚合物质的牙科用材料。 牙科材料含有（a）0〜70重量％ ％的至少一种可聚合单体和/或低聚物; （b）0.1〜5wt。 ％的至少一种聚合引发剂; （c）0至60wt。 ％的一种或多种填料，（d）至少20wt。 ％的蜡状聚合物质。 它们可以在室温下捏合并且可以在非聚合状态下进行建模而无需额外加热，如常规蜡。 在聚合时，蜡组分共价掺入聚合物中。 牙科材料适用于生产临时和永久的牙科假体。

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