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    Blocked polyisocyanates containing amide/imide groups and their use in stoving lacquers
    52.
    发明授权
    Blocked polyisocyanates containing amide/imide groups and their use in stoving lacquers 失效
    含有酰胺/酰亚胺基团的封闭多异氰酸酯及其在烘烤漆中的应用

    公开(公告)号：US5883216A

    公开(公告)日：1999-03-16

    申请号：US671282

    申请日：1996-06-27

    Applicant: Reinhard Halpaap ,  Hans Schlegel ,  Jan Mazanek ,  Hans-Ulrich Meier-Westhues

    Inventor： Reinhard Halpaap ,  Hans Schlegel ,  Jan Mazanek ,  Hans-Ulrich Meier-Westhues

    IPC: C08G18/34 ,  C08G18/65 ,  C08G18/80 ,  C09D5/25 ,  C09D175/00 ,  C09D175/04 ,  H01B3/30 ,  C08G18/40 ,  C07C230/00

    CPC classification number: H01B3/30 ,  C08G18/8009 ,  C08G18/8048 ,  C08G18/8061

    Abstract: The present invention relates to polyisocyanates containingi) 0.5 to 10 wt. % of amide and/or imide structural units (calculated as --CO--N.dbd., MW=42),ii) 5 to 20 wt. % of isocyanate groups (calculated as --NCO, MW=42) blocked with blocking agents which are monofunctional in the context of the isocyanate addition reaction andiii) 0 to 30 wt. % of chemically incorporated urethane groups (calculated as --NH--CO--O--, MW=59) obtained from the reaction of isocyanate groups with the hydroxyl groups of organic polyhydroxyl compounds.The present invention also relates to a process for the production of these lacquer polyisocyanates, their use as a binder for stoving lacquers optionally in combination with organic polyhydroxyl compounds and to their use as a binder component containing free hydroxyl groups and optionally blocked isocyanate groups by reacting and/or blending the polyisocyanates with organic polyhydroxyl compounds having a molecular weight of 62 to 350.

    Abstract translation: 本发明涉及含有i）0.5〜10wt。 酰胺和/或酰亚胺结构单元的％（以-CO-N =，MW = 42计算），ii）5至20重量％ 异氰酸酯基团的％（以-NCO，MW = 42计算）用在异氰酸酯加成反应的上下文中是单官能的封闭剂封闭，和iii）0-30wt。 由异氰酸酯基与有机多羟基化合物的羟基的反应获得的化学引入的氨基甲酸酯基团的％（以-NH-CO-O-，MW = 59计算）。 本发明还涉及生产这些漆多异氰酸酯的方法，它们作为用于烘烤漆的粘合剂的用途，任选地与有机多羟基化合物组合，以及它们作为含有游离羟基和任选的封端异氰酸酯基团的粘合剂组分的用途，通过使 和/或将多异氰酸酯与分子量为62〜350的有机多羟基化合物混合。

    Tertiary polyisocyanate derivatives
    54.
    发明授权
    Tertiary polyisocyanate derivatives 失效
    三元多异氰酸酯衍生物

    公开(公告)号：US4748242A

    公开(公告)日：1988-05-31

    申请号：US930584

    申请日：1986-11-12

    Applicant: Reinhard Halpaap ,  Josef Pedain ,  Hans-Joachim Kreuder ,  Gerhard Klein ,  Dieter Arlt

    Inventor： Reinhard Halpaap ,  Josef Pedain ,  Hans-Joachim Kreuder ,  Gerhard Klein ,  Dieter Arlt

    IPC: C08G18/00 ,  C08G18/02 ,  C08G18/06 ,  C08G18/79 ,  C08G63/52 ,  C07D251/30 ,  C07D251/32

    CPC classification number: C08G18/792 ,  C08G2150/20

    Abstract: The present invention is directed to a process for the production of polyisocyanates containing isocyanurate groups by trimerizing a mixture of aliphatic-cycloaliphatic diisocyanates having a sterically unhindered isocyanate group bound to a primary aliphatic carbon atom and a sterically hindered isocyanate group bound to a tertiary carbon atom which forms a part of a cycloaliphatic ring system and 1,6-diisocyanatohexane. The present invention is also directed to the polyisocyanates containing isocyanurate groups produced according to this process and to their use, optionally in blocked form, as an isocyanate component in the production of polyisocyanate polyaddition products, preferably polyurethane lacquers.

    Abstract translation: 本发明涉及一种制备含有异氰脲酸酯基团的多异氰酸酯的方法，该方法是将具有与伯脂肪族碳原子结合的空间上不受阻碍的异氰酸酯基团和与叔碳原子结合的位阻异氰酸酯基团的脂族 - 脂环族二异氰酸酯的混合物三聚 其形成脂环族环系的一部分和1,6-二异氰酸根合己烷。 本发明还涉及根据该方法制备的含有异氰脲酸酯基团的多异氰酸酯基团，以及它们在多异氰酸酯加聚产物（优选聚氨酯漆）生产中作为异氰酸酯组分的用途，任选地以封闭形式使用。

    Process for the production of combinations of organic polyisocyanates and at least partly blocked polyamines, the combinations obtainable by this process and their use for the production of lacquers, coating or sealing compositions
    55.
    发明授权
    Process for the production of combinations of organic polyisocyanates and at least partly blocked polyamines, the combinations obtainable by this process and their use for the production of lacquers, coating or sealing compositions 失效
    用于生产有机多异氰酸酯和至少部分封闭的多胺的组合的方法，可通过该方法获得的组合及其用于生产漆，涂料或密封组合物的用途

    公开(公告)号：US4481345A

    公开(公告)日：1984-11-06

    申请号：US583918

    申请日：1984-02-27

    Applicant: Klaus Nachtkamp ,  Manfred Bock ,  Reinhard Halpaap ,  Josef Pedain

    Inventor： Klaus Nachtkamp ,  Manfred Bock ,  Reinhard Halpaap ,  Josef Pedain

    IPC: C09K3/10 ,  C08G18/10 ,  C08G18/32 ,  C08G18/65 ,  C09D175/00 ,  C09D175/02 ,  C09D175/04 ,  C08G18/38

    CPC classification number: C08G18/3256 ,  C08G18/10

    Abstract: Process for the production of water-hardenable compositions of organic polyisocyanates and polyamines containing at least partly blocked amino groups present as ketimines, the combinations essentially representing mixtures and optionally reaction products containing urea groups by mixing the organic polyisocyanates with the polyamines in such quantities that the equivalent ratio of isocyanate groups to blocked and free amino groups is between about 0.9:1 and 4:1 and reacting any free amino groups present with some of the isocyanate groups in the polyisocyanate to form ureas, characterized in that the polyamines containing at least partly blocked amino groups used are mixtures comprising(a) from about 50 to 95 amine equivalent percent of organic compounds which are free from primary and secondary amino groups and which contain at least two ketimine groups corresponding to the following formula ##STR1## in which R.sup.1 represents an alkyl or cycloalkyl radical and R.sup.2 represents hydrogen or an alkyl or cycloalkyl radical or in which R.sup.1 and R.sup.2 form a cycloaliphatic hydrocarbon radical together with the two carbon atoms of the ketimine group and(b) from about 5 to 40 amine equivalent percent of organic compounds which are free from primary and secondary amino groups and which contain at least two ketimine groups of which one corresponds to the formula ##STR2## in which R.sup.1 and R.sup.2 are as defined above, the other ketimine group(s) present correspond(s) to the formula shown in (a).

    Abstract translation: 用于生产有机多异氰酸酯和含有至少部分封闭的胺基的多胺的水可硬化组合物作为酮亚胺存在的方法，所述组合基本上代表混合物和任选的含有尿素基团的反应产物，通过将有机多异氰酸酯与多胺混合， 异氰酸酯基与封端和游离氨基的当量比为约0.9:1至4:1，并使与多异氰酸酯中存在的一些异氰酸酯基团存在的任何游离氨基反应形成脲，其特征在于，含有至少部分 使用的封闭氨基是包含（a）约50至95胺当量百分比的不含伯和仲氨基并且含有至少两个对应于下式的酮亚胺基的有机化合物的混合物：其中R 1表示 烷基或环烷基，R 2表示氢或a n烷基或环烷基，或其中R1和R2与酮亚胺基团的两个碳原子一起形成脂环族烃基，和（b）约5至40胺当量百分比的不含伯和仲氨基的有机化合物 并且其包含至少两个酮亚胺基，其中一个对应于式（Ia）其中R 1和R 2如上所定义的式“IMAGE”，其它酮亚胺基与（a）所示的式表示。

    Preparation of polyisocyanates containing uretdione groups using phosphine catalysts
    58.
    发明申请
    Preparation of polyisocyanates containing uretdione groups using phosphine catalysts 有权
    使用磷化氢催化剂制备含有脲二酮基团的多异氰酸酯

    公开(公告)号：US20080262262A1

    公开(公告)日：2008-10-23

    申请号：US12082803

    申请日：2008-04-14

    Applicant: Frank Richter ,  Reinhard Halpaap

    Inventor： Frank Richter ,  Reinhard Halpaap

    IPC: C07C249/00

    CPC classification number: C07D229/00

    Abstract: The invention provides a process for isocyanate dimerization (uretdione formation) and a process for preparing polyisocyanates having a high content of uretdione groups, using specific phosphines as catalysts. The phosphines have one or two tertiary alkyl radicals bound directly to phosphorus.

    Abstract translation: 本发明提供异氰酸酯二聚（脲二酮形成）的方法以及使用特定的膦作为催化剂制备具有高含量脲二酮基团的多异氰酸酯的方法。 膦具有一个或两个直接与磷结合的叔烷基。

    Process for the preparation of polyaddition compounds
    59.
    发明申请
    Process for the preparation of polyaddition compounds 审中-公开
    制备加聚化合物的方法

    公开(公告)号：US20070142608A1

    公开(公告)日：2007-06-21

    申请号：US11638626

    申请日：2006-12-13

    Applicant: Hans Laas ,  Bernd Sojka ,  Michael Grahl ,  Josef Sanders ,  Wolfgang Fischer ,  Reinhard Halpaap

    Inventor： Hans Laas ,  Bernd Sojka ,  Michael Grahl ,  Josef Sanders ,  Wolfgang Fischer ,  Reinhard Halpaap

    IPC: C08G18/00

    CPC classification number: C08G18/798 ,  C08G18/0895 ,  C08G18/12 ,  C08G18/227 ,  C08G18/2825 ,  C08G18/4277 ,  C08G18/664 ,  C08G2150/20 ,  C08G18/42

    Abstract: The present invention relates to a novel process for the preparation of polyaddition products, to the products obtainable by this process and to their use as starting components in the production of polyurethane plastics. The process includes the reaction of A) polyisocyanates with uretdione groups having a mean isocyanate functionality of at least 2.0, optionally with the concomitant use of B) other diisocyanates and/or polyisocyanates, different from A, in an amount of up to 70 wt. %, based on the total weight of components A) and B), with C) polyols in the molecular weight range 62-2000 having a mean functionality of at least 2.0, or mixtures of polyols and optionally D) other isocyanate-reactive monofunctional compounds in an amount of up to 40 wt. %, based on the total weight of components C) and D). An equivalent ratio of isocyanate groups to isocyanate-reactive groups of 1.8:1 to 0.6:1 is maintained in the reactants, and the reaction is carried out in the presence of at least one bismuth-containing catalyst.

    Abstract translation: 本发明涉及一种制备加聚产物的新方法，可通过该方法获得的产品及其作为聚氨酯塑料生产中起始组分的用途。 该方法包括A）多异氰酸酯与平均异氰酸酯官能度至少为2.0的脲二酮基团的反应，任选地伴随使用B）与A不同的其它二异氰酸酯和/或多异氰酸酯，其量高达70wt。 基于组分A）和B）的总重量，C）分子量范围为62-2000的平均官能度至少为2.0的多元醇，或多元醇和任选的D）混合物的其它异氰酸酯反应性单官能化合物 其量可高达40wt。 ％，基于组分C）和D）的总重量。 在反应物中保持异氰酸酯基与异氰酸酯反应性基团的当量比为1.8:1至0.6:1，反应在至少一种含铋催化剂存在下进行。

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