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    Process for the production of combinations of organic polyisocyanates and at least partly blocked polyamines, the combinations obtainable by this process and their use for the production of lacquers, coating or sealing compositions
    1.
    发明授权
    Process for the production of combinations of organic polyisocyanates and at least partly blocked polyamines, the combinations obtainable by this process and their use for the production of lacquers, coating or sealing compositions 失效
    用于生产有机多异氰酸酯和至少部分封闭的多胺的组合的方法，可通过该方法获得的组合及其用于生产漆，涂料或密封组合物的用途

    公开(公告)号：US4481345A

    公开(公告)日：1984-11-06

    申请号：US583918

    申请日：1984-02-27

    申请人： Klaus Nachtkamp ,  Manfred Bock ,  Reinhard Halpaap ,  Josef Pedain

    发明人： Klaus Nachtkamp ,  Manfred Bock ,  Reinhard Halpaap ,  Josef Pedain

    IPC分类号： C09K3/10 ,  C08G18/10 ,  C08G18/32 ,  C08G18/65 ,  C09D175/00 ,  C09D175/02 ,  C09D175/04 ,  C08G18/38

    CPC分类号： C08G18/3256 ,  C08G18/10

    摘要： Process for the production of water-hardenable compositions of organic polyisocyanates and polyamines containing at least partly blocked amino groups present as ketimines, the combinations essentially representing mixtures and optionally reaction products containing urea groups by mixing the organic polyisocyanates with the polyamines in such quantities that the equivalent ratio of isocyanate groups to blocked and free amino groups is between about 0.9:1 and 4:1 and reacting any free amino groups present with some of the isocyanate groups in the polyisocyanate to form ureas, characterized in that the polyamines containing at least partly blocked amino groups used are mixtures comprising(a) from about 50 to 95 amine equivalent percent of organic compounds which are free from primary and secondary amino groups and which contain at least two ketimine groups corresponding to the following formula ##STR1## in which R.sup.1 represents an alkyl or cycloalkyl radical and R.sup.2 represents hydrogen or an alkyl or cycloalkyl radical or in which R.sup.1 and R.sup.2 form a cycloaliphatic hydrocarbon radical together with the two carbon atoms of the ketimine group and(b) from about 5 to 40 amine equivalent percent of organic compounds which are free from primary and secondary amino groups and which contain at least two ketimine groups of which one corresponds to the formula ##STR2## in which R.sup.1 and R.sup.2 are as defined above, the other ketimine group(s) present correspond(s) to the formula shown in (a).

    摘要翻译： 用于生产有机多异氰酸酯和含有至少部分封闭的胺基的多胺的水可硬化组合物作为酮亚胺存在的方法，所述组合基本上代表混合物和任选的含有尿素基团的反应产物，通过将有机多异氰酸酯与多胺混合， 异氰酸酯基与封端和游离氨基的当量比为约0.9:1至4:1，并使与多异氰酸酯中存在的一些异氰酸酯基团存在的任何游离氨基反应形成脲，其特征在于，含有至少部分 使用的封闭氨基是包含（a）约50至95胺当量百分比的不含伯和仲氨基并且含有至少两个对应于下式的酮亚胺基的有机化合物的混合物：其中R 1表示 烷基或环烷基，R 2表示氢或a n烷基或环烷基，或其中R1和R2与酮亚胺基团的两个碳原子一起形成脂环族烃基，和（b）约5至40胺当量百分比的不含伯和仲氨基的有机化合物 并且其包含至少两个酮亚胺基，其中一个对应于式（Ia）其中R 1和R 2如上所定义的式“IMAGE”，其它酮亚胺基与（a）所示的式表示。

    Polyisocyanates containing uretdione and/or isocyanurate groups, a process for their production
    4.
    发明授权
    Polyisocyanates containing uretdione and/or isocyanurate groups, a process for their production 失效
    含有URETDIONE和/或异氰酸酯基团的聚异氰酸酯，其生产过程

    公开(公告)号：US5237058A

    公开(公告)日：1993-08-17

    申请号：US774687

    申请日：1991-10-11

    申请人： Hans J. Laas ,  Reinhard Halpaap ,  Josef Pedain

    发明人： Hans J. Laas ,  Reinhard Halpaap ,  Josef Pedain

    IPC分类号： C07D229/00 ,  C07D251/34 ,  C08G18/79 ,  C09D175/00 ,  C09D175/04

    CPC分类号： C07D229/00 ,  C08G18/792 ,  C08G18/798

    摘要： The present invention relates to a process for the production of polyisocyanates containing uretdione and/or isocyanurate groups bya) partially oligomerizing the isocyanate groups of organic diisocyanates to form uretdione and/or isocyanurate groups in the presence of catalysts containing trivalent phosphorus,b) terminating the oligomerization reaction at the desired degree of oligomerization by converting the catalyst into a catalytically inactive oxidized form by the addition of an oxidizing agent andc) subsequently removing unreacted diisocyanate by thin-layer distillation.The present invention also relates to the polyisocyanates containing uretdione and/or isocyanurate groups obtained by this process.Finally, the present invention also relates to the use of these polyisocyanates, optionally blocked with blocking agents for isocyanate groups, as the isocyanate component in polyurethane coating compositions.

    摘要翻译： 本发明涉及通过以下方法制备含有脲二酮和/或异氰脲酸酯基团的多异氰酸酯的方法：a）在含有三价磷的催化剂存在下，部分低聚有机二异氰酸酯的异氰酸酯基团以形成脲二酮和/或异氰脲酸酯基团，b）终止 通过加入氧化剂将催化剂转化成催化惰性氧化形式，并且c）通过薄层蒸馏随后除去未反应的二异氰酸酯，从而在所需的低聚程度下进行低聚反应。 本发明还涉及通过该方法获得的含有脲二酮和/或异氰脲酸酯基团的多异氰酸酯。 最后，本发明还涉及这些聚异氰酸酯，任选地用封端剂封端的异氰酸酯基团作为聚氨酯涂料组合物中的异氰酸酯组分的用途。

    Polyisocyanate mixture, a process for its preparation and its use in polyurethane coating compositions
    5.
    发明授权
    Polyisocyanate mixture, a process for its preparation and its use in polyurethane coating compositions 失效
    聚异氰酸酯混合物，其制备方法及其在聚氨酯涂料组合物中的用途

    公开(公告)号：US5143994A

    公开(公告)日：1992-09-01

    申请号：US759315

    申请日：1991-09-13

    申请人： Hans J. Laas ,  Reinhard Halpaap ,  Josef Pedain ,  Jurgen Mosbach

    发明人： Hans J. Laas ,  Reinhard Halpaap ,  Josef Pedain ,  Jurgen Mosbach

    IPC分类号： C07D229/00 ,  C07D251/30 ,  C07D251/34 ,  C08G18/72 ,  C08G18/79 ,  C09D175/00 ,  C09D175/04

    CPC分类号： C07D229/00 ,  C07D251/34 ,  C08G18/792 ,  C08G18/798 ,  C08G2150/20

    摘要： The present invention relates to polyisocyanate mixtures prepared from 1,6-diisocyanatohexane (HDI) and 1-isocyanato-3,3,5-trimethyl-5-isocyanatomethyl cyclohexane (IPDI), which have a uretdione content (calculated as C.sub.2 N.sub.2 O.sub.2) of 8 to 25% by weight and an isocyanurate content (calculated as C.sub.3 N.sub.3.sub.O.sub.3) of not more than 24% by weight and containa) 20 to 60% by weight of uretdione diisocyanatesb) 0 to 40% by weight of isocyanurate triisocyanatesc) 15 to 60% by weight of higher homologues of the polyisocyanates of components a) and b) containing more than one uretdione ring and/or isocyanurate ring andd) a total of not more than 1% by weight of (HDI) and (IPDI).The present invention also relates to a process for the preparation of these polyisocyanate mixtures and to their use, optionally blocked with blocking agents for isocyanate groups, as the isocyanate component in polyurethane coating compositions.

    摘要翻译： 本发明涉及由1,6-二异氰酸根合己烷（HDI）和1-异氰酸根合-3,3,5-三甲基-5-异氰酸甲酯环己烷（IPDI）制备的多异氰酸酯混合物，其具有脲二酮含量（以C 2 N 2 O 2计算）为8 至25重量％，并且异氰脲酸酯含量（以C3N3O3计算）不超过24重量％，并含有a）20至60重量％的脲二酮二异氰酸酯b）0至40重量％的异氰脲酸酯三异氰酸酯c）15至 60重量％的含有多于一个脲二环和/或异氰脲酸酯环的组分a）和b）的多异氰酸酯的高级同系物和d）总共不超过1重量％的（HDI）和（IPDI）。 本发明还涉及一种制备这些多异氰酸酯混合物的方法及其用途，任选地用聚异氰酸酯基团的封端剂封端，作为聚氨酯涂料组合物中的异氰酸酯组分。

    Isocyanurate group-containing polyisocyanates
    7.
    发明授权
    Isocyanurate group-containing polyisocyanates 失效
    含异氰脲酸酯基的多异氰酸酯

    公开(公告)号：US4851531A

    公开(公告)日：1989-07-25

    申请号：US74380

    申请日：1987-07-16

    申请人： Reinhard Halpaap ,  Gerhard Klein ,  Roland Richter ,  Hanns P. Muller ,  Josef Pedain ,  Hans-Joachim Kreuder

    发明人： Reinhard Halpaap ,  Gerhard Klein ,  Roland Richter ,  Hanns P. Muller ,  Josef Pedain ,  Hans-Joachim Kreuder

    IPC分类号： C08G18/00 ,  C07D251/34 ,  C08G18/02 ,  C08G18/79 ,  C09D5/46 ,  C09D175/00 ,  C09D175/12

    CPC分类号： C08G18/792 ,  C07D251/34 ,  C08G2150/20

    摘要： The present invention is directed to isocyanato isocyanurates prepared from diisocyanates which contain a sterically unhindered isocyanate group bound to a primary aliphatic carbon atom and a sterically hindered isocyanate group which is bound to a tertiary carbon atom forming part of a cycloaliphatic ring system, said diisocyanate having an NCO content of about 20 to 50% by weight. The present invention is further directed to a process for preparing these isocyanato isocyanurates by catalytic trimerization and the use of the isocyanato isocyanurates in a process for the production of polyisocyanate polyaddition products, preferably two-component polyurethane stoving lacquers.

    摘要翻译： 本发明涉及由二异氰酸酯制备的异氰酸根合异氰脲酸酯，该二异氰酸酯包含与主要脂族碳原子结合的空间上不受阻碍的异氰酸酯基团和与形成脂环族环系的一部分的叔碳原子结合的空间位阻异氰酸酯基团，所述二异氰酸酯具有 约20至50重量％的NCO含量。 本发明还涉及一种通过催化三聚制备这些异氰酸酯异氰脲酸酯的方法，以及在制备多异氰酸酯加聚产物的方法中使用异氰酸酯基异氰脲酸酯的方法，优选为双组分聚氨酯烘烤漆。

    Tertiary polyisocyanate derivatives
    8.
    发明授权
    Tertiary polyisocyanate derivatives 失效
    三元多异氰酸酯衍生物

    公开(公告)号：US4748242A

    公开(公告)日：1988-05-31

    申请号：US930584

    申请日：1986-11-12

    申请人： Reinhard Halpaap ,  Josef Pedain ,  Hans-Joachim Kreuder ,  Gerhard Klein ,  Dieter Arlt

    发明人： Reinhard Halpaap ,  Josef Pedain ,  Hans-Joachim Kreuder ,  Gerhard Klein ,  Dieter Arlt

    IPC分类号： C08G18/00 ,  C08G18/02 ,  C08G18/06 ,  C08G18/79 ,  C08G63/52 ,  C07D251/30 ,  C07D251/32

    CPC分类号： C08G18/792 ,  C08G2150/20

    摘要： The present invention is directed to a process for the production of polyisocyanates containing isocyanurate groups by trimerizing a mixture of aliphatic-cycloaliphatic diisocyanates having a sterically unhindered isocyanate group bound to a primary aliphatic carbon atom and a sterically hindered isocyanate group bound to a tertiary carbon atom which forms a part of a cycloaliphatic ring system and 1,6-diisocyanatohexane. The present invention is also directed to the polyisocyanates containing isocyanurate groups produced according to this process and to their use, optionally in blocked form, as an isocyanate component in the production of polyisocyanate polyaddition products, preferably polyurethane lacquers.

    摘要翻译： 本发明涉及一种制备含有异氰脲酸酯基团的多异氰酸酯的方法，该方法是将具有与伯脂肪族碳原子结合的空间上不受阻碍的异氰酸酯基团和与叔碳原子结合的位阻异氰酸酯基团的脂族 - 脂环族二异氰酸酯的混合物三聚 其形成脂环族环系的一部分和1,6-二异氰酸根合己烷。 本发明还涉及根据该方法制备的含有异氰脲酸酯基团的多异氰酸酯基团，以及它们在多异氰酸酯加聚产物（优选聚氨酯漆）生产中作为异氰酸酯组分的用途，任选地以封闭形式使用。

    Process for the production of light-stable polyisocyanates containing allophanate groups
    10.
    发明授权
    Process for the production of light-stable polyisocyanates containing allophanate groups 失效
    用于生产含有脲基甲酸酯基的光稳定多异氰酸酯的方法

    公开(公告)号：US06392001B1

    公开(公告)日：2002-05-21

    申请号：US08432285

    申请日：1995-05-01

    申请人： Harald Mertes ,  Josef Pedain ,  Reinhard Halpaap

    发明人： Harald Mertes ,  Josef Pedain ,  Reinhard Halpaap

    IPC分类号： C08G1810

    CPC分类号： C08G18/7837 ,  C07C273/1836 ,  C07C275/60

    摘要： The present invention relates to a process for the production of polyisocyanates containing allophanate groups and having aliphatically and/or cycloaliphatically bound isocyanate groups by reacting organic compounds containing urethane groups with organic polyisocyanates containing aliphatically and/or cycloaliphatically bound isocyanate groups in the presence of tin compounds and to the use of these polyisocyanates, optionally blocked with blocking agents for isocyanate groups, as an isocyanate component in the production of polyurethanes, in particular polyurethane coatings.

    摘要翻译： 本发明涉及通过在锡化合物的存在下使含有氨基甲酸酯基团的有机化合物与含有脂族和/或环状结合的异氰酸酯基团的有机多异氰酸酯反应来生产含有脲基甲酸酯基并具有脂族和/或环脂键结的异氰酸酯基团的多异氰酸酯的方法 以及在聚氨酯生产中尤其是聚氨酯涂料中使用这些多异氰酸酯，任选地被异氰酸酯基封端剂封闭，作为异氰酸酯组分。