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    Method of applying high pressures to a high pressure assembly
    71.
    发明授权
    Method of applying high pressures to a high pressure assembly 失效
    向高压组件施加高压的方法

    公开(公告)号：US07540075B2

    公开(公告)日：2009-06-02

    申请号：US11211140

    申请日：2005-08-24

    Applicant: Chien-Min Sung

    Inventor： Chien-Min Sung

    IPC: B23P11/00 ,  B28B3/00

    CPC classification number: B01J3/065 ,  B01J3/067 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0625 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068 ,  B30B11/004 ,  B30B11/007 ,  Y10T29/49826 ,  Y10T29/49863 ,  Y10T29/49998 ,  Y10T29/51

    Abstract: An improved high pressure apparatus can include a plurality of complementary die segments. The die segments can have inner surfaces which are shaped to form a die chamber upon assembly of the die segments. A pair of anvils can be oriented such that an anvil is at each end of the die chamber. To prevent the die segments from being forced apart during movement of the anvils, force members can be connected to the die segments. The force members can apply discrete forces to the die segments sufficient to retain the die segments in substantially fixed positions relative to each other during application of force by the pair of anvils. Using such a high pressure apparatus can achieve pressures as high as 10 GPa with improved useful die life and larger reaction volumes.

    Abstract translation: 改进的高压装置可以包括多个互补的模片段。 模具段可以具有内表面，其在模具段的组装时成形为形成模腔。 一对砧座可以被定向成使得砧座在模腔的每个端部。 为了防止模具段在砧座移动期间被迫分开，可以将力构件连接到模具段。 力构件可以向模具段施加离散的力，足以在由一对砧施加力期间将模具段保持在相对于彼此的基本上固定的位置。 使用这种高压装置可以实现高达10GPa的压力，并且具有改善的有用的模具寿命和较大的反应体积。

    Superabrasive particle synthesis with growth control
    72.
    发明申请
    Superabrasive particle synthesis with growth control 审中-公开
    超研磨颗粒合成与生长控制

    公开(公告)号：US20080047484A1

    公开(公告)日：2008-02-28

    申请号：US11891058

    申请日：2007-08-07

    Applicant: Chien-Min Sung

    Inventor： Chien-Min Sung

    IPC: C30B1/02 ,  C30B1/00

    CPC classification number: B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0625 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068 ,  B01J2203/0685 ,  B22F2005/001 ,  B22F2999/00 ,  B23D61/18 ,  B23D65/00 ,  B23P15/28 ,  B24D3/08 ,  B24D7/066 ,  B24D18/00 ,  B24D99/005 ,  B24D2203/00 ,  C04B35/52 ,  C09K3/1409 ,  C09K3/1445 ,  C22C1/051 ,  C22C26/00 ,  C22C2204/00 ,  E21B10/5676 ,  Y10T428/2991 ,  B22F2207/03 ,  B22F1/0011 ,  B22F3/004 ,  B22F2003/1046

    Abstract: An improved method for synthesizing superabrasive particles provides high quality industrial superabrasive particles with high yield and a narrow size distribution. The synthesis method can include forming a growth precursor of a substantially homogeneous mixture of raw material and catalyst material or layers of raw material and metal catalyst. The growth precursor can have a layer of adhesive over at least a portion thereof. A plurality of crystalline seeds can be placed in a predetermined pattern on the layer of adhesive. The growth precursor can be maintained at a temperature and pressure at which the superabrasive crystal is thermodynamically stable for a time sufficient for a desired degree of growth. Advantageously, the patterned placement of crystalline seeds and disclosed processes allow for production of various morphologies of synthetic diamonds, including octahedral and cubic diamonds, and improved growth conditions generally. As a result, the grown superabrasive particles typically have a high yield of high quality particles and a narrow distribution of particle sizes.

    Abstract translation: 合成超级磨料颗粒的改进方法提供高产率和窄尺寸分布的高质量工业超研磨颗粒。 合成方法可以包括形成原料和催化剂材料或原料和金属催化剂层的基本上均匀的混合物的生长前体。 生长前体可在其至少一部分上具有一层粘合剂。 多个结晶种子可以以预定图案放置在粘合剂层上。 生长前体可以保持在超磨料晶体在热力学稳定的温度和压力下达足以达到所需生长程度的时间。 有利地，结晶晶种的图案化布置和所公开的方法允许生产合成金刚石的各种形态，包括八面体和立方晶体，以及通常改善的生长条件。 结果，生长的超级磨料颗粒通常具有高产率的高质量颗粒和窄的粒度分布。

    Method for the preparation of diamond, graphite or their mixture
    73.
    发明授权
    Method for the preparation of diamond, graphite or their mixture 失效
    金刚石，石墨或其混合物的制备方法

    公开(公告)号：US07270707B2

    公开(公告)日：2007-09-18

    申请号：US10534671

    申请日：2002-11-15

    Applicant: Qianwang Chen ,  Yitai Qian ,  Zhengsong Lou

    Inventor： Qianwang Chen ,  Yitai Qian ,  Zhengsong Lou

    IPC: C30B29/04

    CPC classification number: C30B29/04 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/068 ,  C01B32/20 ,  C01B32/25 ,  C01B32/28 ,  C30B9/10

    Abstract: The present invention provides a method of preparation for diamond, graphite or mixtures of diamond and graphite by reduction of CO or CO2. Said method comprises a step of contacting an active metal capable of reducing a carbon source into elementary carbon with carbon source (such as CO and/or CO2 and/or their origin) under conditions suitable to reduce the carbon source to elementary carbon in the course of a reduction reaction. After the raw diamond or mixtures of diamond and graphite thus obtained are subjected to intensive heat treatment with perchloric acid, pure diamond granules are obtained. The present method employs relatively low reaction temperature and pressure and the facilities needed in the method are simple and easy to operate. Diamond finally obtained has good crystallinity and free of impurities with granule size of several hundred micrometer. In addition, the present invention makes use of the industrial by-product of CO and CO2 which not only turns wastes into valuables and is low in cost, but also improves the environment and thus possesses both good social benefits and economical benefits.

    Abstract translation: 本发明提供通过还原CO或CO 2制备金刚石，石墨或金刚石和石墨的混合物的方法。 所述方法包括在适于减少碳源的条件下将能够将碳源还原成碳源的活性金属与碳源（例如CO和/或CO 2 2和/或它们的来源）接触的步骤 碳还原反应过程中的碳源。 在将生金刚石或由此获得的金刚石和石墨的混合物用高氯酸进行强烈热处理之后，得到纯金刚石颗粒。 本方法采用相对较低的反应温度和压力，该方法所需的设备简单易操作。 最终获得的金刚石具有良好的结晶度，不含颗粒尺寸为几百微米的杂质。 此外，本发明利用CO和CO 2的工业副产品，其不仅将废物转化为贵重物品，成本低，而且改善了环境，因此具有良好的社会性 效益和经济效益。

    Process for the synthesis of diamond
    78.
    发明授权
    Process for the synthesis of diamond 失效
    金刚石合成工艺

    公开(公告)号：US6129900A

    公开(公告)日：2000-10-10

    申请号：US307493

    申请日：1994-09-16

    Applicant: Shuichi Satoh ,  Hitoshi Sumiya ,  Kazuwo Tsuji ,  Yasushi Gouda

    Inventor： Shuichi Satoh ,  Hitoshi Sumiya ,  Kazuwo Tsuji ,  Yasushi Gouda

    IPC: B01J3/06

    CPC classification number: B01J3/062 ,  B01J2203/061 ,  B01J2203/0655 ,  B01J2203/067 ,  B01J2203/068

    Abstract: A colorless and transparent, substantially inclusion-free diamond crystal which can be applied to decorative uses and optical parts is synthesized by a process using a temperature gradient method in an ultra-high pressure apparatus. This process comprises using, as a solvent for the growth of the crystal, at least one metal selected from the group consisting of Fe, Co, Ni, Mn and Cr (at least two metals in the case of containing Fe) and as a nitrogen getter for the removal of nitrogen in the solvent, at least one metal selected from the group consisting of Al, Ti, Zr, Hf, V, Nb and Ta in a proportion of 0.5 to 7% by weight (at most 2% by weight when using only Al) to the solvent metal.

    Abstract translation: PCT No.PCT / JP92 / 00149 Sec。 371日期：1992年10月14日 102（e）日期1992年10月14日PCT提交1992年2月14日PCT公布。 公开号WO92 / 14542 日期1992年9月3日可以应用于装饰用途和光学部件的无色透明的基本上不含夹杂的金刚石晶体通过在超高压装置中使用温度梯度法的方法合成。 该方法包括使用选自Fe，Co，Ni，Mn和Cr中的至少一种金属作为晶体生长的溶剂（在含有Fe的情况下至少有两种金属）和作为氮 吸附剂用于除去溶剂中的氮，至少一种选自Al，Ti，Zr，Hf，V，Nb和Ta的金属，其含量为0.5〜7重量％（最多2重量％ 当仅使用Al时）溶剂金属。

    Diamond synthesis
    79.
    发明授权
    Diamond synthesis 失效
    钻石综合

    公开(公告)号：US5980852A

    公开(公告)日：1999-11-09

    申请号：US203768

    申请日：1994-03-01

    Applicant: Robert Charles Burns ,  Dennis Leonard Welch

    Inventor： Robert Charles Burns ,  Dennis Leonard Welch

    IPC: B01J3/06 ,  C30B29/04

    CPC classification number: B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/068

    Abstract: A reaction vessel for use in producing large diamond crystals of good quality and yield includes a reaction volume and a reaction mass located in the volume. The reaction mass comprises a plurality of seed particles located in or on a surface in the reaction volume and a carbon source separated from the seed particles by a mass of metallic catalyst/solvent for diamond synthesis. The mass comprises alternating layers of carbon-rich and carbon-lean metallic catalyst/solvent which lie parallel or substantially parallel to the surface. There is also provided a mass of alternating layers of carbon-rich and carbon-lean metallic catalyst/solvent.

    Abstract translation: 用于生产质量和产率高的大型金刚石晶体的反应容器包括位于体积中的反应体积和反应物质。 反应物料包括位于反应体积中的表面上或其上的多个种子颗粒，以及通过大量用于金刚石合成的金属催化剂/溶剂与种子颗粒分离的碳源。 该物质包括平行或基本平行于表面的富含碳和贫碳的金属催化剂/溶剂的交替层。 还提供了大量的富含碳和贫碳的金属催化剂/溶剂的交替层。

    Diamond synthesis
    80.
    发明授权
    Diamond synthesis 失效
    钻石综合

    公开(公告)号：US5772756A

    公开(公告)日：1998-06-30

    申请号：US770685

    申请日：1996-12-19

    Applicant: Geoffrey John Davies ,  Aulette Stewart ,  Bronwyn Annette Roberts

    Inventor： Geoffrey John Davies ,  Aulette Stewart ,  Bronwyn Annette Roberts

    IPC: B01J3/06 ,  C30B29/04

    CPC classification number: B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/068

    Abstract: A method of producing diamond crystal growth on a seed crystal is provided. The method includes the steps of providing a seed crystal containing at least one twin plane and re-entrant growth surfaces associated therewith and applying high temperature/high pressure synthesis conditions to the seed crystal to cause diamond growth to occur preferentially on the re-entrant surfaces. The diamond growth on the seed crystal results in a diamond crystal being produced which has an aspect ratio greater than 1.

    Abstract translation: 提供了一种在晶种上生产金刚石晶体生长的方法。 该方法包括以下步骤：提供含有至少一个双平面和与其相关的再生长生长表面的晶种，并将高温/高压合成条件施加到籽晶上，以使金刚石生长优先优先发生在入口表面上 。 晶种上的金刚石生长导致制造出具有大于1的纵横比的金刚石晶体。

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