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    Method of preparing crystalline aluminosilicates
    72.
    发明授权
    Method of preparing crystalline aluminosilicates 失效
    制备结晶硅铝酸盐的方法

    公开(公告)号：US4533649A

    公开(公告)日：1985-08-06

    申请号：US528528

    申请日：1983-09-01

    申请人： William J. Ball ,  Sami A. I. Barri ,  Dennis Young

    发明人： William J. Ball ,  Sami A. I. Barri ,  Dennis Young

    IPC分类号： B01J29/00 ,  B01J29/70 ,  C01B39/04 ,  C01B39/46 ,  C07C1/24 ,  C07C2/12 ,  C07C2/54 ,  C07C4/08 ,  C07C5/02 ,  C07C5/22 ,  C07C5/32 ,  C07C5/41 ,  C10G11/05 ,  C10G35/095 ,  C10G49/08 ,  C01B33/28 ,  B01J29/28

    CPC分类号： C10G49/08 ,  C01B33/2869 ,  C07C1/24 ,  C07C2/12 ,  C07C2/54 ,  C07C4/08 ,  C07C5/02 ,  C07C5/222 ,  C07C5/321 ,  C07C5/41 ,  C10G11/05 ,  C10G35/095 ,  C07C2529/70 ,  Y10S423/35

    摘要： The present invention relates to a process for producing crystalline aluminosilicates having in the hydrogen form an X-ray diffraction pattern substantially as set forth in Table 1 of this specification and the following composition in terms of the mole ratios of the oxides:0.9=0.2 M.sub.2 /.sub.n O:Al.sub.2 O.sub.3 :xSiO.sub.2 :yH.sub.2 O:zNH.sub.3wherein M is at least one cation having a valence n, x is at least 10, y/x is from 0 to 5 and z/x is 0-5. The process comprises mixing a source of silica, a source of alumina, a source of alkali metal(s), water and ammonia until a homogeneous gel is formed and crystallizing the gel at a temperature above 70.degree. C. for a period of at least 2 hours. The crystalline aluminosilicate thus produced can be used, whether or not impregnated and/or ion-exchanged, as catalysts for any one of the following reactions: alkylation, dealkylation, dehydrocyclodimerization, aromatization, transalkylation, isomerization, dehydrogenation, hydrogenation, cracking, cyclization, oligomerization, polymerization, and dehydration reactions.

    摘要翻译： 本发明涉及一种生产结晶铝硅酸盐的方法，其具有氢形式，其基本上如本说明书的表1所示的X射线衍射图，并且以下氧化物摩尔比的组成：0.9 = 0.2M2 / nO：Al 2 O 3：xSiO 2：yH 2 O：zNH 3其中M为至少一个价数为n的阳离子，x为至少10，y / x为0至5，z / x为0-5。 该方法包括将二氧化硅源，氧化铝源，碱金属源，水和氨混合直到形成均匀的凝胶，并将凝胶在高于70℃的温度下结晶至少一段时间 2小时。 无论是否浸渍和/或离子交换，可以使用如此制备的结晶硅铝酸盐作为以下任一反应的催化剂：烷基化，脱烷基化，脱氢环二聚化，芳构化，烷基转移，异构化，脱氢，氢化，裂解，环化， 低聚，聚合和脱水反应。