Method for Producing Compound Single Crystal and Production Apparatus for Use Therein
    82.
    发明申请
    Method for Producing Compound Single Crystal and Production Apparatus for Use Therein 有权
    生产复合单晶的方法及其使用的生产设备

    公开(公告)号:US20070215035A1

    公开(公告)日:2007-09-20

    申请号:US10598095

    申请日:2005-02-18

    IPC分类号: C30B25/00

    摘要: The present invention provides a method for producing a compound single crystal that can improve a growth rate and grow a large single crystal with high crystal uniformity in a short time, and a production apparatus used for the method. The compound single crystal is grown while stirring a material solution to create a flow from a gas-liquid interface in contact with a source gas toward the inside of the material solution. With this stirring, the source gas can be dissolved easily in the material solution, and supersaturation can be achieved in a short time, thus improving the growth rate of the compound single crystal. Moreover, the flow formed by the stirring goes from the gas-liquid interface where a source gas concentration is high to the inside of the material solution where the source gas concentration is low, so that dissolution of the source gas becomes uniform. Accordingly, it is possible not only to suppress nonuniform nucleation at the gas-liquid interface, but also to improve the quality of the compound single crystal produced.

    摘要翻译: 本发明提供了一种能够在短时间内提高生长速度和生长具有高结晶均匀性的大单晶的化合物单晶的制造方法和用于该方法的制造装置。 在搅拌材料溶液的同时培养复合单晶以产生与源气体接触的气液界面朝向材料溶液内部的流动。 通过该搅拌,能够将源气体容易地溶解在原料溶液中,可以在短时间内实现过饱和,从而提高复合单晶的生长速度。 此外,通过搅拌形成的流动源于源气体浓度高的气液界面到源气体浓度低的材料溶液的内部,使得源气体的溶解变得均匀。 因此,不仅可以抑制气液界面的不均匀成核,而且可以提高制造的复合单晶的质量。

    Method for flattening surface of oxide crystal to ultra high degree
    84.
    发明授权
    Method for flattening surface of oxide crystal to ultra high degree 失效
    氧化物晶体表面超高度平坦化的方法

    公开(公告)号:US07029528B2

    公开(公告)日:2006-04-18

    申请号:US10469987

    申请日:2002-03-15

    IPC分类号: C30B29/22

    摘要: There are provided a method of superflattening an oxide crystal that is soluble neither with acid nor with alkaline, a method of making a ReCa4O(BO3)3 family oxide single crystal thin film using the superflattening method, a ReCa4O(BO3)3 family oxide single crystal thin film having a SHG property, a superflattening method for light incident/emitting surfaces, and a defect assessing method for oxide crystals. The surface of an oxide crystal that is soluble neither with acid nor with alkaline is reduced with a reducing agent, the reduced oxide crystal surface is dissolved with an aqueous solution of acid or alkaline, the surface dissolved oxide crystal is heat-treated in the atmosphere, whereby the surface of an oxide crystal that is soluble neither with acid nor with alkaline is superflattened to an atomic level. According to this method, a chemically stable oxide which because of its complexity in both composition and structure is soluble neither with acid nor with alkaline and is insoluble even with a fluoric acid is allowed by reduction to be converted into a simpler oxide conventionally soluble with hydrochloric, nitric or sulfuric acid; hence a surface of its crystal is rendered capable of dissolving. Then, heat-treating the dissolved surface in the atmosphere at a suitable temperature for a suitable time period allows surface atoms to be rearranged and the surface to be superflattened to an atomic level. The present invention is applicable to the technical fields that require ultraviolet laser light, especially as core technologies of optical devices applied to optical information processing, optical communication or the like.

    摘要翻译: 提供了一种对既不具有酸也不与碱性溶解的氧化物晶体进行超平坦化的方法,制备ReCa 4 O(BO 3 3)3的方法 使用超平坦化方法的ReCa 4 O 3(3-3)3族氧化物单晶薄膜 具有SHG特性的膜,用于光入射/发射表面的超平面方法,以及氧化物晶体的缺陷评估方法。 用还原剂还原不溶于酸和碱的氧化物晶体的表面,还原的氧化物晶体表面用酸或碱的水溶液溶解,表面溶解的氧化物晶体在大气中进行热处理 由此,不仅酸和碱也不溶解的氧化物晶体的表面被超级原子化。 根据该方法,化学稳定的氧化物由于其组成和结构的复杂性既不溶于酸也不溶于碱,并且即使用氟酸也不溶于还原,可以转化为常规可溶于盐酸的简单氧化物 ,硝酸或硫酸; 因此其晶体的表面能够溶解。 然后,在合适的温度下对溶解在大气中的表面进行适当的时间周期处理,使得表面原子被重新排列并将表面超平坦化到原子水平。 本发明适用于需要紫外线激光的技术领域,特别是作为光学信息处理,光通信等的光学装置的核心技术。

    Nonlinear optical crystal
    85.
    发明申请
    Nonlinear optical crystal 审中-公开
    非线性光学晶体

    公开(公告)号:US20050254118A1

    公开(公告)日:2005-11-17

    申请号:US11169668

    申请日:2005-06-30

    IPC分类号: G02F1/355 G02F1/35 H01S3/10

    CPC分类号: G02F1/3551

    摘要: There is provided a nonlinear optical crystal which is presented by the formula: K2Al2B2O7. This nonlinear optical crystal is a vacuum ultraviolet light generating nonlinear optical crystal which is easy to grow and of high practical use. There are also provided a wavelength conversion method using this crystal, and an element and a wavelength conversion apparatus for use in the method.

    摘要翻译: 提供了一种非线性光学晶体,其由下列公式表示:K 2 2 Al 2 B 2 N 2 O 7 。 这种非线性光学晶体是一种容易生长和高实用性的真空紫外线发生非线性光学晶体。 还提供了使用该晶体的波长转换方法以及用于该方法的元件和波长转换装置。

    Cesium-lithium borate crystal
    87.
    发明授权
    Cesium-lithium borate crystal 失效
    铯硼酸锂晶体

    公开(公告)号:US5998313A

    公开(公告)日:1999-12-07

    申请号:US788840

    申请日:1997-01-27

    CPC分类号: C30B15/00 C30B17/00 C30B29/10

    摘要: A cesium-lithium borate crystal, of which the chemical composition is expressed by any of the following formulae:Cs.sub.1-x Li.sub.1-y M.sub.x+y B.sub.6 O.sub.10,andCs.sub.2(1-z) Li.sub.2 L.sub.z B.sub.12 O.sub.20(where, M is an alkali metal element, and L is an alkali earth element), and in which an exotic element is doped or annealed.

    摘要翻译: 硼酸铯晶体,其化学成分由下式表示:Cs1-xLi1-yMx + yB6O10和Cs2(1-z)Li2LzB12O20(其中,M为碱金属元素,L为 碱土元素),并且其中外来元素被掺杂或退火。

    Cesium-lithium-borate crystal and its application to frequency conversion of laser light
    90.
    发明申请
    Cesium-lithium-borate crystal and its application to frequency conversion of laser light 有权
    铯硼酸锂晶体及其应用于激光的变频

    公开(公告)号:US20060165578A1

    公开(公告)日:2006-07-27

    申请号:US11315134

    申请日:2005-12-23

    IPC分类号: C01B35/10

    摘要: The present invention provides a cesium-lithium-borate crystal, which can be used as a high-performance wavelength converting crystal, having a chemical composition expressed as CsLiB6O10, and substituted cesium-lithium-borate crystals expressed by the following formula: Cs1-xLi1-yMx+yB6O10 or Cs2(1−z)Li2LzB12O20 (where, M is an alkali metal element, and L is an alkali earth metal element); a method for manufacturing same by heating and melting; and an optical apparatus using such crystals.

    摘要翻译: 本发明提供一种可用作具有以CsLiB6O10表示的化学组成的高性能波长转换晶体的铯 - 硼酸锂晶体和由下式表示的取代的铯 - 锂 - 硼酸盐晶体:<β -line-formula description =“In-line Formulas”end =“lead”?> Cs> Li Li Li Li Li x x x x x x x / / / / / / / / / / / / / / / / / β-in-line-formula description =“In-line Formulas”end =“tail”?> <?in-line-formula description =“在线公式”end =“lead”?>或<?in-line-formula description =“In-line Formulas”end =“tail”?> <?in-line-formula description =“In-line 2“(1-z)2”>“2”>“2”> - > (式中,M为碱金属元素,L为碱土类金属元素)(式中,M为碱金属元素) ; 通过加热和熔融制造相同方法; 以及使用这种晶体的光学装置。