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    Resin dispersions having high pigment binding capacity
    2.
    发明授权
    Resin dispersions having high pigment binding capacity 失效
    具有高颜料结合能力的树脂分散体

    公开(公告)号：US4395515A

    公开(公告)日：1983-07-26

    申请号：US334228

    申请日：1981-12-24

    申请人： Horst Dinklage ,  Herbert Fink ,  Peter Frank ,  Hubert Rauch ,  Werner Siol

    发明人： Horst Dinklage ,  Herbert Fink ,  Peter Frank ,  Hubert Rauch ,  Werner Siol

    IPC分类号： C08F220/00 ,  C08F2/22 ,  C08F2/24 ,  C08F220/04 ,  C08F220/06 ,  C09D11/107 ,  C09D17/00 ,  C08L33/02

    CPC分类号： C09D11/107 ,  C08F2/24 ,  C08F220/04 ,  C08F220/06

    摘要： What are disclosed are methods for making an aqueous dispersion of a synthetic resin copolymer, said dispersion having high pigment binding capacity and adaptable to use in the preparation of printing inks or pastes, said copolymer comprising a predominant amount of water insoluble monomers together with from 3 to 8 percent by weight of an acid component which is a water soluble acid or salt, which method comprises gradually adding said water insoluble monomers, together with a portion of said acid component, to an aqueous medium containing the balance of the acid component in the form of a dissolved water soluble salt; aqueous synthetic resin dispersions made by these methods; and printing inks comprising such an aqueous synthetic resin dispersion which has been neutralized and combined with such an amount of an organic solvent as converts the dispersion into a solution or colloidal dispersion of the synthetic resin.

    摘要翻译： 所公开的方法是制备合成树脂共聚物的水分散体的方法，所述分散体具有高的颜料结合能力并且适用于制备印刷油墨或浆料，所述共聚物包含主要量的水不溶性单体和3 至8重量％的作为水溶性酸或盐的酸组分，该方法包括将所述水不溶性单体与一部分所述酸组分逐渐加入到含有余量的酸组分的水性介质中 溶解的水溶性盐的形式; 通过这些方法制备的水性合成树脂分散体; 以及包含这样的水性合成树脂分散体的印刷油墨，其被中和并与这种量的有机溶剂组合以将分散体转化为合成树脂的溶液或胶体分散体。

    Pharmaceutical coating materials soluble or swellable in gastric juice and pharmaceutical dosage forms coated therewith
    5.
    发明授权
    Pharmaceutical coating materials soluble or swellable in gastric juice and pharmaceutical dosage forms coated therewith 失效
    在胃液中可溶或溶胀的药物包衣材料和用其涂覆的药物剂型

    公开(公告)号：US4452862A

    公开(公告)日：1984-06-05

    申请号：US345478

    申请日：1982-02-03

    申请人： Gerhard Markert ,  Dieter Dreher ,  Klaus Lehmann ,  Werner Siol ,  Hubert Rauch

    发明人： Gerhard Markert ,  Dieter Dreher ,  Klaus Lehmann ,  Werner Siol ,  Hubert Rauch

    IPC分类号： A61K9/58 ,  A61K9/28 ,  A61K9/32 ,  A61K47/32 ,  B32B5/16

    CPC分类号： A61K9/2846 ,  Y10T428/2998

    摘要： Coating materials for pharmaceutical dosage forms contain, besides the conventional liquid or solid additives for pharmaceutical coatings, a binder comprising a synthetic polymer, prepared by emulsion polymerization, having 5 to 100% by weight of units derived from monomers of the formula ##STR1## wherein R.sub.1 is a hydrogen atom or a lower alkyl group, R.sub.2 is an alkylene or aralkylene group having at least 3 carbon atoms in the chain between the amino nitrogen and the ester oxygen atom of which at least one is tertiary or quaternary, and R.sub.3 and R.sub.4 are lower alkyl radicals or together with the amino-nitrogen atom form a heteroaliphatic ring, and, optionally, additional comonomer units.

    摘要翻译： 用于药物剂型的涂层材料除了用于药物涂层的常规液体或固体添加剂外，还包含通过乳液聚合制备的包含合成聚合物的粘合剂，其具有5至100重量％的衍生自下式的单体的单元：其中 R1是氢原子或低级烷基，R2是在氨基氮和酯氧原子之间的链中具有至少3个碳原子的亚烷基或亚芳基，其至少一个是叔或四价，R3和R4 是低级烷基或与氨基 - 氮原子一起形成杂脂族环，和任选的另外的共聚单体单元。

    Method for making polymodal aqueous synthetic resin dispersions
    7.
    发明授权
    Method for making polymodal aqueous synthetic resin dispersions 失效
    多型水性合成树脂分散体的制备方法

    公开(公告)号：US4539361A

    公开(公告)日：1985-09-03

    申请号：US708096

    申请日：1985-03-04

    申请人： Werner Siol ,  Wolfgang Klesse ,  Norbert Suetterlin ,  Hubert Rauch

    发明人： Werner Siol ,  Wolfgang Klesse ,  Norbert Suetterlin ,  Hubert Rauch

    IPC分类号： C08F2/00 ,  C08F2/04 ,  C08F2/22 ,  C08F2/24 ,  C08F265/06 ,  C08F291/00 ,  C08J3/06

    CPC分类号： C08F265/06 ,  C08F291/00

    摘要： A method for making an aqueous polymodal synthetic resin dispersion by the emulsion polymerization of an ethylenically unsaturated monomer difficultly soluble in water, or a mixture of such monomers forming a polymer which is water insoluble under the conditions of polymerization, in an aqueous phase containing an emulsifier and a water soluble polymerization initiator, which method comprises adding a seed latex to the polymerization mixture in the course of the emulsion polymerization before more than 40 weight percent of said monomers have been polymerized, the particles of said seed latex being smaller by a factor ranging from 2 to 15 than are particles already formed by emulsion polymerization, the amount by weight of the particles in the seed latex being not greater than 10 percent by weight of the monomers and the ratio by weight of particles of said seed latex to the weight of the monomers already polymerized being from 1:4 to 1:500.

    摘要翻译： 通过难溶于水的烯键式不饱和单体的乳液聚合或在聚合条件下形成水不溶性的聚合物的这些单体的混合物在含有乳化剂的水相中制备水性聚合物合成树脂分散体的方法 和水溶性聚合引发剂，该方法包括在超过40重量％的所述单体聚合之前，在乳液聚合过程中向聚合混合物中加入种子胶乳，所述种子胶乳的颗粒小于一定范围 从已经通过乳液聚合形成的颗粒的2至15比例，种子胶乳中颗粒的重量百分比不大于单体的10重量％，并且所述种子胶乳颗粒的重量比 已经聚合的单体为1:4至1:500。

    Method for making aqueous dispersions of a synthetic resin
    8.
    发明授权
    Method for making aqueous dispersions of a synthetic resin 失效
    制造合成树脂的水性分散体的方法

    公开(公告)号：US4456726A

    公开(公告)日：1984-06-26

    申请号：US434825

    申请日：1982-10-18

    申请人： Werner Siol ,  Herbert Fink ,  Wolfgang Klesse ,  Hubert Rauch ,  Norbert Suetterlin

    发明人： Werner Siol ,  Herbert Fink ,  Wolfgang Klesse ,  Hubert Rauch ,  Norbert Suetterlin

    IPC分类号： C08F2/00 ,  C08F2/22 ,  C08F2/24 ,  C08F265/06 ,  C08F291/00 ,  C08F2/16

    CPC分类号： C08F265/06 ,  C08F291/00

    摘要： What is disclosed is making highly concentrated, bimodal, aqueous synthetic resin dispersions by the emulsion polymerization of ethylenically unsaturated monomers, in the presence of emulsifiers and free radical-forming initiators, by adding to a first latex containing a first dispersed synthetic resin and an aqueous phase, a second latex containing a second dispersed synthetic resin and an aqueous phase and a monomer phase containing a free-radically polymerizable monomer, and then polymerizing the monomer, the average size of the particles of said first resin differing by a factor between 2 and 15 from that of the particles of second resin, the total weight of the resins and monomers representing 100 parts by weight, and the total weight of the aqueous phases representing not more than 70 parts by weight.

    摘要翻译： 公开的是通过在乳化剂和自由基形成引发剂的存在下，通过烯属不饱和单体的乳液聚合制备高浓度双峰水性合成树脂分散体，通过加入含有第一分散的合成树脂和含水的 相，含有第二分散合成树脂和水相的第二胶乳和含有可自由基聚合的单体的单体相，然后使单体聚合，所述第一树脂的颗粒的平均尺寸在2和 15与第二树脂颗粒的重量比，树脂和单体的总重量代表100重量份，水相的总重量不大于70重量份。