摘要:
The present invention relates to a process for preparing catalyst composition for the synthesis of carbon nanotube with high yields using the spray pyrolysis method. More particularly, this invention relates to a process for preparing catalyst composition for the synthesis of carbon nanotube comprising the steps of i) dissolving multi-component metal precursors of catalyst composition in de-ionized water; ii) spraying obtained catalytic metal precursor solution into the high temperature reactor by gas atomization method; iii) forming the catalyst composition powder by pyrolysis of gas atomized material; and iv) obtaining the catalyst composition powder, wherein said catalyst composition comprises i) main catalyst selected from Fe or Co, ii) Al, iii) optional co-catalyst at least one selected from Ni, Cu, Sn, Mo, Cr, Mn, V, W, Ti, Si, Zr or Y, iv) inactive support of Mg. Further, the catalyst composition prepared by this invention has a very low apparent density of 0.01˜0.50 g/ml as well as the catalyst composition affords high production yield (1,000˜1,800%) of carbon nanotube.
摘要:
The present invention relates to a catalyst composition for the synthesis of thin multi-walled carbon nanotube (MWCNT) and a method for manufacturing a catalyst composition. More particularly, this invention relates to a multi-component metal catalyst composition comprising i) main catalyst of Fe and Al, ii) inactive support of Mg and iii) optional co-catalyst at least one selected from Co, Ni, Cr, Mn, Mo, W, V, Sn, or Cu. Further, the present invention affords thin multi-walled carbon nanotube having 5˜20 nm of diameter and 100˜10,000 of aspect ratio in a high yield.
摘要:
The present invention is to provide anode active material hybridized with carbon nano fibers for lithium secondary battery prepared by following steps comprising, i) dispersing the nano size metal catalyst to the surface of anode material selected from graphite, amorphous silicon or the complex of graphite and amorphous silicon; and ii) growing the carbon nano fiber by chemical vapor deposition method, wherein carbon nano fibers are grown in a vine form and surround the surface of anode active material.
摘要:
Disclosed are a carbon nanomaterial pellet and a method for preparing same. More particularly, it relates to a carbon nanomaterial pellet having a specific size and a high apparent density prepared by a simple process using only a rotary tablet press without mixing a carbon nanomaterial powder with a solvent or an additive, which is capable of solving the powder dust problem occurring when preparing a polymer composite from a carbon nanomaterial in the form of powder, thus improving physical properties and remarkably reducing cost of packaging and transportation, and a method for preparing the carbon nanomaterial pellet from a carbon nanomaterial powder.
摘要:
Disclosed is a method for preparing a carbon nanomaterial/polymer composite. More particularly, it relates to an improved method for preparing a carbon nanomaterial/polymer composite capable of solving a dust problem of a carbon nanomaterial powder and a layer separation problem due to large density difference between the carbon nanomaterial powder and a polymer pellet and providing superior physical properties of the composite, whereby an additive used to prepare the carbon nanomaterial/polymer composite is mixed with the carbon nanomaterial powder and prepared into a pellet, which is then mixed with the polymer pellet.
摘要:
The present invention relates to a method for evaluating an initial capacity of secondary batteries and, more specifically, to a method for evaluating an initial capacity of secondary batteries that involves mathematical operation of specific internal resistance components obtained from an equivalent circuit model of an impedance spectrum measured for a short time period instead of using direct discharge characteristics, thereby allowing selection of batteries having a different initial discharge characteristic.
摘要:
The present invention relates to a catalyst composition for the synthesis of multi-walled carbon nanotube having high apparent density in a manner of high yield. More particularly, this invention relates to a multi-component metal catalyst composition comprising i) main catalyst of Fe and Mo, ii) inactive support of Al and iii) optional co-catalyst at least one selected from Co, Ni, Ti, Mn, W, Sn or Cu. Further, the present invention affords multi-walled carbon nanotube having 5˜15 nm of fibrous diameter and 0.5˜4 μm bundle diameter.
摘要:
Disclosed are a carbon nanomaterial pellet and a method for preparing same. More particularly, it relates to a carbon nanomaterial pellet having a specific size and a high apparent density prepared by a simple process using only a rotary tablet press without mixing a carbon nanomaterial powder with a solvent or an additive, which is capable of solving the powder dust problem occurring when preparing a polymer composite from a carbon nanomaterial in the form of powder, thus improving physical properties and remarkably reducing cost of packaging and transportation, and a method for preparing the carbon nanomaterial pellet from a carbon nanomaterial powder.
摘要:
The present invention relates to a catalyst composition for preparing carbon nanotube containing multi-component support materials of amorphous Si, Mg and Al as well as a bulk scale preparation process for preparing carbon nanotube using said catalyst composition. More specifically, this invention relates to a process for preparing carbon nanotube using the catalyst composition comprising a transition metal catalyst and support materials of amorphous Si, Mg and Al.
摘要:
The present invention relates to a process for preparing catalyst composition for the synthesis of carbon nanotube with high yields using the spray pyrolysis method. More particularly, this invention relates to a process for preparing catalyst composition for the synthesis of carbon nanotube comprising the steps of i) dissolving multi-component metal precursors of catalyst composition in de-ionized water; ii) spraying obtained catalytic metal precursor solution into the high temperature reactor by gas atomization method; iii) forming the catalyst composition powder by pyrolysis of gas atomized material; and iv) obtaining the catalyst composition powder, wherein said catalyst composition comprises i) main catalyst selected from Fe or Co, ii) Al, iii) optional co-catalyst at least one selected from Ni, Cu, Sn, Mo, Cr, Mn, V, W, Ti, Si, Zr or Y, iv) inactive support of Mg. Further, the catalyst composition prepared by this invention has a very low apparent density of 0.01˜0.50 g/ml as well as the catalyst composition affords high production yield (1,000˜1,800%) of carbon nanotube.