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公开(公告)号：US5681531A
公开(公告)日：1997-10-28
申请号：US552889
申请日：1995-11-03
申请人： Mark A. LaPack , James C. Tou , Terry J. Nestrick
发明人： Mark A. LaPack , James C. Tou , Terry J. Nestrick
CPC分类号： G01N35/1097 , C02F1/008 , G01N33/1826 , G01N2035/00465 , Y10T436/117497 , Y10T436/119163 , Y10T436/12 , Y10T436/255
摘要： Apparatus for optimizing a treatment for removing organic substances from a chemical process stream wherein known quantities and kinds of organic or other compounds are injected into and dissolved in the stream prior to treatment thereof. Samples of the compounds are extracted from the stream before and after treatment thereof and compared with one another to determine the efficiency of the treatment. The injecting apparatus is one that enables a substance that is at least partially immiscible with the liquid of the stream to be injected into the stream at a velocity sufficiently great to cause adequate dissolution of the substance in the stream.
摘要翻译： 用于优化从化学工艺流中除去有机物质的处理的装置，其中已知量的和种类的有机或其它化合物在处理之前被注入并溶解在流中。 在处理之前和之后，从流中提取化合物样品并相互比较以确定处理效率。 注射装置是使能够以足够大的速度将流体的液体至少部分不混溶的物质注入流中的物质使得物质在流中的充分溶解的装置。
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2.发明授权Self-regulated biological scrubber and/or gas stripper for the treatment of fluid streams 失效用于处理流体流的自调节生物洗涤器和/或气体汽提器
公开(公告)号：US5597402A
公开(公告)日：1997-01-28
申请号：US549137
申请日：1995-10-27
CPC分类号： C02F1/20 , C02F3/006 , C02F2209/02 , C02F2209/06 , C02F2209/36 , C02F2209/38 , C02F2209/40
摘要： This invention relates to a self-regulated apparatus and method for extracting biodegradable and/or strippable constituents from a gaseous stream by the action of biomass which consumes or degrades such substances. Such self-regulation permits the monitoring and optimization of the bioactivity of the system and the overall degree of treatment of the gaseous stream.
摘要翻译： 本发明涉及通过消耗或降解这些物质的生物质的作用从气流中提取可生物降解和/或可剥离的成分的自调节装置和方法。 这种自我调节允许监测和优化系统的生物活性和气流的总体处理程度。
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公开(公告)号：US4242227A
公开(公告)日：1980-12-30
申请号：US62380
申请日：1979-07-31
CPC分类号： B01J20/286 , B01J20/3204 , B01J20/3219 , B01J20/3227 , B01J20/3246 , B01J20/3257 , B01J20/3272 , C08G83/001 , B01J2220/54 , B01J2220/58
摘要： Improved packings for columns useful in gas chromatography are made by a multistep process whereby polysiloxane molecules having various organic substituents are chemically bonded to the surface of a siliceous support. The process comprises one or more cycles of successive reactions with an activated support surface of silicon tetrachloride, an organic dichlorosilane, silicon tetrachloride a second time, a polysiloxane polyol, with intermediate hydrolyses where appropriate to provide reactive terminal silanol groups and a final capping reaction with an organic monochlorosilane. The packing as so prepared is further improved by coating with a conventional stationary phase.
摘要翻译： 通过多步法制备用于气相色谱的色谱柱的改进的填料，由此具有各种有机取代基的聚硅氧烷分子化学键合到硅质载体的表面。 该方法包括与四氯化硅的活化载体表面，有机二氯硅烷，四氯化硅第二次，聚硅氧烷多元醇的连续反应的一个或多个循环，其中适当地进行中间水解以提供反应性末端硅烷醇基团，并且最终加帽反应与 有机一氯硅烷。 如此制备的填料通过用常规固定相涂覆进一步改善。
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4.发明授权Dehydrohalogenation of (polyhaloalkyl) benzenes with support Lewis acid catalysts 失效（多卤烷基）苯与支持路易斯酸催化剂的脱卤化氢
公开(公告)号：US4205015A
公开(公告)日：1980-05-27
申请号：US906893
申请日：1978-05-18
CPC分类号： C07C17/278 , C07C17/25 , C07C17/35
摘要： A process for the dehydrohalogenation of a (polyhaloalkyl)benzene containing a benzylic halogen such as 1,3-dichloro-5-(2,4,4,4-tetrachlorobutyl)-benzene by contacting the (polyhaloalkyl)benzene with a Lewis acid such as AlCl.sub.3 deposited on an inert support such as silica gel or alumina under conditions sufficient to catalyze said dehydrohalogenation to form a (polyhaloalkenyl)benzene such as 3,5-dichloro-.alpha.-(2,2,2-trichloroethyl)styrene.
摘要翻译： 通过使（多卤代烷基）苯与路易斯酸接触而使含有苄基卤如1,3-二氯-5-（2,4,4,4-四氯丁基） - 苯的（多卤烷基）苯脱卤化氢的方法， 作为AlCl 3在足以催化所述脱卤化氢以形成（多卤代烯）苯如3,5-二氯-α-（2,2,2-三氯乙基）苯乙烯的条件下沉积在惰性载体如硅胶或氧化铝上的条件下。
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5.发明授权Self-regulated biological scrubber and/or gas stripper for the treatment of fluid streams 失效用于处理流体流的自调节生物洗涤器和/或气体汽提器
公开(公告)号：US5490933A
公开(公告)日：1996-02-13
申请号：US210108
申请日：1994-03-17
CPC分类号： C02F1/20 , C02F3/006 , C02F2209/02 , C02F2209/06 , C02F2209/36 , C02F2209/38 , C02F2209/40
摘要： This invention relates to a self-regulated apparatus and method for extracting biodegradable and/or strippable constituents from a fluid stream by the action of biomass which consumes or degrades such substances or by gas stripping. Such self-regulation permits the monitoring and optimization of the bioactivity of the system and the overall degree of treatment of the fluid stream.
摘要翻译： 本发明涉及一种自调节装置和方法，用于通过消耗或降解这些物质或通过汽提的生物质的作用从流体流中提取可生物降解和/或可剥离的成分。 这种自我调节允许监测和优化系统的生物活性和流体流的整体处理程度。
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6.发明授权
公开(公告)号：US5233876A
公开(公告)日：1993-08-10
申请号：US680463
申请日：1991-04-04
申请人： Mark A. LaPack , James C. Tou , Joanna L. Shih , William E. Martin , Renne Y. Keith , Terry J. Nestrick
发明人： Mark A. LaPack , James C. Tou , Joanna L. Shih , William E. Martin , Renne Y. Keith , Terry J. Nestrick
CPC分类号： B01D63/02 , B01D61/00 , G01N1/2035 , G01N1/34 , G01N33/0026 , G01N33/18 , B01D2313/90 , G01N1/16 , G01N2001/4016
摘要： Apparatus and methods for on-line analysis of multiple stream processes wherein each stream has an influent delivered to a treatment zone and an effluent discharged from such zone and wherein both the influent and effluent are analyzed and the analyses compared for the evaluation of the effectiveness of the treatment.
摘要翻译： 用于在线分析多个流程的装置和方法，其中每个流具有输送到处理区域的流入物和从该区域排出的流出物，并且其中分析流入物和流出物两者，并且对分析进行比较以评估有效性 治疗。
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公开(公告)号：US5482862A
公开(公告)日：1996-01-09
申请号：US337125
申请日：1994-11-10
申请人： Mark A. LaPack , Terry J. Nestrick , James C. Tou
发明人： Mark A. LaPack , Terry J. Nestrick , James C. Tou
CPC分类号： G01N35/1097 , C02F1/008 , G01N33/1826 , G01N2035/00465 , Y10T436/117497 , Y10T436/119163 , Y10T436/12 , Y10T436/255
摘要： Method for optimizing a treatment for removing organic substances from a chemical process stream wherein known quantities and kinds of organic or other compounds are injected into and dissolved in the stream prior to treatment thereof. Samples of the compounds are extracted from the stream before and after treatment thereof and compared with one another to determine the efficiency of the treatment.
摘要翻译： 用于优化从化学工艺流中除去有机物质的处理的方法，其中将已知量的和种类的有机或其它化合物注入并溶解在流中。 在处理之前和之后，从流中提取化合物样品并相互比较以确定处理效率。
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公开(公告)号：US4376641A
公开(公告)日：1983-03-15
申请号：US330343
申请日：1981-12-14
IPC分类号： B01D15/20 , B01J20/281 , B01J20/286 , C03C17/30 , C03C17/34 , G01N30/60 , B01D15/08
CPC分类号： B01J20/286 , B01D15/206 , C03C17/30 , C03C17/3405 , B01J2220/54 , B01J2220/86 , G01N30/6078
摘要： In the production of a wall coated open tubular capillary chromatographic column, improved deactivation of the inner surface of a glass or fused silica capillary tube prior to coating with stationary phase is obtained by a multi-step process whereby siloxane polymer molecules are chemically bonded to the capillary inner surface. The process comprises multiple cycles of successive reactions with silicon tetrachloride and a diorganodichlorosilane vapor with intermediate hydrolyses and a final capping reaction with a triorganochlorosilane. The deactivated surface is adapted to coating with an apolar liquid stationary phase.
摘要翻译： 在制备涂有壁涂层的开放式管状毛细管色谱柱时，通过多步法获得玻璃或熔融石英毛细管内表面在固定相涂覆之前的失活，由此硅氧烷聚合物分子化学键合到 毛细管内表面。 该方法包括与四氯化硅的连续反应的多个循环和具有中间水解的二有机二氯硅烷蒸气和与三有机氯硅烷的最终封端反应。 失活的表面适于用非极性液体固定相涂覆。
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公开(公告)号：US4276061A
公开(公告)日：1981-06-30
申请号：US149868
申请日：1980-05-14
IPC分类号： B01J20/286 , B01J20/32 , C08G83/00 , B01D15/08
CPC分类号： B01J20/286 , B01J20/103 , B01J20/14 , B01J20/262 , B01J20/28004 , B01J20/3092 , B01J20/3204 , B01J20/3227 , B01J20/3246 , B01J20/3272 , B01J20/3278 , C08G83/001 , B01J2220/54 , B01J2220/58
摘要： Improved packings for columns useful in gas chromatography are made by a multistep process whereby polysiloxane molecules having various organic substituents are chemically bonded to the surface of a siliceous support. The process comprises one or more cycles of successive reactions with an activated support surface of silicon tetrachloride, an organic dichlorosilane, silicon tetrachloride a second time, a polysiloxane polyol, with intermediate hydrolyses where appropriate to provide reactive terminal silanol groups and a final capping reaction with an organic monochlorosilane. The packing as so prepared is further improved by coating with a conventional stationary phase.
摘要翻译： 用于气相色谱的色谱柱的改进的填料通过多步法制备，其中具有各种有机取代基的聚硅氧烷分子化学键合到硅质载体的表面。 该方法包括与四氯化硅的活化载体表面，有机二氯硅烷，四氯化硅第二次，聚硅氧烷多元醇的连续反应的一个或多个循环，其中适当地进行中间水解以提供反应性末端硅烷醇基团，并且最终加帽反应与 有机一氯硅烷。 如此制备的填料通过用常规固定相涂覆进一步改善。
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公开(公告)号：US4199330A
公开(公告)日：1980-04-22
申请号：US5274
申请日：1979-01-22
CPC分类号： B01J20/262 , B01J20/103 , B01J20/286 , B01J20/287 , B01J20/288 , B01J20/29 , B01J20/3092 , B01J20/3204 , B01J20/3217 , B01J20/3219 , B01J20/3246 , B01J20/3257 , B01J20/3261 , B01J20/3272 , B01J2220/54 , B01J2220/58
摘要： Highly effective chromatographic column packings are prepared by reacting hydroxyl groups on a silica surface with SiCl.sub.4 and then reacting the chlorosilylated surface with a polyglycol or polymeric glycol ester in a slurry reaction. Residual chlorosilane groups on the reacted surface are neutralized by reaction with methanol or other lower alkanol. The resulting modified silica has a bonded, essentially monomolecular organic surface film which provides thermal stability, uniform efficiency, and rapid analysis when the material is used as a column packing in gas-liquid chromatography.
摘要翻译： 通过使二氧化硅表面上的羟基与SiCl 4反应，然后使氯代甲硅烷基化的表面与聚二醇或聚乙二醇酯在淤浆反应中反应制备高效的色谱柱填料。 通过与甲醇或其它低级链烷醇的反应中和反应表面上残留的氯代硅烷基团。 所得到的改性二氧化硅具有键合的基本上单分子的有机表面膜，当将该材料用作气液色谱法中的柱填料时，其提供热稳定性，均匀的效率和快速分析。
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