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    Carbon dioxide-blown overbased calcium alkylphenolate lubricating compositions
    1.
    发明授权
    Carbon dioxide-blown overbased calcium alkylphenolate lubricating compositions 失效
    二氧化碳吹制高碱性烷基酚钙润滑组合物

    公开(公告)号：US4320016A

    公开(公告)日：1982-03-16

    申请号：US78346

    申请日：1979-09-24

    申请人： Benjamin H. Zoleski ,  Gayle P. Herbert ,  Rodney L. Sung ,  Robert M. Scarberry

    发明人： Benjamin H. Zoleski ,  Gayle P. Herbert ,  Rodney L. Sung ,  Robert M. Scarberry

    IPC分类号： C10M159/22 ,  C10M1/38

    CPC分类号： C10M159/22 ,  C10M2219/087 ,  C10M2219/088 ,  C10M2219/089

    摘要： A lubricating oil composition containing a blend of sulfurized calcium alkylphenolate having an alkylphenol to calcium metal rate of about 1.0 to 1.4 and a Ca content of 0.5 to 12 wt. % prepared by: (1) reacting at a temperature between 250.degree. and 410.degree. F. an alkylphenol with calcium alkoxyalkoxide to form a first reaction mixture utilizing between about 45 and 90 wt. % of the stoichiometric amount required to convert the alkylphenol to calcium alkylphenolate: (2) contacting the reaction mixture with sulfur at a temperature between about 440.degree. and 460.degree. F. in the presence of between about 13 and 20 wt. % of a lubricating oil based on the step 2 second reaction mixture, (3) contacting the second reaction mixture with calcium alkoxyalkoxide at a temperature between about 400.degree. and 425.degree. F.; first and second additions totaling about 280 percent of the stoichiometric amount of calcium alkoxyalkoxide to form said calcium alkylphenolate; (4) hydrolyzing the blown mixture by steam sparging with at least 100% of the stoichiometric amount of steam required for complete hydrolysis of the calcium-2-methoxyethoxide to calcium hydroxide at a temperature ranging from 350.degree. to 410.degree. F., blowing the hydrolyzed mixture with about 20% of the stoichiometric amount of CO.sub.2 required for partial carbonation to form a blend of 20% carbonate overbased sulfurized calcium alkylphenolate and 80% hydroxide overbased sulfurized calcium alkylphenolate and adding thereto at a temperature of 340.degree. to 350.degree. F. a diluent oil.

    摘要翻译： 一种润滑油组合物，其含有烷基酚与硫酸化的烷基酚钙与钙金属速率约为1.0-1.4，Ca含量为0.5-12重量％的共混物。 通过以下方法制备的：（1）在250-410°F的温度下使烷基酚与烷氧基烷氧基烷烃反应形成第一反应混合物，其中使用约45-90wt。 将烷基酚转化为烷基酚盐酸盐所需的化学计量量的百分比：（2）在约440℃至460℃之间的温度下，将反应混合物与硫接触，在约13至20重量％ 基于步骤2第二反应混合物的润滑油的％;（3）在约400至425°F的温度下使第二反应混合物与烷氧基烷氧基烷烃接触; 第一和第二次加入总计约280％的化学计量的烷氧基烷烃氧化物以形成所述烷基酚钙; （4）通过蒸汽喷射将吹入的混合物水解成至少100％的化学计量量的蒸汽，所述蒸汽在350-410°F的温度下完全水解为氢氧化钙。 水解混合物，其中约20％的部分碳酸化所需的CO 2的化学计量量形成20％碳酸盐高碱性硫化烷基酚钙盐和80％氢氧化物高碱性硫化烷基酚钙酸盐的共混物，并在340°至350°F的温度下加入。 稀释油。

    Lubricant oil composition containing a friction modifier
    2.
    发明授权
    Lubricant oil composition containing a friction modifier 失效
    含有摩擦改性剂的润滑油组合物

    公开(公告)号：US4505835A

    公开(公告)日：1985-03-19

    申请号：US528348

    申请日：1983-08-31

    申请人： Rodney L. Sung ,  Benjamin H. Zoleski ,  Sheldon Herbstman ,  Peter Dorn

    发明人： Rodney L. Sung ,  Benjamin H. Zoleski ,  Sheldon Herbstman ,  Peter Dorn

    IPC分类号： C10M133/16 ,  F02B3/06 ,  C10M1/36

    CPC分类号： C10M133/16 ,  C10M2207/028 ,  C10M2215/12 ,  C10M2219/046 ,  C10N2240/10 ,  C10N2240/102 ,  C10N2240/103 ,  F02B3/06

    摘要： A lubricant composition includes a mineral lubricanting lubricant composition and a friction modifying amount of a reaction product of an amine and maleic anhydride represented by the formula: ##STR1## in which X and X' are either: ##STR2## in which R and R' can be any hydrocarbon radicals and the total number of carbon atoms in R plus R' varies from about 6 to about 30, and wherein the nitrogen is bound to a secondary carbon atom, or wherein R is a hydrogen atom and R' is a branched hydrocarbon radical having from about 6 to 30 carbon atoms, or ##STR3## in which Y varies from 2 to 6, and in which R" is a hydrocarbon radical having from about 6 to 30 carbon atoms, and R"' is hydrogen or a methyl radical. The lubricant composition finds use in various internal combustion engines including slow and medium speed diesel engines and as a lubricant in the upper cylinder of a slow speed marine diesel engine.

    摘要翻译： 润滑剂组合物包括矿物润滑润滑剂组合物和由下式表示的胺和马来酸酐的反应产物的摩擦改进量：其中X和X'为：其中R 并且R'可以是任何烃基，并且R + R'中的碳原子总数从约6至约30变化，并且其中氮与仲碳原子结合，或其中R是氢原子，R' 是具有约6至30个碳原子的支链烃基，或其中Y从2-6变化且其中R“是具有约6-30个碳原子的烃基，或 R“'是氢或甲基。 润滑剂组合物可用于各种内燃机，包括缓慢和中等速度的柴油发动机，以及作为慢速船用柴油发动机的上部气缸中的润滑剂。