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    Silyl terminated prepolymers, method for making them and adhesive compositions made therefrom
    1.
    发明授权
    Silyl terminated prepolymers, method for making them and adhesive compositions made therefrom 有权

    公开(公告)号：US09920199B2

    公开(公告)日：2018-03-20

    申请号：US14835761

    申请日：2015-08-26

    Applicant: Dow Global Technologies LLC

    Inventor： Syed Z. Mahdi ,  Yiyong He

    IPC: C08L75/08 ,  C08G18/10

    CPC classification number: C08L75/08 ,  C08G18/10 ,  C08G18/2865 ,  C08G18/289

    Abstract: An improved silane modified polymer useful in adhesive compositions is made from a silane precursor material made by a process comprising reacting an organic compound having a backbone that is terminated by an amino group having at least one active amino hydrogen and a hydrolysable silane, wherein the backbone is comprised of at least one secondary amino group having one active amino hydrogen and a Michael addition acceptor compound, wherein the Michael addition compound fails to have a group reactive with an isocyanate group to form the silane precursor compound. The silane precursor compound is reacted with an isocyanate terminated polyurethane prepolymer to form a silane modified prepolymer. The silane modified prepolymer may then be cured with moisture and may be employed in an adhesive composition containing other components such as a plasticizer, catalyst and filler.

    SILYL TERMINATED PREPOLYMERS, METHOD FOR MAKING THEM AND ADHESIVE COMPOSITIONS MADE THEREFROM
    3.
    发明申请
    SILYL TERMINATED PREPOLYMERS, METHOD FOR MAKING THEM AND ADHESIVE COMPOSITIONS MADE THEREFROM 有权
    SILYL终止预处理剂，制备它们的方法和粘合组合物

    公开(公告)号：US20150068661A1

    公开(公告)日：2015-03-12

    申请号：US14467746

    申请日：2014-08-25

    Applicant: DOW GLOBAL TECHNOLOGIES LLC

    Inventor： Syed Z. Mahdi ,  Susan P. Sevidal

    IPC: C09J175/08 ,  C09J5/00 ,  B32B37/12 ,  C08G18/10

    CPC classification number: C09J175/08 ,  C03C27/00 ,  C03C27/048 ,  C08G18/10 ,  C08G18/4825 ,  C08G18/7671 ,  C09J5/00 ,  C09J183/16 ,  C08G18/289

    Abstract: The invention is an adhesive composition comprising a silyl terminated prepolymer having a number molecular weight average (Mn) of about 8,000 to about 80,000 g/mole, a filler, and a silanol condensation reaction catalyst. The silyl terminated prepolymer is comprised of a polymeric backbone of alkylene oxide and at least three urethane groups and at least two terminal groups comprised of a silicon atom having at least two alkoxy silane groups, wherein each silicon atom in the terminal groups is separated from the urethane groups in the polymeric backbone by an amount of alkylene oxide that has a molecular weight of 200 to 15,000 g/mole.

    Abstract translation: 本发明是包含数均分子量（Mn）为约8,000至约80,000g / mol的甲硅烷基封端的预聚物，填料和硅烷醇缩合反应催化剂的粘合剂组合物。 甲硅烷基封端的预聚物由环氧烷和至少三个氨基甲酸酯基团的聚合物骨架和至少两个由具有至少两个烷氧基硅烷基团的硅原子组成的端基组成，其中端基中的每个硅原子与 聚合物主链中的氨基甲酸酯基团具有分子量为200至15,000g / mol的烯化氧。

    Rubber vibration damping material
    4.
    发明授权
    Rubber vibration damping material 有权

    公开(公告)号：US10189960B2

    公开(公告)日：2019-01-29

    申请号：US15509016

    申请日：2015-12-10

    Applicant: Dow Global Technologies LLC ,  Rohm and Haas Company

    Inventor： Roger A. Cassell ,  Syed Z. Mahdi ,  Parvinder S. Walia

    IPC: C08L9/00 ,  C08J3/24 ,  C08C19/18 ,  C08J3/26 ,  C08K3/06

    Abstract: A vulcanized rubber is formed by a method comprising blending a halogenated unsaturated polymer into a rubber comprised of cis 1-4 polyisoprene to form a vulcanizable polymer blend, adding a vulcanization material to the vulcanizable polymer blend, and vulcanizing the vulcanizable polymer blend to form a homogeneous vulcanized rubber. The method may be used to form a vulcanized rubber comprised of polyisoprene uniformly crosslinked with a halogenated unsaturated polymer that is a reaction product of (i) an unsaturated polymer miscible with polyisoprene and having conjugated dienes that undergo a Diels Alder reaction and (ii) a polyhalogenated cyclopentadiene.

    SILYL TERMINATED PREPOLYMERS, METHOD FOR MAKING THEM AND ADHESIVE COMPOSITIONS MADE THEREFROM
    7.
    发明申请
    SILYL TERMINATED PREPOLYMERS, METHOD FOR MAKING THEM AND ADHESIVE COMPOSITIONS MADE THEREFROM 有权
    SILYL终止预处理剂，制备它们的方法和粘合组合物

    公开(公告)号：US20160060382A1

    公开(公告)日：2016-03-03

    申请号：US14835761

    申请日：2015-08-26

    Applicant: Dow Global Technologies LLC

    Inventor： Syed Z. Mahdi ,  Yiyong He

    IPC: C08G18/83 ,  C08L75/08

    CPC classification number: C08L75/08 ,  C08G18/10 ,  C08G18/2865 ,  C08G18/289

    Abstract: An improved silane modified polymer useful in adhesive compositions is made from a silane precursor material made by a process comprising reacting an organic compound having a backbone that is terminated by an amino group having at least one active amino hydrogen and a hydrolysable silane, wherein the backbone is comprised of at least one secondary amino group having one active amino hydrogen and a Michael addition acceptor compound, wherein the Michael addition compound fails to have a group reactive with an isocyanate group to form the silane precursor compound. The silane precursor compound is reacted with an isocyanate terminated polyurethane prepolymer to form a silane modified prepolymer. The silane modified prepolymer may then be cured with moisture and may be employed in an adhesive composition containing other components such as a plasticizer, catalyst and filler.

    Abstract translation: 可用于粘合剂组合物的改进的硅烷改性聚合物由硅烷前体材料制成，所述硅烷前体材料通过包括使具有由具有至少一个活性氨基氢的氨基封端的主链与可水解硅烷反应的有机化合物反应而制备，其中主链 由具有一个活性氨基氢和迈克尔加成受体化合物的至少一个仲氨基组成，其中迈克尔加成化合物不能具有与异氰酸酯基反应形成硅烷前体化合物的基团。 将硅烷前体化合物与异氰酸酯封端的聚氨酯预聚物反应以形成硅烷改性预聚物。 硅烷改性预聚物然后可以用水分固化，并且可以用于含有其它组分例如增塑剂，催化剂和填料的粘合剂组合物中。

    TWO-PART POLYURETHANE ADHESIVE FOR BONDING FIBER-REINFORCED PLASTICS
    8.
    发明申请
    TWO-PART POLYURETHANE ADHESIVE FOR BONDING FIBER-REINFORCED PLASTICS 有权
    用于粘合纤维增强塑料的双组分聚氨酯粘合剂

    公开(公告)号：US20130255880A1

    公开(公告)日：2013-10-03

    申请号：US13990149

    申请日：2011-11-17

    Applicant: DOW GLOBAL TECHNOLOGIES LLC

    Inventor： Syed Z. Mahdi ,  Yee Y. Wang ,  Arthur F. Cawley

    IPC: C09J175/04 ,  C09J5/06

    CPC classification number: C09J175/04 ,  C08G18/089 ,  C08G18/10 ,  C08G18/168 ,  C08G18/3206 ,  C08G18/4072 ,  C08G18/4816 ,  C08G18/4841 ,  C08G18/4858 ,  C08G18/632 ,  C08G18/7664 ,  C08G18/797 ,  C09J5/06 ,  C08G18/6511 ,  C08G18/6674

    Abstract: A two-part polyurethane adhesive system includes a resin component A and a curative B. The resin component A includes a monomeric polyisocyanate and a prepolymer. The curative B includes a of ether polyol having a molecular weight of from 3000 to 20,000 and another polyol having 4-8 hydroxyl groups and a molecular weight of from 200 to 1000. The system includes a tin (IV) catalyst, which is contained in the resin component, and a blocked aza-type catalyst, which is contained in the curative. The system has excellent shelf stability, gives an excellent open time at ambient temperatures, and cures rapidly when heated to 65° C. or higher.

    Abstract translation: 双组分聚氨酯粘合剂体系包括树脂组分A和固化剂B.树脂组分A包括单体多异氰酸酯和预聚物。 固化剂B包括分子量为3000至20,000的醚多元醇和具有4-8个羟基并且分子量为200至1000的另一种多元醇。该体系包括锡（IV）催化剂，其包含在 树脂组分和封闭的氮杂型催化剂。 该系统具有优异的储存稳定性，在环境温度下提供优异的开放时间，并且当加热至65℃或更高时可迅速固化。

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