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    High Molecular Weight Hydrophobic Polyol
    4.
    发明申请
    High Molecular Weight Hydrophobic Polyol 审中-公开

    公开(公告)号：US20180346637A1

    公开(公告)日：2018-12-06

    申请号：US15774827

    申请日：2016-11-09

    Applicant: Dow Global Technologies LLC

    Inventor： Adam C. Colson ,  Dan Yu ,  Daniel A. Aguilar ,  Amber Marie Stephenson ,  William H. Heath ,  Shouren Ge

    IPC: C08G18/48 ,  C08G18/76 ,  C08G18/10 ,  C09J175/08 ,  C09D175/08

    CPC classification number: C08G18/4854 ,  C08G18/10 ,  C08G18/3206 ,  C08G18/4812 ,  C08G18/7614 ,  C08G18/7671 ,  C09D175/08 ,  C09J175/08 ,  C08G18/48

    Abstract: A cured composition including a reaction product of a mixture that includes an isocyanate component having one or more isocyanates and an isocyanate-reactive component having a butylene oxide based polyol, which has a number average molecular weight greater than 2,000 g/mol and less than 8,000 g/mol and a nominal hydroxyl functionality from (2) to (4). At least (50) wt % of a total weight of alkylene oxides used to form the butylene oxide based polyol is butylene oxide. An isocyanate index of the mixture is from (90) to (150). The cured composition in a cured state exhibits a first tan delta peak between a first temperature range of 50° C. to 0° C. and a second tan delta peak between a second temperature range of 75° C. and 150° C., according to a tan delta plot over a range of temperatures, and a value of the first tan delta peak and a value of the second tan delta peak each represents a ratio of a loss modulus of the cured composition and a storage modulus of the cured composition at a specific temperature within the range of temperatures, as measured according to dynamic mechanical thermal analysis. The values of the first and the second tan delta peaks are from (0.10) to (0.90).

    PROCESS OF MANUFACTURING SURFACTANTS AND LUBRICANTS
    10.
    发明申请
    PROCESS OF MANUFACTURING SURFACTANTS AND LUBRICANTS 审中-公开

    公开(公告)号：US20200277436A1

    公开(公告)日：2020-09-03

    申请号：US16646060

    申请日：2018-09-14

    Applicant: Dow Global Technologies LLC

    Inventor： Arjun Raghuraman ,  William H. Heath ,  Bruce D. Hook ,  Wanglin Yu ,  Sukrit Mukhopadhyay ,  Heather A. Spinney ,  David R. Wilson

    IPC: C08G65/26

    Abstract: A method of producing an alcohol ethoxylate surfactant or lubricant, the method including reacting a low molecular weight initiator with ethylene oxide in the presence of a polymerization catalyst, the low molecular weight initiator having a nominal hydroxyl functionality at least 1, and the polymerization catalyst being a Lewis acid catalyst having the general formula M(R1)1(R2)1(R3)1(R4)0 or 1, whereas M is boron, aluminum, indium, bismuth or erbium, R1, R2, R3, and R4 are each independent, R1 includes a first fluoroalkyl-substituted phenyl group, R2 includes a second fluoroalkyl-substituted phenyl group or a first fluoro/chloro-substituted phenyl group, R3 includes a third fluoroalkyl-substituted phenyl group or a second fluoro/chloro-substituted phenyl group, and optional R4 includes a functional group or functional polymer group, R1 being different from at least one of R2 and R3. The method further including forming an alcohol ethoxylate surfactant or lubricant having a number average molecular weight of greater than the number average molecular weight of the low molecular weight initiator in the presence of the Lewis acid catalyst.

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