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1.发明授权
公开(公告)号：US4302399A
公开(公告)日：1981-11-24
申请号：US128718
申请日：1980-03-10
CPC分类号： C09B69/10 , C09B5/14 , Y10S534/03
摘要： Acetylation of residual primary and secondary alkyl amine groups in polymeric colorants, when said colorants are in the form of a crude preparation reaction mixture, is disclosed. The acetylation improves the colorants' water solubility.
摘要翻译： 公开了当所述着色剂为粗制备反应混合物形式时，聚合着色剂中残留的伯和仲烷基胺基的乙酰化作用。 乙酰化改善着色剂的水溶性。
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公开(公告)号：USRE30362E
公开(公告)日：1980-08-05
申请号：US30781
申请日：1979-04-17
CPC分类号： C09B69/106 , C08F8/44
摘要： Poly(vinylamine salts of mineral acids are produced by reacting acetaldehyde and acetamide at a mole ratio of 1:2-4 with acid catalyst, cracking the ethylidene-bisacetamide which results into vinylacetamide, polymerizing the vinylacetamide with a free radical polymerization catalyst, and hydrolyzing the poly(vinylacetamide) to the desired amine salts by contacting the polyvinylacetamide with an aqueous solution of the corresponding mineral acid. This product may be converted to the free amine, which in turn may function as a precursor in the manufacture of certain polymeric dyes and colorants.
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3.发明授权Water-soluble polymeric colorants containing anionic water-solubilizing groups 失效含有阴离子水溶性基团的水溶性聚合物着色剂
公开(公告)号：US4169203A
公开(公告)日：1979-09-25
申请号：US743205
申请日：1976-11-18
CPC分类号： C09B69/10 , Y10S534/03
摘要： Acetylation of residual primary and secondary alkyl amine groups present in the structure of polymeric colorants and the acetylated colorant products are disclosed. The acetylation is a post production step. The acetylation improves the colorants' water solubility.
摘要翻译： 公开了存在于聚合着色剂和乙酰化着色剂产品结构中的残留的伯和仲烷基胺基团的乙酰化。 乙酰化是后期制作步骤。 乙酰化改善着色剂的水溶性。
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4.发明授权Process for preparing polymeric colorants having a poly(vinylamine) backbone 失效制备具有聚（乙烯胺）主链的聚合物着色剂的方法
公开(公告)号：US4275002A
公开(公告)日：1981-06-23
申请号：US760201
申请日：1977-01-17
IPC分类号： A23L1/275 , C08F8/00 , C08F8/12 , C09B29/00 , C09B69/10 , C07C107/02 , C07C107/08 , C09B31/30
CPC分类号： C09B69/106 , A23L5/47 , C08F8/00 , C08F8/12 , C09B29/00 , Y10S534/03
摘要： Polymeric colorants are prepared by the process of (a) reacting acetaldehyde and acetamide in a mole ratio of 1:2-4 with an acid catalyst to form ethylidene-bis-acetamide, (b) cracking the ethylidene-bis-acetamide to vinylacetamide, (c) polymerizing the vinylacetamide with a free-radical catalyst, (d) hydrolyzing the resulting polymer with mineral acid and neutralizing with base to yield poly(vinylamine), and (e) coupling monomeric optically chromophoric groups to amine nitrogens of the poly(vinylamine).
摘要翻译： 通过以下方法制备聚合着色剂：（a）使乙醛与乙酰胺以1：2-4的摩尔比与酸催化剂反应，形成亚乙基 - 双 - 乙酰胺，（b）将亚乙基双乙酰胺裂解成乙烯基乙酰胺， （c）用自由基催化剂聚合乙烯基乙酰胺，（d）用无机酸水解所得聚合物并用碱中和以产生聚（乙烯基胺），和（e）将单体光学发色基团与聚（乙烯基）胺的胺氮键合， 乙烯胺）。
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公开(公告)号：US4018826A
公开(公告)日：1977-04-19
申请号：US520530
申请日：1974-11-04
IPC分类号： A23L1/275 , C08F8/00 , C08F8/12 , C09B29/00 , C09B69/10 , A23L1/27 , C07C87/24 , C08F120/52 , C08F126/02
CPC分类号： C09B69/106 , A23L5/47 , C08F8/00 , C08F8/12 , C09B29/00 , Y10S534/03
摘要： Poly(vinylamine) salts of mineral acids are produced by reacting acetaldehyde and acetamide at a mole ratio of 1:2-4 with acid catalyst, cracking the ethylidene-bis-acetamide which results into vinylacetamide, polymerizing the vinylacetamide with a free radical polymerization catalyst, and hydrolyzing the poly(vinylacetamide) to the desired amine salts by contacting the polyvinylacetamide with an aqueous solution of the corresponding mineral acid. This product may be converted to the free amine, which in turn may function as a precursor in the manufacture of certain polymeric dyes and colorants.
摘要翻译： 无机酸的聚（乙烯胺）盐通过使乙醛和乙酰胺以1:2-4的摩尔比与酸催化剂反应制得，使亚乙基双 - 乙酰胺裂解成乙烯基乙酰胺，用自由基聚合催化剂聚合乙烯基乙酰胺 ，并通过使聚乙烯基乙酰胺与相应的无机酸的水溶液接触来将聚（乙烯基乙酰胺）水解成所需的胺盐。 该产物可以转化为游离胺，其又可以在制备某些聚合物染料和着色剂时起到前体的作用。
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6.发明授权
公开(公告)号：US4532128A
公开(公告)日：1985-07-30
申请号：US651654
申请日：1984-09-17
IPC分类号： A61K31/74 , A61K31/745 , A61K31/785 , A01N33/12
CPC分类号： A61K31/745 , A61K31/74 , A61K31/785 , Y10S514/912
摘要： Polymeric quaternary ammonium compounds having recurring vinylbenzyl ammonium units are disclosed. The quaternary ammonium units preferably have 2 alkyl substituents of 1 to 4 carbons and 1 alkyl substituent of 4 to 12 carbons. These materials have antimicrobial properties and are particularly useful for preserving ophthalmic solutions.
摘要翻译： 公开了具有重复的乙烯基苄基铵单元的聚合季铵化合物。 季铵单元优选具有1至4个碳的2个烷基取代基和4至12个碳的1个烷基取代基。 这些材料具有抗微生物性质，特别适用于保护眼用溶液。
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7.发明授权
公开(公告)号：US4482680A
公开(公告)日：1984-11-13
申请号：US484721
申请日：1983-04-13
IPC分类号： A61K31/74 , A61K31/745 , A61K31/785 , C08F114/02 , A01N33/12 , C08F214/02
CPC分类号： A61K31/785 , A61K31/74 , A61K31/745 , Y10S514/97
摘要： Polymeric quaternary ammonium compounds having recurring vinylbenzyl ammonium units are disclosed. The quaternary ammonium units preferably have 2 alkyl substituents of 1 to 4 carbons and 1 alkyl substituent of 4 to 12 carbons. These materials have antimicrobial properties and are particularly useful for preserving ophthalmic solutions.
摘要翻译： 公开了具有重复的乙烯基苄基铵单元的聚合季铵化合物。 季铵单元优选具有1至4个碳的2个烷基取代基和4至12个碳的1个烷基取代基。 这些材料具有抗微生物性质，特别适用于保护眼用溶液。
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公开(公告)号：US4381185A
公开(公告)日：1983-04-26
申请号：US271912
申请日：1981-06-09
摘要： Water-fast printing of paper stock using a colorant solution containing water-soluble polymeric dyes is accomplished by a three step process. Step 1 is selecting a paper stock characterized as containing at least 250 ppm by weight of cation, particularly a polyvalent metal cation (especially Ca.sup.2+ or Al.sup.3+). In step 2, a colorant solution is applied to the paper. This solution is water-based, containing up to 30 wt % of an organic paper-penetrating agent (such as an alkanol), and at least 500 ppm of one or more anionic group-possessing polymeric colorants. In step 3, the solvent is exhausted by either evaporation (which may be aided by the application of heat) or diffusion into the paper stock, or by a combination of both.
摘要翻译： 使用含有水溶性聚合物染料的着色剂溶液对纸料进行水快速印刷通过三步法完成。 步骤1是选择特征在于含有至少250ppm重量的阳离子，特别是多价金属阳离子（特别是Ca 2+或Al 3+）的纸料。 在步骤2中，将着色剂溶液施加到纸上。 该溶液是水性的，其含有至多30重量％的有机纸张渗透剂（例如链烷醇）和至少500ppm的一种或多种含阴离子基团的聚合物着色剂。 在步骤3中，溶剂通过蒸发（其可以通过施加热量）或扩散到纸料中或通过两者的组合而被排出。
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9.发明授权Photo acid generator compounds, photo resists, and method for improving bias 失效照片酸发生剂化合物，光致抗蚀剂和改善偏压的方法
公开(公告)号：US6074800A
公开(公告)日：2000-06-13
申请号：US64955
申请日：1998-04-23
申请人： Gregory Breyta , Phillip J. Brock , Daniel J. Dawson , Ronald A. DellaGuardia , Charlotte R. DeWan , Andrew R. Eckert , Hiroshi Ito , Premlatha Jagannathan , Leo L. Linehan , Kathleen H. Martinek , Wayne M. Moreau , Randolph J. Smith
发明人： Gregory Breyta , Phillip J. Brock , Daniel J. Dawson , Ronald A. DellaGuardia , Charlotte R. DeWan , Andrew R. Eckert , Hiroshi Ito , Premlatha Jagannathan , Leo L. Linehan , Kathleen H. Martinek , Wayne M. Moreau , Randolph J. Smith
IPC分类号： G03F7/004
CPC分类号： G03F7/0045 , Y10S430/115
摘要： Several mid UV photo acid generators (PAGs), a chemically amplified photo resist (CAMP), and method for improving nested to isolated line bias are provided. Similarly, photo speed may also be improved. Unlike conventional mid UV PAGs, the present invention's PAG compounds, resist composition, and method do not require a mid UV sensitizer. Specifically, PAGs are provided that bear a chromophore capable of receiving mid UV radiation, particularly I-line, and that are suitable for use in a chemically amplified photo resist having a photo speed of 500 mJ/cm.sup.2 or less, but preferrably 200 mJ/cm.sup.2 or less. For example, the PAGs can be a sulfonium or iodonium salt, such as anthryl, butyl, methyl sulfonium triflate and bis(4-t-butylphenyl)iodonium 9,10-dimethoxyanthracene sulfonate. The chromophore forming a part of the PAGs can be selected from polyaromatic hydrocarbons, for example, chrysenes, pyrenes, fluoranthenes, anthrones, benzophenones, thioxanthones, anthracenes, and phenanthrenes, but preferably anthracenes.
摘要翻译： 提供了几个中等紫外光酸产生剂（PAG），化学放大光抗蚀剂（CAMP）和改进嵌套到隔离线偏压的方法。 类似地，也可以提高照相速度。 与传统的中等紫外线PAG不同，本发明的PAG化合物，抗蚀剂组合物和方法不需要中等紫外线敏化剂。 具体地说，提供了能够承受中等紫外线辐射，特别是I线的发色团的PAG，并且适合用于光速为500mJ / cm 2以下但优选为200mJ / cm 2的化学放大型光致抗蚀剂的PAG， cm2以下。 例如，PAG可以是锍或碘鎓盐，例如蒽基，丁基，甲基锍三氟甲磺酸酯和双（4-叔丁基苯基）碘9,10-二甲氧基蒽磺酸盐。 形成PAG的一部分的发色团可以选自多芳族烃，例如氯仿，芘，荧蒽，蒽，二苯甲酮，噻吨酮，蒽和菲，但优选为蒽。
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公开(公告)号：US4013801A
公开(公告)日：1977-03-22
申请号：US657906
申请日：1976-02-13
IPC分类号： A23G3/00 , A23G3/36 , A23L27/20 , A23L27/30 , A61K8/49 , A61K47/22 , A61Q11/00 , C07C45/71 , C07C45/74 , C07C49/84 , C07D295/26 , C07D311/32 , A23L1/236
CPC分类号： C07D311/32 , A23G3/36 , A23L27/2052 , A23L27/30 , A61K47/22 , A61K8/498 , A61Q11/00 , C07C45/71 , C07C45/74 , C07C49/84 , C07D295/26
摘要： Edible materials including foods, beverages and oral pharmaceuticals are sweetened by the addition of a sweetening amount in the range of from about 0.002% to 1% by weight (basis edible material) of flavanone represented by the structural formula ##STR1## wherein R is a lower alkyl of from one to three carbon atoms inclusive, n is an integer of from one to three inclusive and M is hydrogen or a physiologically acceptable metal cation.
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