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22 条记录 (耗时 0.024 秒)

    Process for preparing a thioindigo derivatives comprising cyclizing in a liquid mixture of an aluminium halide an alkali metal halide, and a carboxamide or sulfonamide
    1.
    发明授权
    Process for preparing a thioindigo derivatives comprising cyclizing in a liquid mixture of an aluminium halide an alkali metal halide, and a carboxamide or sulfonamide 失效
    制备硫靛衍生物的方法，其包括在卤化铝和碱金属卤化物的液体混合物中环化，以及羧酰胺或磺酰胺

    公开(公告)号：US4652660A

    公开(公告)日：1987-03-24

    申请号：US755048

    申请日：1985-07-15

    申请人： Detlef-Ingo Schutze ,  Klaus Wunderlich

    发明人： Detlef-Ingo Schutze ,  Klaus Wunderlich

    IPC分类号： C09B7/10 ,  C07D333/64 ,  C07D409/04

    CPC分类号： C09B7/10

    摘要： Process for preparing thioindigo compounds of the formula ##STR1## in which A and B denote identical or different, optionally substituted benzene rings or benzene rings to which may be joined further carbocyclic and heterocyclic rings,characterized in that compounds of the formulae ##STR2## in which A and B have the abovementioned meaning andX denotes halogen, such as bromine and preferably chlorine,are reacted in a liquid mixture of an aluminium halide, an alkali metal halide and a carboxamide or sulphonamide, and the resulting intermediate product is subsequently, if desired after prior isolation, oxidized in a manner known per se, and the batch is worked up for the compounds of the formula (I).

    摘要翻译： 制备式（I）的硫靛化合物的方法，其中A和B表示相同或不同的任选取代的苯环或苯环，其中可以连接有碳环和杂环，其特征在于式 其中A和B具有上述含义并且X表示卤素如溴，优选氯，在卤化铝，碱金属卤化物的液体混合物中反应的图像（IIa）和/或

    Process for the preparation of naphthalene-1,8-dicarboximides
    2.
    发明授权
    Process for the preparation of naphthalene-1,8-dicarboximides 失效
    萘-1,8-二羧酰亚胺的制备方法

    公开(公告)号：US4892950A

    公开(公告)日：1990-01-09

    申请号：US204468

    申请日：1988-06-09

    申请人： Detlef-Ingo Schutze ,  Klaus Wunderlich ,  Karl-Heinz Reinhardt ,  Martin Wienkenhover

    发明人： Detlef-Ingo Schutze ,  Klaus Wunderlich ,  Karl-Heinz Reinhardt ,  Martin Wienkenhover

    IPC分类号： C07D221/14

    CPC分类号： C07D221/14

    摘要： Process for the preparation of naphthalene-1,8-dicarboximide which is optionally substituted in the naphthalene ring, characterized in that naphthalene-1,8-dicarboxylic anhydride which is optionally substituted in the naphthalene ring is reacted with an ammonium salt in an aqueous medium at a pH near to the neutral point, the reaction mixture is then acidified to a pH of 1 to 4 and the pH is subsequently adjusted to a value near to the neutral point.

    摘要翻译： 在萘环中任选取代的萘-1,8-二羧酰亚胺的制备方法，其特征在于在萘环中任选取代的萘-1,8-二羧酸酐与含水介质中的铵盐反应 在接近中性点的pH下，将反应混合物酸化至1至4的pH，随后将pH调节至接近中性点的值。

    Process for the preparation of thioindigo compounds
    3.
    发明授权
    Process for the preparation of thioindigo compounds 失效
    制备硫靛化合物的方法

    公开(公告)号：US4555580A

    公开(公告)日：1985-11-26

    申请号：US535543

    申请日：1983-09-26

    申请人： Detlef-Ingo Schutze ,  Reinold Schmitz ,  Klaus Wunderlich

    发明人： Detlef-Ingo Schutze ,  Reinold Schmitz ,  Klaus Wunderlich

    IPC分类号： C09B7/10 ,  C07D333/24

    CPC分类号： C09B7/10

    摘要： Process for the preparation of thioindigo compounds of the formula ##STR1## in which A and B designate identical or different, optionally substituted benzene rings or benzene rings to which further carbocyclic and heterocyclic rings can be fused,characterized in that compounds of the formula ##STR2## in which A and B have the abovementioned meaning, are reacted in a mixture of chlorosulphonic acid and a further halide of an inorganic acid and, if appropriate, the resulting reaction product is oxidized in a manner which is in itself known and the batch is worked up to give compounds of the formula (I).

    摘要翻译： 制备式（I）的硫靛化合物的方法，其中A和B表示相同或不同的任选取代的苯环或苯环，其中可以与其进一步的碳环和杂环稠合，其特征在于， 其中A和B具有上述含义的式（IIa）和/或（IIb）在氯磺酸和无机酸的另外的卤化物的混合物中反应，如果合适的话，所得反应 产物以本身已知的方式被氧化，并且批处理以得到式（I）的化合物。

    Polycyclic dyestuffs
    4.
    发明授权
    Polycyclic dyestuffs 失效
    多环染料

    公开(公告)号：US4190726A

    公开(公告)日：1980-02-26

    申请号：US915020

    申请日：1978-06-13

    申请人： Detlef-Ingo Schutze ,  Klaus Wunderlich

    发明人： Detlef-Ingo Schutze ,  Klaus Wunderlich

    IPC分类号： C09B57/00 ,  C09B57/08 ,  C07D471/22

    CPC分类号： C09B57/08 ,  Y10S8/922

    摘要： In spite of their pigment character, dyestuffs of the formula ##STR1## are outstandingly suitable for dyeing synthetic fibres, in particular polyester fibres, by customary methods, strong yellow dyeings with good fastness to light and sublimation being obtained. In the abovementioned formula:R.sub.1 and R.sub.3 denote hydrogen, alkyl, aralkyl, alkoxyalkyl, alkoxycarbonyl, alkoxycarbonylalkyl or aryl,R.sub.2 and R.sub.4 denote alkylcarbonyl, arylcarbonyl, alkoxycarbonyl, --CN or --CONX.sub.1 X.sub.2,X.sub.1 denotes hydrogen, alkyl, aralkyl, aryl or cycloalkyl andX.sub.2 denotes hydrogen or alkyl.

    摘要翻译： 尽管它们具有颜料特性，但是通过常规方法对式（IMAGE）的染料非常适合用于染色合成纤维，特别是聚酯纤维，得到具有良好的耐光牢度和升华性的强黄色染色。 在上述式中：R 1和R 3表示氢，烷基，芳烷基，烷氧基烷基，烷氧基羰基，烷氧基羰基烷基或芳基，R 2和R 4表示烷基羰基，芳基羰基，烷氧基羰基，-CN或-CONX 1 X 2，X 1表示氢，烷基，芳烷基，芳基或环烷基 X2表示氢或烷基。

    Process for the preparation of thioindigo compounds
    5.
    发明授权
    Process for the preparation of thioindigo compounds 失效
    制备硫靛化合物的方法

    公开(公告)号：US4260778A

    公开(公告)日：1981-04-07

    申请号：US40520

    申请日：1979-05-21

    申请人： Detlef-Ingo Schutze ,  Klaus Wunderlich

    发明人： Detlef-Ingo Schutze ,  Klaus Wunderlich

    IPC分类号： C09B7/10

    CPC分类号： C09B7/10

    摘要： Process for the preparation of thioindigo compounds of the formula ##STR1## in which A and B designate identical or different optionally substituted benzene rings or benzene rings onto which further carbocyclic and heterocyclic rings are fused,characterized in that compounds of the formula ##STR2## in which A and B have the meaning indicated above andX designates halogen, such as bromine and, preferably, chlorine,are reacted in a liquid mixture of an aluminium halide, an alkali metal halide and SO.sub.2 and the resulting intermediate product is then oxidized in a manner which is in itself known, if appropriate after first being isolated, and the mixture is worked up to give the compounds of the formula (I).

    摘要翻译： 制备式（I）的硫靛化合物的方法，其中A和B表示相同或不同的任选取代的苯环或苯环，其上还有碳环和杂环稠合，其特征在于式 （IIa）（IIb）其中A和B具有上述含义，X表示卤素，例如溴，优选氯，在卤化铝，碱金属卤化物的液体混合物中反应 然后将所得中间产物以本身已知的方式氧化，如果在首次分离后适当，则将其混合，得到式（I）化合物。

    Process for the preparation of 6,13-dihydroquinacridones and quinacridones
    6.
    发明授权
    Process for the preparation of 6,13-dihydroquinacridones and quinacridones 失效
    制备6,13-​​二氢喹吖啶酮和喹吖啶酮的方法

    公开(公告)号：US4812568A

    公开(公告)日：1989-03-14

    申请号：US12921

    申请日：1987-02-10

    申请人： Helmut Herzog ,  Detlef-Ingo Schutze ,  Jurgen Schneider ,  Reinold Schmitz

    发明人： Helmut Herzog ,  Detlef-Ingo Schutze ,  Jurgen Schneider ,  Reinold Schmitz

    IPC分类号： C07D471/04 ,  C09B48/00

    CPC分类号： C07D471/04 ,  C09B48/00

    摘要： Process for the preparation of a 6,13-dihydroquinacridone of the general formula (I) ##STR1## in which R.sup.1, R.sup.2, R.sup.3 and R.sup.4 designate hydrogen or substituents customary for quinacridone, characterized in that an optionally substituted dialkyl 2,5-di-(phenylamino)-3,6-dihydroterephthalate is heated to temperatures of 240.degree.-320.degree. C. in an essentially oxygen-free atmosphere in the presence of a dimethyl-diphenyl ether isomer mixture of the formula ##STR2## as the solvent and/or diluent, and a process for the preparation of optionally substituted quinacridone, characterized in that the resulting 6,13-dihydroquinacridone is oxidized in the customary manner.

    摘要翻译： 用于制备通式（I）的化合物（I）的6,13-​​二氢喹吖啶酮的方法其中R 1，R 2，R 3和R 4表示氢或通常用于喹吖啶酮的取代基，其特征在于任选取代的二烷基2， 将5-二 - （苯基氨基）-3,6-二氢对苯二甲酸酯在基本上不含氧的气氛中在二甲基 - 二苯基醚异构体混合物存在下加热到240-320℃的温度，式 II）和/或作为溶剂和/或稀释剂的（IIa）和/或制备任选取代的喹吖啶酮的方法，其特征在于所得的6,13-​​二氢喹吖啶酮以常规方式被氧化。

    Dispersion of post-curable coating compounds
    8.
    发明授权
    Dispersion of post-curable coating compounds 失效
    后固化涂料化合物的分散

    公开(公告)号：US5738912A

    公开(公告)日：1998-04-14

    申请号：US760093

    申请日：1996-12-11

    申请人： Eberhard Konig ,  Detlef-Ingo Schutze ,  Josef Pedain

    发明人： Eberhard Konig ,  Detlef-Ingo Schutze ,  Josef Pedain

    IPC分类号： C08G18/08 ,  C08G18/12 ,  C08G18/28 ,  C08G18/44 ,  C14C11/00 ,  D06N3/14 ,  B05D7/12

    CPC分类号： D06N3/14 ,  C08G18/0804 ,  C08G18/12 ,  C08G18/283 ,  C08G18/44 ,  C14C11/006

    摘要： The invention relates to a method for coating textiles and/or leather with an aqueous dispersion comprising (A) a mixture of (i) a urethane-containing blocked NCO prepolymer having a number average molecular weight of 2000 to 10,000, a content of blocked isocyanate groups (calculated as NCO) of 0.5 to 5 wt. %, an ethoxy group content of 2 to 50 wt. %, an ionic group content of 5 to 30 meq per 100 g of the prepolymer, and (ii) a polyamine having (cyclo)aliphatically bonded primary and/or secondary amino groups, wherein the equivalent ratio of blocked NCO groups of component (i) to amino groups of component (ii) is 1:0.9 to 1:1.2, and (B) an aqueous phase.

    摘要翻译： 本发明涉及一种用水分散体涂布纺织品和/或皮革的方法，其包含（A）（i）数均分子量为2000至10,000的含氨基甲酸酯的封闭NCO预聚物，封端异氰酸酯的含量 基团（以NCO计算）为0.5〜5wt。 ％，乙氧基含量为2〜50wt。 ％，每100g预聚物的离子基团含量为5至30meq，和（ii）具有（环）脂族键合的伯和/或仲氨基的多胺，其中组分（i）的封闭NCO基团的当量比 ）至组分（ⅱ）的氨基为1：0.9至1：1.2，和（B）水相。

    Coating compositions for coatings that are permeable to water vapor and a process for their preparation
    9.
    发明授权
    Coating compositions for coatings that are permeable to water vapor and a process for their preparation 失效
    可渗透水蒸气的涂料涂料组合物及其制备方法

    公开(公告)号：US5252671A

    公开(公告)日：1993-10-12

    申请号：US887213

    申请日：1992-05-21

    申请人： Josef Pedain ,  Klaus Noll ,  Wilhelm Thoma ,  Detlef-Ingo Schutze

    发明人： Josef Pedain ,  Klaus Noll ,  Wilhelm Thoma ,  Detlef-Ingo Schutze

    IPC分类号： C14C11/00 ,  C08L75/00 ,  C09D133/04 ,  C09D175/00 ,  C09D175/04 ,  D06M15/564 ,  D06N3/04 ,  D06N3/14 ,  C08F8/30

    CPC分类号： D06N3/14 ,  C09D133/04 ,  C09D175/04 ,  C08L75/00 ,  Y10S528/904

    摘要： The present invention relates to coating compositions containing(A) 70 to 98% by weight, based on the sum of components (A) and (B), of(a) isocyanate-free polymers of ethylenically unsaturated monomers and/or polyurethanes or blocked isocyanate prepolymers, and(b) optional organic solvents, wherein component (A) contains no significant quantities of groups capable of reacting with component (B) or starting materials thereof and has a viscosity (at 23.degree. C.) of 2000 to 100,000 mPa.s;(B) 2 to 30% by weight, based on the sum of components (A) and (B), of a polyaddition product prepared in and dispersed in component (A), wherein the polyaddition product is a polyurethane, polyurethane urea, polyurea, or mixture thereof, containing ionic groups and/or potentially ionic groups in a quantity corresponding to from 0.5 to 20 milliequivalents per 100 g of component (B) but containing substantially no free isocyanate, hydroxyl, or amino groups: and(C) optional cross-linking agents;in which component (B) is formed in situ in component (A).

    摘要翻译： 本发明涉及涂料组合物，其包含（A）70至98重量％，基于组分（A）和（B）的总和，（a）烯属不饱和单体和/或聚氨酯或封闭的无异氰酸酯的聚合物 异氰酸酯预聚物和（b）任选的有机溶剂，其中组分（A）不含有显着量的能够与组分（B）或其原料反应的基团，并且具有2000至100,000mPa的粘度（在23℃） .s; （B）基于组分（A）和（B）的总和，制备和分散在组分（A）中的加聚产物的2-30重量％，其中所述加聚产物是聚氨酯，聚氨酯脲，聚脲 或其混合物，其含有相对于每100g组分（B）0.5至20毫当量但基本上不含游离异氰酸酯，羟基或氨基的量的离子基团和/或潜在的离子基团：和（C）任选的 交联剂; 其中组分（B）在组分（A）中原位形成。